• Title/Summary/Keyword: Diffraction angle

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The molecular structure of (+) -6-methoxy-.alpha. 1-2-naphtha-leneacetic acid determined by X-Ray method

  • Kim, Yang-Bae;Song, Hyun-June
    • Archives of Pharmacal Research
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    • v.7 no.2
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    • pp.137-139
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    • 1984
  • The molecular structure of (+)-6-Me hoxy-.alpha.-methyl-2-naphthaleneacetic acid (Naproxen), $C_{14}H_{14}O_{ 3}$, was determined by X-Ray diffraction technique. Naproxen crystallized in $P2_1$ with two molecules on the unit cell of dimensions a = 7.855, b = 5.783, c = 13.347$\AA$ and $\beta$ = $93.9^{\circ}$

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Effects of the Bio-diesel Blending Rate on the Spray Characteristics of the Pressure Swirl Nozzle (바이오 디젤 혼합율이 압력식 스월노즐의 분무 특성에 미치는 영향)

  • Yoon, S.J.
    • Journal of ILASS-Korea
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    • v.16 no.4
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    • pp.210-214
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    • 2011
  • This paper presents the spray characteristics of the gun type burner nozzle with bio-diesel blending rate. The burner nozzle used in this experiment is a pressure swirl type nozzle. For the spray characteristics, visualization of spray was conducted to obtain the spray angle, and laser diffraction spectroscope (LDS) was used for the measurement of the droplet diameters. The results showed that the $D_{max}$, SMD and spray angle were decreased with increasing the bio-diesel blending rate and BD30 (30% bio-diesel blending rate) could be found to be the maximum blending rate for using without any modification of the gun type burner of the homesize kerosene fuel boiler.

Hexaphenylbenzene $C_6(C_6H_5)_6$

  • Kim Young-Sang;Ko Jaejung;Kang Sang Ook;Han Won-Sik;Jeong Jae-Ho;Suh Il-Hwan
    • Korean Journal of Crystallography
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    • v.16 no.1
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    • pp.1-5
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    • 2005
  • The structure of the title compound has been determined by single-crystal X-ray diffraction work. The crystals are orthorhombic, space group $Pna2_1$ with a=11.095(3), b=21.834(7), c=12.574(4) $\AA$, and R1=0.0667. The average carbon bond length in aromaticity In the molecule is 1.386(1) $\AA$ and the average single bond length linking the central benEene ring and peripheral phenyl rings is 1.491(3) $\AA$. The average dihedral angle between the central benzene ring and each of six peripheral phenyl rings is $67.1(1)^{\circ}$ and the average dihedral angle between neighboring two phenyl rings is $55.0(1)^{\circ}$. Thus the molecule adopts a quasi-propeller configuration with approximate six-fold rotation symmetry.

VHOE-based Multi-view Stereoscopic 3D Display System (VHOE광학판을 이용한 다시점 스테레오 입체영상 디스플레이 시스템)

  • Cho, Byung-Chul;Koo, Jung-Sik;Kim, Seung-Cheol;Kim, Eun-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.04b
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    • pp.42-44
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    • 2002
  • The experimental model of the 8-view stereoscopic display system using the photopolymer-based VHOE is proposed. At first, the VHOE is implemented by angle-multiplexed recording of 8-view's diffraction gratings using the optimized exposure-time scheduling scheme in the photopolymer (HRF-150-100) and then. the VHOE-based 8-view stereoscopic display system is implemented by sequentially synchronizing the incident angles of the reference beam of the VHOE with the 8-view stereo images on the LCD pannel. Accordingly, from some experimental results using 8-view images generated by the toed-in stereo camera system, it is found that 8-view stereo images can be diffracted to eight different directions time-sequentially and there is some disparity between the stereo images.

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A study on the properties of amorphous (Se,S)-system thin films for reversible hologram device development (가역적 Hologram 소자개발을 위한 비정질 (Se,S)계 박막 특성에 관한 연구)

  • 김상덕;이재규;김종빈
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.31A no.12
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    • pp.71-79
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    • 1994
  • In this paper, $As_{40}Se_{50-x}S_[x}Ge_{10}$(x=0, 25, 35, at.%) bulk and thin films, to develope device of reversible hologram, proved amorphous by X-RD analysis. On the thin films with composition rate, as Se-doped-quantity increased, absorption edge shifted to long wavelength, and we found that reversible photodarkening effect occurred when thin films are exposed and annealed. Optical energy gap was larger when thin films are annealed than exposed. In this effect thin films structurally stabilized by annealing. It is to formed grating hologram by the bragg method on the $As_{40}Se_{15}S_[35}Ge_{10}$ thisn films with the best transmittance properties As polariging angle grew larger, we found that maximum diffraction efficiency became smaller, and obtained it of 4.5% on the thin fim thicknesss of 0.6 m, polarizing angle of 40$^[\circ}$ and exposing for 20sec.

