• 제목/요약/키워드: Diffraction pattern

검색결과 677건 처리시간 0.031초

Neutron Diffraction Study of Powders Prepared by Self-propagating High Temperature Synthesis

  • Park, Yong;Kim, Y S.;Y. D. Hahn;S. H. Shim;Lee, J. S.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2000년도 추계학술대회 및 발표대회 강연 및 발표논문 초록집
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    • pp.11-12
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    • 2000
  • Non-stoichiometric ceramics of $Ni_{x}ZnO_{1-x}Fe_{2}O_{4}$ were prepared by self-propagating high temperature synthesis reaction with various processing conditions and their stoichometric numbers were determined by neutron diffraction. The neutron diffraction patterns were measured at room temperature using monochromatic neutrons with a wave length of 0.18339 nm from a Ge(331) mocochromator at a 90 degree take off angle. The Rietveld refinement of each pattern converged to good agreement (x2=1.88-2.24). The neutron diffraction analysis revealed the final stoichiometries of the ferrites were $Ni_{0.38}Zn_{0.62}Fe_{2}O_{4}$ and $Ni_{0.33}Zn_{0.67}Fe_{2}O_{4]$, respectively. This supports that final stoichiometric number of the self-propagating high temperature synthesis product can be controlled by the processing parameters during the combustion reaction.

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Block-Quantized 이진 위상 홀로그램을 이용한 효율적인 광학적 perfect shuffle의 구현 (An implementation of the efficient optical perfect shuffle interconnection with block-quantized binary phase hologram)

  • 김희주;허현;반재경
    • 전자공학회논문지A
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    • 제33A권5호
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    • pp.125-131
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    • 1996
  • In this paper, we introduced the BQBPH method for making the grating of high efficiency which was improtant in implementing optical PS. The pattern of graing was obtianed by computer simulations using iterative method, and the diffraction efficeincy of designed grating was about 67% through BPM simulation. The grating was fabricated by laser beam writer, and the diffraction efficiency BPM simulation. The grating was fabricated by laser beam writer, and the diffraction efficiency was 47%. We implemented the optical PS with the grating and showed that optical experimental output patterns were good agreement with PS output patterns and first order was main diffraction order.

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Development of Dark Field image Processing Technique for the Investigation of Nanostructures

  • Jeon, Jongchul;Kim, Kyou-Hyun
    • 한국분말재료학회지
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    • 제24권4호
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    • pp.285-291
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    • 2017
  • We propose a custom analysis technique for the dark field (DF) image based on transmission electron microscopy (TEM). The custom analysis technique is developed based on the $DigitalMicrograph^{(R)}$ (DM) script language embedded in the Gatan digital microscopy software, which is used as the operational software for most TEM instruments. The developed software automatically scans an electron beam across a TEM sample and records a series of electron diffraction patterns. The recorded electron diffraction patterns provide DF and ADF images based on digital image processing. An experimental electron diffraction pattern is recorded from a IrMn polycrystal consisting of fine nanograins in order to test the proposed software. We demonstrate that the developed image processing technique well resolves nanograins of ~ 5 nm in diameter.

A Diffraction Transfer Function Approach to the Calculation of the Transient Field of Acoustic Radiators

  • Lee, Chan-Kil
    • ETRI Journal
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    • 제16권1호
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    • pp.1-15
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    • 1994
  • A computationally-efficient approach to the calculation of the transient field of an acoustic radiator was developed. With this approach, a planar or curved source, radiating either continuous or pulsed waves, is divided into a finite number of shifted and/or rotated versions of an incremental source such that the Fraunhofer approximation holds at each field point. The acoustic field from the incremental source is given by a 2-D spatial Fourier transform. The diffraction transfer function of the entire source can be expressed as a sum of Fraunhofer diffraction pattern of the incremental sources with the appropriate coordinate transformations for the particular geometry of the radiator. For a given spectrum of radiator velocity, the transient field can be computed directly in the frequency domain using the diffraction transfer function. To determine the accuracy of the proposed approach, the impulse response was derived using the inverse Fourier transform. The results obtained agree well with published data obtained using the impulse response approach. The computational efficiency of the proposed method compares favorably to those of the point source method and the impulse response approach.

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마게마이트(${\gamma}$-Fe$_2$O$_3$)대한 연구 I -분말 X-선 회절무늬의 Rietveld 분석- (An Study on the Structure of Maghemite(${\gamma}$-Fe$_2$O$_3$) I -Rietveld Analysis of Powder XRD Patterns-)

  • 신형섭
    • 한국세라믹학회지
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    • 제35권10호
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    • pp.1113-1119
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    • 1998
  • Crystal structure of needle-shaped maghemite(${\gamma}$-{{{{ { {Fe }_{2 }O }_{3 } }}) has been studied by the Rieveld analysis of powder X-ray diffraction patterns. The tetragonal space group P41,.3212 and cubic space group P41,.32 have been have been used for the refinement of X-ray diffraction patterns. The crystal system of maghemite is closed to tetragonal more than cubic. The tetragonal lattice parameters are a=8.3460$\AA$ and c=25.034$\AA$ The standard X-ray diffraction pattern of the tetragonal maghemite analyzed with space group P41,.3212 is proposed.

