• Title/Summary/Keyword: Dried Layer

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Dehydration Kinetics of Rehmannia (Rehmannia glutinosa Liboschitz)

  • Rhim, Jong-Whan;Kim, Ji-Hye;Jeong, Won-Chul
    • Food Science and Biotechnology
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    • v.16 no.5
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    • pp.771-777
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    • 2007
  • Sliced and whole root of rehmannia were dehydrated in a laboratory dryer at 40, 60, 80, and $100^{\circ}C$ to evaluate the kinetic parameters for dehydration of rehmannia. The drying curves of both samples were characterized by a falling-rate drying period only. Sliced rehmannia dried 1.1 to 3.1 times faster than whole root of rehmannia depending on drying temperature. Equilibrium moisture content (EMC) of rehmannia samples at the drying temperature tested were 0.069-0.078 g water/g dry solid, which was coincided with the monolayer moisture content (0.06 and 0.07 g water/g dry solid) evaluated from desorption isotherms using GAB (Guggenheim-Anderson-de Boer) model. A logarithmic model for thin layer drying was applied to evaluate the drying time to reach EMC ($t_{EMC}$) and drying constant (k). The effect of temperature on $1/t_{EMC}$ and k was described by the Arrhenius model with activation energy values of 32.56 and 47.14 kJ/mol determined using the former parameter, and 34.27 and 38.26 kJ/mol determined using the latter parameter for sliced and whole root of rehmannia, respectively.

Minimum Specific Airflow Rate Requirements for Natural Air Drying of Rough Rice in Korea (벼 상온통풍건조의 최소풍량비에 관한 연구)

  • 금동혁;박선태
    • Journal of Biosystems Engineering
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    • v.21 no.1
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    • pp.60-71
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    • 1996
  • The purposes of this study were to develop a simulation model and to determine minimum specific airflow rate requirements for natural air drying of rough rice in Korea. A simulation model was developed considering energy and mass balances within grain bed, drying and rewetting rates, and hysterisis effect between sorption and desorption isotherms. As the results of validation test, the moisture contents predicted by the model agreed very well with the actual data. The criteria for determining minimum specific airflow rate requirements was that the top loom layer in the bin be dried to a moisture content below 16 percent wet basis with less than 0.5% drymatter decomposition. The minimum specific airflow rate requirements in 13 locations of Korea were presented based on the worst one among the past 7 to 13-year weather data. These requirements were also presented for all the combinations of three harvest dates and four harvest moisture contents. Specific airflow rate requirements seemed to be half by each 2 percent reduction in moisture content from 24 percent. As harvest date was delayed by 10 days from October 1, these requirements were reduced by about 20 to 40 percent.

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DRYING CHARACTERISTINCS OF THIN-LAYERS OF WHEAT AND BARLEY AT NEAR-AMBIENT TEMPERATURE

  • Sun, Da-Wen;J.J.Woods
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 1993.10a
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    • pp.896-905
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    • 1993
  • Thin-layers of wheat and barley are dried at near-ambient temperatures(3.5$^{\circ}C$ -5$0^{\circ}C$) in order to obtain the intrinsic drying data. The well established apparatus was modified to enable it to record all the sample weight data in still air by using a purpose -built automatically controlled sliding valve. The air could be diverted in less than 0.5seconds and a 7 second period was required to attain a steady weight reading. With this apparatus, very smooth drying curves were obtained. The data of sample weight , drying temperature and dew point temperature wee recorded continuously . The drying process was terminated when the moisture content change in 24 hours was less than 0.004 d.b. This was achieved by drying a sample for about a week . The final points were recorded as the dynamic equilibrium moisture content(EMC). The drying data were than fitted to the exponential Newton model and the dynamic EMC data were fitted to the Modified-Chung-Pfost Model . All the fitted parameters are given and comparison is made with previous published data. The comparisons who that the current drying constants are lower than the previous data, the dynamic EMC data obtained for wheat and barely agree with the previous data. The results show that to obtain the drying constant in the exponential Newton model, adequate drying time is necessary.