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Diffraction by a sub-wavelength-sized aperture in a metal plane (파장보다 작은 금속 구멍을 통한 회절)

  • ;;Arturo Chavez-Pirson
    • Proceedings of the Optical Society of Korea Conference
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    • 2000.02a
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    • pp.164-165
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    • 2000
  • 구멍에 의한 빛의 회절은 광학의 기본적인 문제로서, 최근 근접장 광학(Near-Field Optics)의 발전과 더불어서 파장보다 작은 구멍에서 일어나는 빛의 회절에 대한 관심이 고조되고 있다.$^{(1)(2)(3)}$ 본 연구에서는 그동안 주로 이론적으로 다루어지고 있던 파장보다 작은 금속 구멍을 통한 빛의 회절에 대해 실험결과들을 보고한다. 회절된 빛의 먼장(Far-field)과, 근접장(Near-field)을 모두 측정하기 위해서 고체각 주사기(Solid angle scanner)와 근접장 주사 광학 현미경(Near-field Scanning Optical Microscopy)이 사용되었다. 고체각 주사기(Solid angle scanner)를 사용하여 반구면 위에서의 빛의 이차원 세기 분포가 다양한 편광 상태에 따라서 측정되었고$^{(4)}$ 근접장 탐침(NSOM probe)으로 작은 금속 구멍주변을 주사함으로서 근접장이 측정되었다. 작은 구멍은 최근에 개발된 고출력 근접장 광섬유 탐침(High-power near-field fiber probe)구조를 이용하여 제작되었다.$^{(5)}$

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Transission type bandpass filter using wavelength selectivity of photorefractive crystal (광굴절결정의 파장선택성을 이용한 투과형 대역통과필터)

  • An, Jun-Won;Kim, Nam;Lee, Kwon-Yeon;An, Ju-Heon
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.23 no.4
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    • pp.1051-1058
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    • 1998
  • We propose a bandpass filter using wavelength selectivity as variation of writing beam incident angle in photorefractive crystal. From TWM(Two-Wave Mixing) experiment, optimal diffraction properties are induced, and bandpass filter for selection wavelength transmission bandwidth are taken by change of writing beam incident angle.

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Synthesis of PSSQs Siloxane Resin Polymer Using Monomolecular Fluoro Silane

  • Bae, Jae Young;Mun, Han Jun;Kim, Tae Ho;Park, Hyun Ho
    • Elastomers and Composites
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    • v.55 no.2
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    • pp.103-107
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    • 2020
  • Herein, resin-formed polysilsesquioxanes (PSSQs) were synthesized using monomolecular fluoro silane as a precursor. The synthesized PSSQs exhibited anti-smudge performance and were used as coating liquid. Two structures were acquired by controlling the amount of the silane precursor and the K2CO3 catalyst; these materials were used to prepare the anti-smudge coating liquid solution. The synthesized product was analyzed by various methods such as nuclear magnetic resonance spectroscopy, X-ray diffraction analysis, gel permeation chromatography, and water contact angle measurement. The results confirmed that the as-synthesized PSSQs exhibited the ladder structure and had a molecular weight of 5,117 g/mol and water contact angle of 102.31°.

Investigation on formation mechanism of ZnO thin films deposited by pulsed laser deposition depending on plume-substrate angles (펄스 레이저 증착법에서 증착 각도 변화에 따른 ZnO 박막 형성 메카니즘)

  • Kim, Jae-Won;Kang, Hong-Seong;Lee, Sang-Yeol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07a
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    • pp.200-202
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    • 2004
  • ZnO thin films were grown at different plume-substrate angles by pulsed laser deposition(PLD). From the X-ray diffraction(XRD) result, all ZnO thin films were found to be well c-axis oriented and c-axis lattice constant approached the value of bulk ZnO as plume-substrate(P-S) angle decreased. The grain size of ZnO thin films measured by atomic force microscopy increased and the UV intensity of ZnO thin films investigated by photoluminescence increased as P-S angle decreased. It is found that the improvement of structural and optical properties mainly comes from the reduction of the flux of ablated species arriving on a substrate per a laser shot by tilting a substrate parallel to the plume propagation direction.

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Crystal Structure of Antiinflammatory Sulindac

  • Koo Chung Hoe;Kim Sang Hern;Shin Wanchul
    • Bulletin of the Korean Chemical Society
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    • v.6 no.4
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    • pp.222-224
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    • 1985
  • The crystal structure of sulindac, $C_{20}H_{17}Fo_3S$, one of the nonsteroid antiinflammatory agents, has been determined by the X-ray diffraction techniques using diffractometer data obtained by the $\varpi-2{\theta}$ scan technique with Cu $$K_{\alpha}$$ radiation from a crystal with space group symmetry Pbca and unit cell parameters a = 8.166(1), b = 18.291(8), c = 23.245(10) ${\AA}.$ The structure was solved by direct methods and refined by full-matrix least-squares to a final R = 0.11 for the 1153 observed reflections. The carboxyl group is nearly perpendicular to the indenyl ring as observed in indomethacin. The dihedral angle between the indenyl and phenyl rings is $35^{\circ}while$ the corresponding angle in indomethacin is $67^{\circ}.$ Crystal packing consists of a hydrogen bond and partial ring stacking between the indenyl rings.