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위상편이 회절격자 간섭계의 가시도 최적화 (Visibility optimization of phase-shifting diffraction-grating interferometer)

  • 황태준;김승우
    • 한국광학회지
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    • 제14권6호
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    • pp.643-648
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    • 2003
  • 위상편이 회절격자 간섭계의 회절격자는 간섭을 일으키는 측정광과 기준광을 분할하고, 재결합하여 간섭무늬를 생성하고, 또한 위상을 편이시키는 다양한 용도로 사용되는 핵심부품이다. 위상편이 회절격자 간섭계는 회절격자에서 회절되는 다양한 회절차수의 광들을 측정광과 기준광으로 선정하고 서로 간섭시켜 간섭무의를 얻을 수 있는데, 그 회절차수와 사용하는 회절격자의 형상에 따라서 측정광과 기준광의 효율이 달라져서 간섭무늬의 가시도가 달라진다. 본 논문에서는 두 가지 위상편이 회절격자 간섭계에서 측정광과 기준광의 상대적인 효율을 격자에서 일어나는 회절현상의 전자기학적인 수치모사를 통해 산출해내어 각 간섭계에 최적인 회절격자의 형상을 선정한다.

Influence of Intermolecular Interactions on the Structure of Copper Phthalocyanine Layers on Passivated Semiconductor Surfaces

  • Yim, Sang-Gyu;Jones, Tim S.
    • Bulletin of the Korean Chemical Society
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    • 제31권8호
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    • pp.2247-2254
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    • 2010
  • The surface structures of copper phthalocyanine (CuPc) thin films deposited on sulphur-passivated and plane perylene-3,4,9,10-tetracarboxylic dianhydride (PTCDA)-covered InAs(100) surfaces have been studied by low energy electron diffraction (LEED) and van der Waals (vdW) intermolecular interaction energy calculations. The annealing to $300^{\circ}C$ and $450^{\circ}C$ of $(NH_4)_2S_x$-treated InAs(100) substrates produces a ($1{\times}1$) and ($2{\times}1$) S-passivated surface respectively. The CuPc deposition onto the PTCDA-covered InAs(100) surface leads to a ring-like diffraction pattern, indicating that the 2D ordered overlayer exists and the structure is dominantly determined by the intermolecular interactions rather than substrate-molecule interactions. However, no ordered LEED patterns were observed for the CuPc on S-passivated InAs(100) surface. The intermolecular interaction energy calculations have been carried out to rationalise this structural difference. In the case of CuPc unit cells on PTCDA layer, the planar layered CuPc structure is more stable than the $\alpha$-herringbone structure, consistent with the experimental LEED results. For CuPc unit cells on a S-($1{\times}1$) layer, however, the $\alpha$-herringbone structure is more stable than the planar layered structure, consistent with the absence of diffraction pattern. The results show that the lattice structure during the initial stages of thin film growth is influenced strongly by the intermolecular interactions at the interface.

기계적 합금화한 $\sigma$-VFe합금의 중성자 및 X선 회절에 의한 상분석 (Phase Analysis of Mechanically Alloyed $\sigma$-VFe Alloy Powders by Neutron and X-ray Diffraction)

  • 이충효;조재문;이상진;심해섭;이창희
    • 한국재료학회지
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    • 제11권8호
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    • pp.664-664
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    • 2001
  • $\sigma$-VFe 금속간화합물에 대한 기계적 합금화(MA) 효과를 중성자 및 X선 회절법으로 조사하였다. MA 분말의 구조분석은 X선 회절(Cu-K$\alpha$) 린 중성자회절(HRPD, λ=1.835$\AA$)을 이용하여 행하였다. $\sigma$-VFe화합물의 MA시 큰 구조변화가 관찰되었으며, MA 60시간의 경우 Fe-Fe 훤자분포는 unit cell에 30개의 원자를 포함하고 있는 $\sigma$상의 tetragonal구조에서 $120^{\circ}C$이상에서 안정하게 존재하는 $\alpha$-(V,Fe) 고용체의 bcc 구조로 상변화함을 알 수 있었다. 또한 $\alpha$-VFe 화합물에 대한 중성자 및 X선 회절패턴의 비교분석을 행하였으며 그 결과 $\sigma$상이 가지는 화학적 규칙성에 기인하는 (101)과 (111) 회절 피크가 중성자 회절에서 뚜렷하게 관찰됨을 알 수 있었다.

Fabrication of Poly(3,4-ethylenedioxythiopene) Patterns using Vapor Phase Polymerization

  • 조보람;성명모
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제45회 하계 정기학술대회 초록집
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    • pp.265.2-265.2
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    • 2013
  • We fabricate poly(3,4-ethylenedioxythiopene patterns using liquid-bridge-mediated nanotransfer (LB-nTM) printing via vapor phase polymerization (VPP). LB-nTM printing method can simultaneously enable the synthesis, alignment and patterning of the nanowires from molecular ink solutions. Two- or three-dimensional complex structures of VPP-PEDOT were directly fabricated over a large area using many types of molecular inks. VPP method is a versatile technique that can be used to obtain highly conducting coatings of conjugated polymer on both conducting and non-conducting substrates. The PEDOT patterns has analyzed crystallinity from X-ray diffraction pattern and select-area diffraction patterns. In addition, the PEDOT pattern has high conductivity compared other conducting polymers.

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유전체 매질내에 있는 구형공동에 의한 근거리 회절패턴 (NEAR=FIELD DIFFRACTION PATTERN BY A SPHERICAL AIR CAVITY IN A DIELECTRIC MEDIUM)

  • 강진섭;라정웅
    • 전자공학회논문지A
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    • 제32A권2호
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    • pp.19-30
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    • 1995
  • Diffraction patterns of the copolarized and the crosspolarized total electric fields by a spherical air cavity in a dielectric medium are analyzed in the forward near-field region when the wavelength of the incident plane wave is comparable to one half of the cavity radius. It is shown that double nulls and dips of the copolarized and the crosspolarized total electric fields exist in the measurement plane tansverse to the propagating direction of the incident field, and their dependences on the frequency, the distance of the measurement plane, and the measurement angle are analyzed.

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