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Antioxidant Activity and Total Phenolic Content of Triphala churna

  • Jayajothi, E.;Elavarasu, T.;Hamsaveni, M.;Sridhar, S.K.
    • Natural Product Sciences
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    • v.10 no.1
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    • pp.16-19
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    • 2004
  • Triphala churna is a widely used herbal formulation that contains equal proportion of dried fruit powder of Emblica officinalis, Terminalia chebula and Terminalia belirica. In the Indian system of medicine, it is used in cleaning wounds, urinary disorders, diabetes mellitus, leprosy, constipation, eyesight promotion, piles, and as a rejuvenator. In the present study, the methanolic extract of 5 commercial Triphala was evaluated for antioxidant activity by 1,1-diphenyl-2-picryl-hydrazyl free radical scavenging method, total phenolic content by Folin-Ciocalteu method and gallic acid equivalents (GAE) by high performance thin layer chromatographic (HPTLC) method. All extracts exhibited antioxidant activity significantly. The $IC_{50}$ of the extracts ranged between $7.16\;to\;12.96\;{\mu}g/ml$. The total phenolic content of the extracts was found to be 195.3-296.4 mg of GAE/gm of GAE/gm dw. The HPTLC chromatographic data reveal that the content of GAE present in the extract was found to be $7.17-4.11\;{\mu}g/ml$. The study reveals that out of the churnas analysed, C was found to exhibit the most potent antioxidant activity. A clear correlation between $IC_{50}$ and content of GAE nor the total phenolic content could be observed. The study reveals that the consumption of Triphala would exert several beneficial effects by virtue of its antioxidant activity.

Improved Method for the Preparation of Crude Ginseng Saponin (인삼 조사포닌의 조제 방법 개선)

  • 김시관;곽이성
    • Journal of Ginseng Research
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    • v.22 no.3
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    • pp.155-160
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    • 1998
  • This stuffy was carried to establish a new efficient method for the preparation of edible crude ginseng saponin. The conventional butanol extraction and resin adsorption methods were compared for the contents of total crude ginseng saponin and major ginsenosides. Seventy- percent methanol extract was applied to Diaion HP-20 column and the resin was washed with Hn and eluted with absolute methanol. The methanol elute was dried in vivo and analyzed for its ginsenosides. Use of ethanol instead of methanol to make edible crude ginseng saponin gave a similar result. Butanol extraction was performed by the conventional method. The final aqueous layer from butanol extraction was passed through Diaion HP-20 column followed by elution with methanol and Diaion HP-20 passed fraction was extracted with butanol to recover remaining components, respectively, in order to determine saponin loss. TLC and HPLC qualitatively and quantitatively monitored Ginsenosides, respectively. Loss of ginsenosides was higher in butanol extraction method than in Diction HP-20 adsorption method. In addition, saponin fractions prepared by Diction HP-20 adsorption method showed higher content of each ginsenoside, showing 8.2% higher purity than that of butanol extracted fraction. From these results, we propose the resin adsorption method as a new efficient measure for the preparation of crude ginseng saponin, which is edible by using spirit instead of methanol.

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Evaluation of Life Span for Al2O3 Nano Tube Formed by Anodizing with Current Density

  • Lee, Seung-Jun;Kim, Seong-Jong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.148-148
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    • 2017
  • Surface modification is a type of mechanical manipulation skills to achieve extensive aims including corrosion control, exterior appearance, abrasion resistance, electrical insulation and electrical conductivity of substrate materials by generating a protective surface using electrical, physical and chemical treatment on the surface of parts made from metallic materials. Such surface modification includes plating, anodizing, chemical conversion treatment, painting, lining, coating and surface hardening; this study conducted cavitation experiment to assess improvement of durability using anodizing. In order to observe surface characteristics with applied current density, the electrolyte temperature, concentration was maintained at constant condition. To prevent hindrance of stable growth of oxide layer due to local temperature increase during the experiment, stirring was maintained at constant speed. In addition, using galvanostatic method, it was maintained at processing time of 40minutes for 10 to $30mA/cm^2$. The cavitation experiment was carried out with an ultra sonic vibratory apparatus using piezo-electric effect with modified ASTM-G32. The peak-to-peak amplitude was $30{\mu}m$ and the distance between the horn tip and specimen was 1mm. The specimen after the experiment was cleaned in an ultrasonic bath, dried in a vacuum oven for more than 24 hours, and weighed with an electric balance. The surface damage morphology was observed with 3D analysis microscope. As a result of the study, differences were observed surface hardness and anti-cavitation characteristics depending on the development of oxide film with the anodizing process time.

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A Study on the Grain Growth and PLZT Ceramics Fabrication by Freeze Drying Method. (동결건조법에 의한 PLZT 세라믹 제조 및 결정립 성자에 관한 연구.)

