• Composites Research
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• v.24 no.5
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• pp.39-43
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• 2011

For the last twenty years, nanocomposites composed of polymer matrices reinforced with carbon nanotubes (CNTs) have been an active research area. Also, the polymeric nanocomposites reinforced with CNTs are being investigated to be used matrices of carbon fiber composites. Carbon tiber composites have achieved advanced properties in the direction of carbon fibers due to enhanced carbon fiber properties. However, the matrix dominated properties need to be improved further to fully utilize the advanced carbon fiber properties. In particular, delamination is a typical and critical reason for fracture of carbon fiber composites. Mode I fracture toughness test which is also often called double cantilever beam (DCB) test shows the resistance to delamination of carbon fiber composites and this test is performed on carbon fiber composite samples incorporated with carbon nanotubes functionalized with various functional groups. The specimens with mat-like CNT layers showed the increased fracture toughness by 10.6%.

• Composites Research
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• v.34 no.5
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• pp.323-329
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• 2021

In this paper, the characteristics of fracture in mode I loading were analyzed for adhesively bonded joints with non-uniform adhesion. The Double Cantilever Beam test was performed and mode I fracture toughness was obtained. In the case of non-uniform adhesively bonded joints, the stable crack growth sections and unstable crack growth section were shown. The fracture characteristics of each section were observed through the load-displacement curve of the DCB test and the fracture surface of the specimen. Finite Element Analysis was performed at the section based on segmented section by crack length measured through the test and using the mode I fracture toughness of each section. Through DCB test results and finite element analysis results, it was confirmed that the fracture behavior of specimens with non-uniform adhesion can be simulated.

• Journal of the Korea Concrete Institute
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• v.13 no.2
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• pp.153-160
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• 2001

In this study, the size effect on axial compressive strength for concrete members was experimentally investigated. Experiment of mode I failure, which is one of the two representative compressive failure modes, was carried out by using double cantilever beam specimens. By varying the eccentricity of applied loads with respect to the axis on each cantilever and the initial crack length, the size effect of axial compressive strength of concrete was investigated, and new parameters for the modified size effect law (MSEL) were suggested using least square method (LSM). The test results show that size effect appears for axial compressive strength of cracked specimens. For the eccentricity of loads, the influence of tensile and compressive stress at the crack tip are significant and so that the size effect is present. In other words, if the influence of tensile stress at the crack tip grows up, the size effect of concrete increases. And the effect of initial crack length on axial compressive strength is present, however, the differences with crack length are not apparent because the size of fracture process zone (FPZ) of all specimens in the high-strength concrete is similar regardless of differences of specimen slenderness.

• Journal of the Microelectronics and Packaging Society
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• v.27 no.3
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• pp.41-47
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• 2020

The effect of Co interlayer on the interfacial reliability of SiN_x/Co/Cu thin film structure for advanced Cu interconnects was systematically evaluated by using a double cantilever beam test. The interfacial adhesion energy of the SiN_x/Cu thin film structure was 0.90 J/㎡. This value of the SiN_x/Co/Cu thin film structure increased to 9.59 J/㎡.Measured interfacial adhesion energy of SiN_x/Co/Cu structure was around 10 times higher than SiN_x/Cu structure due to CoSi₂ reaction layer formation at SiN_x/Co interface, which was confirmed by X-ray photoelectron spectroscopy analysis. The interfacial adhesion energy of SiN_x/Co/Cu structure decreased sharply after post-annealing at 200℃ for 24 h due to Co oxidation at SiN_x/Co interface. Therefore, it is required to control the CoO and Co₃O₄ formation during the environmental storage of the SiN_x/Co/Cu thin film to achieve interfacial reliability for advanced Cu interconnections.

• Composites Research
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• v.29 no.2
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• pp.45-52
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• 2016

An understanding of the failure mechanisms of the adhesive layer is decisive in interpreting the performance of a particular adhesive joint because the delamination is one of the most common failure modes of the laminated composites such as the fiber metal laminates. The interface between different materials, which is the case between the metal and the composite layers in this study, can be loaded through a combination of fracture modes. All loads can be decomposed into peel stresses, perpendicular to the interface, and two in-plane shear stresses, leading to three basic fracture mode I, II and III. To determine the load causing the delamination growth, the energy release rate should be identified in corresponding criterion involving the critical energy release rate ($G_C$) of the material. The critical energy release rate based on these three modes will be $G_{IC}$, $G_{IIC}$ and $G_{IIIC}$. In this study, to evaluate the fracture behaviors in the fracture mode I and II of the adhesive layer in fiber metal laminates, the double cantilever beam and the end-notched flexure tests were performed using the reference adhesive joints. Furthermore, it is confirmed that the experimental results of the adhesive fracture toughness can be applied by the comparison with the finite element analysis using cohesive zone model.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.23 no.11 s.170
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• pp.1886-1895
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• 1999

