• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2001년도 추계학술대회 논문집
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• pp.533-536
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• 2001

Single crystal cubic silicon carbide(3C-SiC) thin film were deposited on Si(100) substrate up to a thickness of 4.3 $\mu\textrm{m}$ by APCVD(atmospheric pressure chemical vapor deposition) method using hexamethyildisilane(HMDS) at 1350$^{\circ}C$. The HMDS flow rate was 0.5 sccm and the carrier gas flow rate was 2.5 slm. The HMDS flow rate was important to get a mirror-like. The growth rate of the 3C-SiC films was 4.3 $\mu\textrm{m}$/hr. The 3C-SiC epitaxical layers on Si(100) were characterized by XRD(X-ray diffraction), raman scattering and RHEED(reflection high-energy electron diffraction), respectively The 3C-SiC distinct phonons of TO(transverse optical) near 796 cm$\^$-1/ and LO(longitudinal optical) near 974${\pm}$1 cm$\^$-1/ were recorded by raman scattering measurement. The deposition films were identified as the single crystal 3C-SiC phase by XRD spectra(2$\theta$=41.5$^{\circ}$). Also, with increase of films thickness, RHEED patterns gradually changed from a spot pattern to a streak pattern

• Macromolecular Research
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• 제14권6호
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• pp.588-595
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• 2006

The morphology, structure and melting behaviour of cold-crystallized isotactic polystyrene (iPS) were studied by differential scanning calorimetry (DSC), wide angle X-ray diffraction (WAXD) and small angle X-ray scattering (SAXS). The polymer was found to crystallize according to the dual-lamellar stack model. The two populations of lamellae, along with a melting-recrystallization phenomenon, determined the appearance of multiple melting peaks in DSC traces. The annealing peak was attributed to the relaxation of a rigid amorphous phase, rather than to the melting of crystalline material.

• 한국진공학회지
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• 제2권2호
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• pp.171-180
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• 1993

X-선 광전자 분광법(XPD)을 이용하여 GaAs(110) 절개면의 결정구조를 이해하였다. 각분해 X-선 분광법으로 GaAs(110) 면의 내각준위 Ga 및 As 3d의 스펙트럼을 얻어, 이 내각 준위의 세기 비율(intensity ratio)의 방위각과 편각에 따른 변화를 SSC(Single Scattering Cluster) 모델에서 얻은 회절패턴으로 곡선분석(fitting)하여 절개면의 재구성 구조(reconstruction geometry)를 얻었다. 이 절개면의 재구성된 값은 다른 실험의 결과와 비슷하였다.

• Journal of Welding and Joining
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• 제33권1호
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• pp.30-34
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• 2015

Residual stresses are inherently introduced into the engineering components during manufacturing including rolling, forging, bending and welding processes. Excessive residual stresses are known to be detrimental to the proper integrity and performance of components. Neutron diffraction has become a well-established technique for the determination of residual stresses in welds. The deep penetration capability of neutrons into most metallic materials makes neutron diffraction a powerful tool for the residual stress measurements through the thickness of the weld specimen. Furthermore, the unique volume-averaged bulk characteristic of the scattering beam and mapping capability in three dimensions is suitable for the engineering purpose. In this presentation, the neutron diffraction measurements of the residual stresses will be introduced and measurement results will highlighted in thick weld plates.

• 한국재료학회지
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• 제14권5호
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• pp.348-352
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• 2004

The mechanical alloying (MA) effect in immiscible V-Cu system with positive heat of mixing was studied by not only the neutron and X-ray diffraction but also the analysis of DSC spectra. The total energy, ΔHt accumulated during MA for the mixture of $V_{50}$ $Cu_{50}$ / powders increased with milling time and approached the saturation value of 14 kJ/mol after 120 h of milling. It can be seen that the free energy difference between the amorphous phase and the pure V and Cu powders with an atomic ratio 5:5 is estimated to be 11 kJ/mol by Miedema et al. This is thermodynamically taken as one of the evidences for the amorphization. The structural changes of V-Cu MA powders were characterized by the X-ray diffraction and neutron diffraction. We take a full advantage of a negligibly small scattering length of the V atom in the neutron diffraction measurement. The neutron diffraction data definitely indicate that the amorphization proceeds gradually but incompletely even after 120 h of MA and bcc-Cu Bragg peaks appears after 60 h of MA.

