• Title/Summary/Keyword: Differential thermal analysis

Search Result 676, Processing Time 0.025 seconds

Characteristic Studies of Plasma Treated unidirectional Hildegardia Populifolia Fabric

  • Prasad, C. Venkata;Lee, D.W.;Sudhakara, P.;Jagadeesh, D.;Kim, B.S.;Bae, S.I.;Song, J.I.
    • Composites Research
    • /
    • v.26 no.1
    • /
    • pp.54-59
    • /
    • 2013
  • This study deals with effect of plasma treatment on the properties of unidirectional ligno cellulosic fabric Hildegardia Populofolia (HDP) fabric. Thermal stability of the fabric was determined by differential scanning calorimetry (DSC) and Thermo gravimetric analysis (DSC). Morphological properties was analyzed by SEM analysis and found that the surface was rough upon plasma treatment which provides good interfacial adhesion with matrix during composite fabrication. Thermal stability and mechanical properties of the plasma treated fabric slightly increases compare to alkali and untreated fabric. It was observed that tensile properties of the fabric increases upon plasma treatment due to the formation of rough surface. SEM analysis indicates formation of rough surface on plasma treatment which helps in increasing the interfacial interaction between the matrix (hydrophobic) and fabric (hydrophilic).

Effect of Al2O3 on the Structure and Properties of Bioglass (생체 유리의 구조 및 물성에 미치는 Al2O3의 영향)

  • 노종남;황진명;김철영
    • Journal of the Korean Ceramic Society
    • /
    • v.26 no.6
    • /
    • pp.811-819
    • /
    • 1989
  • There have been many studies on the biological phenomena of Bioglasses, which nay be used as implant materials in human body. However, not many works on the Bioglass compositions have been reported. In the present study, the effect of Al2O3 substitution for SiO2 in Bioglass of Na2O-CaO-P2O5-SiO2 system on its structure and properties was examined. Infrared and Raman spectroscopic studies for the glass structural analysis, differential thermal analysis and X-ray diffraction analysis for crystallization of the glass were perfomed. Several physical properties, such as thermal expansion coefficient, softening point, microhardness and reaction phenomena, were also measured. The major crystalline phase, after heat treatment of the glasses, was Na2Ca2(SiO2)3 and the crystal was transformed into other phase with increased substitution of Al2O3. The added Al2O3 reduced non-bridging oxygen in glass structure and thermal expansion coefficient, but increased glass density, sofening point and microhardness. When the glasses are reacted in Tris-buffer solution, the substituted Al2O3 inhibited the formation of hydroxyapatite on the Bioglas surface, and no hydroxyapatite was formed for the sample which contained more than 6wt.% of Al2O3 even if they were reacted for 600 hours.

  • PDF

Studies on Transparently Crystallized Glass -On Li2O-Al2O3-SiO2 Composition- (투명 결정화 유리에 관한 연구 -Li2O-Al2O3-SiO2계 조성에 관하여-)

  • 박용완;김건은;연석주;조중희
    • Journal of the Korean Ceramic Society
    • /
    • v.26 no.3
    • /
    • pp.315-322
    • /
    • 1989
  • Li2O-Al2O3-SiO2 system glasses contained P2O5, TiO2 and ZrO2as the nucleating agents were melted and formed. The glass was subsequently heated first to nucleate and then to grow the crystals. At constant nucleating agent content the base glass compositions were varied and the influences of these variations on the crystallization behaviour were investigated. The study was made by measurement of thermal expansion coefficient, differential thermal analysis, X-ray diffraction analysis, scanning electron microscope observation and transmission measurement of crystallized glass specimen in visible region. It was shown that the content of crystalline phase decreased with increasing SiO2 content as well as decresing Li2O in the base glass compositions. As the result of X-ray diffrection analysis, the major crystal was $\beta$-quartz solid solution. The degree of crystallinity which was calculated using the noncrystalline scattering methods increased in S-shape with increasing heat treatment time. This change was similar to that in thermal expansion coefficient. The transmissions of 5mm thick samples were 80-90% in visible ray region.