  • Lee, Sung-Gap;Ryu, Ki-Won;Lee, Young-Hie
    • Proceedings of the KIEE Conference
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    • 1987.11a
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    • pp.492-495
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    • 1987
  • In this study, PLZT ceramics were fabricated by freeze-drying and normal sintering method. The compositional rate of specimen was selected 9/65/35 (La/Zr/Ti) which have good optical and dielectric properties, sintering time was varied 1, 10, 30, 40, 50, 55, 60 and 65 hr at $1250^{\circ}C$. After sintering, the optical and dielectric properties were investigated with the grain size. As the result of the experiment, freeze-dried powder appeared particle size less than 1 um. The relative dielectric constant was increased linearly with the sintering time, specimen which sintered for 65 hr had the highest value, 5780. Grain was grown with increasing time, in the case of specimen sintered for 60 hr, the grain size was 8.4 um. Transmittance was increased with the grain size. In the case of 8.4 um grain size, the transmittance was 56 %. Curie temperature was decreased linearly by the surface-layer effect of space-charge, in the case of grain size which were 1.8 um and 8.4 um, appeared at $100^{\circ}C$ and $80^{\circ}C$, respectively.

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Fungal Flora and Mycotoxins Associated with Onion (Allium cepa L.) in Egypt (양파에 관련된 균독소 및 균프로라에 관한 연구)

  • Zohri, A. A.;Sabah, Asber M.;Abdel-Gawad, K. M.
    • The Korean Journal of Mycology
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    • v.20 no.4
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    • pp.302-308
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    • 1992
  • Seven genera and 15 species of fungi were isolated from 50 samples of then different steps of dried onion (5 samples of each step) collected from an onion factory in Sohag Governorate, Egypt, and grown on glucose-Czapek's agar (7 genera and 15 species) and 10% NaCl glucose-Czapek's (2 genera and 6 species). The average total counts of fungi were gradually decreased throughout the different steps of drying from 2090 to zero and 152 to zero colonies/g on glucose-Czapek's agar and 10% NaCl glucose-Czapek's agar media, respectively. Aspergillus was the most common genus on the two types of media used. The dominant species were Aspergillus niger, A. flavus, A. terreus, Penicillium chrysogenum and Fusarium of oxysporum on glucose-Czapek's agar and A. terreus and A. niger on 10% NaCl glucose-Czapek's agar. The chloroform extracts of different samples were tested for the presence of mycotoxins using thin layer chromatographic analysis. The results indicated that aflatoxin was present at concentrations decreased throughout the different steps of the drying from step No. 1, onion bulbs, $120\;{\mu}g/kg$; to step No. 8, standard A, $20\;{\mu}g/kg$ while step Nos. 9 & 10 (completely dry powdered onion) were free from aflatoxin. Citrinin was also present in the first three steps at concentrations gradually decreased from 30 to 10 mg/kg.

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Isolation and Identification of Antimicrobial Compound from Dansam (Saliuia miltiorrhiza Bunge) (단삼으로부터 식품부패미생물에 대한 항균성 물질의 분리 및 동정)

  • 최해연;한영실
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.32 no.1
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    • pp.22-28
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    • 2003
  • Antimicrobial effect of Dansham (Saliuia miltiorrhiza Bunge) was investigated. Methanol extract of dried Dansham was fractionated to hexane, chloroform, ethylacetate, butanol and aqueous fraction. Chloroform fraction showed the highest inhibitory effect on the microorganisms such as B. subtilis, S. aureus, E. coli, L. monocytogenes and V. parahaemolyticus at 250 $\mu\textrm{g}$/disc. Chloroform fraction was further fractionated by silica gel column and thin layer chromatography (TLC). The antimicrobial compound was isolated from their fractions and its chemical structure was identified as a cryptotanshinone by GC-MS and $^1$H-NMR, $^{13}$ C-NMR.

An Experimental Study on the Freeze Drying Process for Poly γ Glutamic Acid (폴리감마글루탐산의 동결 건조 과정의 실험적 연구)

  • Kang, Jisu;Sim, Yeon-Ho;Byun, Si-Ye;Chang, Young Soo;Kang, Byung Ha
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.27 no.12
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    • pp.645-651
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    • 2015
  • This paper presents an experimental study on the freeze drying process for poly ${\gamma}$ glutamic acid. The physical properties of poly ${\gamma}$ glutamic acid are measured during the freeze-drying process. The moisture contents of poly ${\gamma}$ glutamic acid according to the glass transient temperature are obtained by DSC (Differential Scanning Calorimetry) analysis. The end point of primary drying for the poly ${\gamma}$ glutamic acid with a thickness of 3 mm is obtained by measuring the thickness of the dried layer, the amount of moisture evaporation, the moisture content, and the pressure in the drying vacuum chamber during the freeze-drying process. By considering the variation in the glass transient temperature with respect to the moisture content of the material, a control schedule for the heating plate temperature is suggested during the secondary drying process.