The delamination behavior of multidirectional carbon-fiber/epoxy composite laminates under 10NA intermediate and high rates of test, up to rate of about 11.4m s has been investigated using the double cantilever beam specimens. The mode I loading under rates above l.0m/s showed considerable dynamic effects on the load-time curves and thus higher values of the average crack velocity than that expected from a simple proportional relationship with the test rate. The modified beam analysis utilizing only the opening displacement and crack length exhibited an effective means for evaluating the dynamic fracture energy $G_{IC}$. Based on the assumption of constant flexural modulus, values of $G_{IC}$ at the crack initiation and arrest were decreased with an increase of the test rate up to 5.7m/s, but the maximum $G_{IC}$ was increased at 11.4m/s.

• Journal of the Korean Wood Science and Technology
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• v.43 no.6
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• pp.861-867
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• 2015

The Compact Tension (CT) type test was performed in order to evaluate the fracture toughness performance of glass fiber-reinforced laminated timber. Glass fiber textile and sheet Glass fiber reinforced plastic were used as reinforcement. The reinforced laminated timber was formed by inserting and laminating the reinforcement between laminated woods. Compact tension samples are produced under ASTM D5045. The sample length was determined by taking account of the end distance of 7D, and bolt holes (12 mm, 16 mm, 20 mm) had been made at the end of artificial notches in advance. The fracture toughness load of sheet fiberglass reinforced plastic reinforced laminated timber was increased 33 % in comparison to unreinforced laminated timber while the glass fiber textile reinforced laminated timber was increased 152 %. According to Double Cantilever Beam theory, the stress intensity factor was 1.08~1.38 for sheet glass fiber reinforced plastic reinforced laminated timber and 1.38~1.86 for glass fiber textile reinforced laminated timber, respectively. That was because, for the glass fiber textile reinforced laminated timber, the fiber array direction of glass fiber and laminated wood orthogonal to each other suppressed the split propagation in the wood.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.8 no.2
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• pp.135-145
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• 1988

This study deals with the prediction of crack propagation in concrete mortar subjected to static and dynamic load. Total 54 CLWL-DCB(Crack-line-loaded-double-cantilever beam) concrete mortar specimens were tested to measure crack growth using ASTM 561-80. Main variables were sand to cement ratio and water to cement ratio. The resulting load(P)-COD(Crack Opening Displacement; $2V_1$) curves and COD-CTOD (Crack Tip Opening Displacement; $2V_2$) curves were analyzed to calculate effective crack length and physical crack length by way of ASTM 561-80 proposed. Replica crack length were also obtained directly during the test. The differences in crack propagation between under static load and under dynamic load were investigated.

• Composites Research
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• v.32 no.1
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• pp.6-12
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• 2019

This paper describes the characteristics for mode I interlaminar and intralaminar fractures of cross-ply carbon/epoxy composite laminates. We obtained mode I interlaminar fracture toughness and mode I intralaminar fracture toughness based on energy release rate and Finite Element Analysis (FEA). For this purpose, the Double-Cantilever Beam (DCB) test and FEA were performed for cross-ply DCB specimens. Also, the behavior of load-displacement curve at the interlaminar and intralaminar crack was analyzed. The results show that mode I intralaminar fracture toughness was lower than mode I interlaminar fracture toughness in the cross-ply DCB specimen.

• Journal of the Microelectronics and Packaging Society
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• v.28 no.1
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• pp.39-46
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• 2021

The quantitative measurement of interfacial adhesion energy (Gc) of multilayer thin films for Cu interconnects was investigated using a double cantilever beam (DCB) and 4-point bending (4-PB) test. In the case of a sample with Ta diffusion barrier applied, all Gc values measured by the DCB and 4-PB tests were higher than 5 J/㎡, which is the minimum criterion for Cu/low-k integration without delamination. However, in the case of the Ta/Cu sample, measured Gc value of the DCB test was lower than 5 J/㎡. All Gc values measured by the 4-PB test were higher than those of the DCB test. Measured Gc values increase with increasing phase angle, that is, 4-PB test higher than DCB test due to increasing plastic energy dissipation and roughness-related shielding effects, which matches well interfacial fracture mechanics theory. As a result of the 4-PB test, Ta/Cu and Cu/Ta interfaces measured Gc values were higher than 5 J/㎡, suggesting that Ta is considered to be applicable as a diffusion barrier and a capping layer for Cu interconnects. The 4-PB test method is recommended for quantitative adhesion energy measurement of the Cu interconnect interface because the thermal stress due to the difference in coefficient of thermal expansion and the delamination due to chemical mechanical polishing have a large effect of the mixing mode including shear stress.