  • PDF

Frequency characteristics and sensitivity analysis of a size-dependent laminated nanoshell

  • Dai, Zuocai;Jiang, Zhiyong;Zhang, Liang;Habibi, Mostafa
    • Advances in nano research
    • /
    • v.10 no.2
    • /
    • pp.175-189
    • /
    • 2021
  • In this article, frequency characteristics, and sensitivity analysis of a size-dependent laminated composite cylindrical nanoshell under bi-directional thermal loading using Nonlocal Strain-stress Gradient Theory (NSGT) are presented. The governing equations of the laminated composite cylindrical nanoshell in thermal environment are developed using Hamilton's principle. The thermodynamic equations of the laminated cylindrical nanoshell are obtained using First-order Shear Deformation Theory (FSDT) and Fourier-expansion based Generalized Differential Quadrature element Method (FGDQM) is implemented to solve these equations and obtain natural frequency and critical temperature of the presented model. The novelty of the current study is to consider the effects of bi-directional temperature loading and sensitivity parameter on the critical temperature and frequency characteristics of the laminated composite nanostructure. Apart from semi-numerical solution, a finite element model was presented using the finite element package to simulate the response of the laminated cylindrical shell. The results created from finite element simulation illustrates a close agreement with the semi-numerical method results. Finally, the influences of temperature difference, ply angle, length scale and nonlocal parameters on the critical temperature, sensitivity, and frequency of the laminated composite nanostructure are investigated, in details.

Effect by Change of Geometries and Material Properties for Flip-Chip (플립 칩의 기하학적 형상과 구성재료의 변화에 따른 효과)

  • Kwon, Yong-Su;Choi, Sung-Ryul
    • Journal of the Korean Society of Industry Convergence
    • /
    • v.3 no.1
    • /
    • pp.69-75
    • /
    • 2000
  • Multichip packages are comprised of dissimilar materials which expand at different rates on heating. The differential expansion must be accommodated by the various structural elements of the package. A types of heat exposures occur operation cycles. This study presents a finite element analysis simulation of flip-chip among multichip. The effects of geometries and material properties on the reliability were estimated during the analysis of temperature and thermal stress of flip-chip. From the results, it could be obtained that the more significant parameters to the reliability of flip-chip arc chip power cycle, heat convection and height of solder bump.

  • PDF

Effect of Al2O3 on Crystallization Behavior and Microstructure of Na2O-CaO-P2O5-SiO2 Glass-ceramic System

  • Mirhadi, Bahman;Mehdikhani, Behzad
    • Journal of the Korean Ceramic Society
    • /
    • v.49 no.2
    • /
    • pp.146-150
    • /
    • 2012
  • The effects of $Al_2O_3$ on the crystallization behavior of glass compositions in the $Na_2O$-CaO-$SiO_2$ system were investigated by differential thermal analysis (DTA), X-ray diffraction (XRD), and scanning electron microscopy (SEM). The effect of $Al_2O_3$ content on the mechanical properties, density, phase formation, and microstructures of $Na_2O$-CaO-$P_2O_5$-$SiO_2$ glass ceramics were studied. The thermal parameters of each glass were studied by DTA. The density of the glass ceramic samples was measured by Archimedes' method. It was found that the glass-ceramic containing 2.0 molar percent $Al_2O_3$ had desirable sintering behavior and reached an acceptable density. Phase investigation and micro-structural analysis were performed by XRD and SEM, respectively.