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 1998년도 추계종합학술대회 논문집
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• pp.363-366
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• 1998

High frequency scattered fields by a double impedence wedge are computed. In the procedure of the computation, arbitrary impedence faces and wedge angles are considered. The diffraction coefficients for the single, double and triple diffraction mechanism are founded. The second-order and third-order diffracted fields are approximated via the extended spectral ray method and the modified Pauli-Clemmow method of the steepest descent. The maliuzhinets function which is very difficult to obtain accurate value is approximated by the Volakis's asymtotic expression. Numerical computations are performed for the various wedge angles and surface impedence values.

• Journal of the Optical Society of Korea
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• 제2권2호
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• pp.58-63
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• 1998

Cross-talk effects in high-density volume holographic interconnections are investigated using perturbative iteration method of the integral form of Maxwell's wave equation. In this method, the paraxial approximation and negligence of backward scattering introduced in conventional coupled mode theory is not assumed. Interaction geometries consisting of non-coplanar light waves and multiple index gratings are studied. Arbitrary light polarization is considered. Systematic analysis of cross-talk effects due to multiple index gratings is performed in increasing level of diffraction orders corresponding to successive iterations. Some numerical examples are given for first and third order diffraction.

• 한국세라믹학회지
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• 제40권6호
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• pp.513-518
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• 2003

La/sub 2/3-x/Li/sub 3x/□/sub 1/3-2x/TiO₃ compounds with x=0.13 and 0.12 were prepared by slow cooling (x=0.13) and rapid quenching (x=0.12) into the liquid nitrogen after sintering at 1350℃ for 6 h. Their crystal structure has been determined by Rietveld refinement of both the powder neutron and X-ray diffraction data. From neutron diffraction data, we found that the main phase was not tetragonal (P4/mmm), but trigonal (R3cH). The refinement of neutron diffraction for the slow cooled samples were in a good agreement with a new model; a mixture of trigonal (R3cH, 45.7 wt％), tetragonal (p4/mmm, 37.0 wt％), and Li/sub 0.57/Ti/sub 0.86/O₂(pbnm, 17.2 wt%), but the quenched sample was found not to contain tetragonal (p4/mmm). X-ray diffraction data couldn't be well fitted because of the Poor scattering factor of lithium ions and the similar reflection patterns among trigonal (R3cH), tetragonal (p4/mmm), and cubic (Pm3m). We also knew that one transport bottlenecks is destroyed by one La vacancy in the case of trigonal (R3cH).

• 한국인터넷방송통신학회논문지
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• 제22권5호
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• pp.123-128
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• 2022

정확한 모드전송선로 이론 (MTLT)을 적용하여 원추형 광 입사에서 공진 회절격자의 특성을 조사하였다. 원추형 구성에서 공진 회절과 관련된 모드 벡터가 전형적이 구조의 회절격자와 관련된 것보다 입사각에 따라 작게 변한다는 것을 보여주었다. 더욱이, 소멸하는 회절파가 공진 효과를 담당하는 누설 모드를 구동함에 따라, 원추형 장착은 기존 회절격자보다 더 큰 각도 허용 오차를 회절격자에 부여함을 보였다. 이에 기초하여, 수치 계산을 통하여 원추형 입사에서 발견된 스펙트럼을 사용하여, 원추형 및 클래식 구성에서 공진 회절격자의 각도-스펙트럼과 파장-스펙트럼 성능을 정량화하였다. 이러한 결과는 효율적이고 물리적으로 희소한 공진 회절격자를 요구하는 다양한 응용 분야에서 유용할 것이다.

• 한국자기학회지
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• 제20권4호
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• pp.160-166
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• 2010

엑스선 공명 자기산란은 엑스선 반사율과 회절의 원리를 이용하여 자기 다층박막 내 깊이 방향의 자화 모양 및 자기 나노 구조체 내의 자화 분포를 특정 원소별로 구할 수 있다. 여기서는 엑스선 공명 자기산란에 대한 간단한 설명과 이를 이용한 자성 다층박막 및 나노 구조체의 자기 구조와 자기 스위칭의 연구에 대하여 몇 가지 예를 들어 설명하려 한다.