An Experimental Study on Combustion Behavior of Different Ranks of Coals and Their Blends (저등급탄과 혼탄의 연소거동에 관한 실험적 연구)

  • Moon, Cheoreon;Sung, Yonmo;Ahn, Seongyool;Kim, Taekyung;Choi, Gyungmin;Kim, Duckjool
    • 한국연소학회:학술대회논문집
    • /
    • 2012.04a
    • /
    • pp.205-208
    • /
    • 2012
  • In this study, the thermal behavior and combustion characteristics of different ranks of coals and their blends were investigated to obtain information necessary for the evaluation of the co-processing of blends with low-rank coals. Thermogravimetric analysis(TGA) and differential thermal analysis(DTA) were carried out at different temperature from ambient temperature to $800^{\circ}C$, and a laboratory-scale pulverized coal combustion burner was used with coal feeing rate of $1.04{\times}10^{-4}kg/s$.

  • PDF

Preparation of $BaTiO_3$ Powder by Coprecipitation Method (공심법에 의한 $BaTiO_3$ 분말제조)

  • Kim, Yoon-Ho;Lee, Joon;Han, Il-Ho
    • Journal of the Korean Ceramic Society
    • /
    • v.23 no.4
    • /
    • pp.11-16
    • /
    • 1986
  • $BaTiO_3$ ceramics powder was prepared by coprecipitation method either in oxalic acid solution or in potassium hydroxide solution. Thermal decomposition of coprecipitated $BaTiO(C_2O_4)_2$.$4H_2O$ powder in oxalic acid solution was investigated by means of Themogravimetry Differential Thermal Analysis and X-ray Diffraction Analysis. Low temperature decomposition of coprecipitated $BaTiO(C_2O_4)_2$.$4H_2O$ caused narrow particle size distribution whereas high temperature decomposition caused fairly wide particle size distribution by partial sintering. As the reaction time increased the average particle size of coprecipitated $BaTiO_3$ powder in KOH solution was increased. The most narrow paticle size distribution was obtained when the coprecipi-tates were ripened for 4hrs.

  • PDF

Comprehensive piezo-thermo-elastic analysis of a thick hollow spherical shell

  • Arefi, M.;Khoshgoftar, M.J.
    • Smart Structures and Systems
    • /
    • v.14 no.2
    • /
    • pp.225-246
    • /
    • 2014
  • The present paper develops piezo-thermo-elastic analysis of a thick spherical shell for generalized functionally graded piezoelectric material. The assumed structure is loaded under thermal, electrical and mechanical loads. The mechanical, thermal and electrical properties are graded along the radial direction based on a power function with three different non homogenous indexes. Primarily, the non homogenous heat transfer equation is solved by applying the general boundary conditions, individually. Substitution of stress, strain, electrical displacement and material properties in equilibrium and Maxwell equations present two non homogenous differential equation of order two. The main objective of the present study is to improve the relations between mechanical and electrical loads in hollow spherical shells especially for functionally graded piezoelectric materials. The obtained results can evaluate the effect of every non homogenous parameter on the mechanical and electrical components.

Axisymmetric Finite Element Analysis of Decomposing Polymeric Composites and Structures (열경화성 고분자 복합재 구조물의 축대칭 유한요소해석)

  • Lee, Seon-Pyo
    • 연구논문집
    • /
    • s.24
    • /
    • pp.81-96
    • /
    • 1994
  • To investigate failure mechanisms observed in carbon-phenolic thermal insulators, differential equations which govern the decomposition process in a deformable anisotropic porous solid are derived for three-dimensional axisymmetric constructions. The governing equations not only couple the material deformation with pore pressure, but also couple pressure and temperature, which means that heat convected by the pyrolysis gases is properly accounted for. Then the Bubnov-Galerkin finite element method is applied to these equations to transform them into a semidescrete finite element system. A thermal insulation liner in the cowl region under typical operating conditions is analyzed to find a mechanism for plylift. The results from the structural analysis show across-ply failure in the cowl zone. The mechanism for plylift is hypothesized as a sequential procedure : 1) the across-ply failure which is the precursor to plylift and 2) the local fiber buckling caused by generation of excessive in-plane compressive stress. To prevent plylift, the across-ply stress can be reduced by using appropriate material ply angles in cowl zone design.

  • PDF