• 제목/요약/키워드: Differential temperature control

검색결과 123건 처리시간 0.022초

Magnetic Characteristics of BaFe12-2xCoxTixO19 Particles Prepared by Sol-gel Synthesis (졸-겔 합성에 의한 BaFe12-2xCoxTixO19 미립자의 자기적 특성)

  • 최현승;정지형;박효열;김태옥
    • Journal of the Korean Ceramic Society
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    • 제40권1호
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    • pp.62-68
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    • 2003
  • Ba-ferrite particles added with Co and Ti, which were known well the additives for the control in coercivity, were synthesized by sol-gel method. In the range 90 to 120 minute reaction time, a stable sol solution which showed no change with temperature, pH, viscosity and aging time. After dried and heat treatment of sol solution, Ba-ferrite phase formed at $700^{\circ}C$ with Differential Thermal Analysis(DTA) and X-Ray Diffractometer(XRD) measurement. The crystallinity became to be better with increasing the temperature. It were showed by Scanning Electron Microscopy(SEM) that Ba-ferrite increased to particle sizes as increasing heating temperature and obtained of narrow particles size distribution. Also, magnetic characteristics of Ba-ferrite powders Co and Ti added were observed by a Vibrating Sample Magnetometer(VSM). Saturation magnetization$(M_s)$ was not much changed, however. the coercivity$(H_c)$dramatically dropped with addition of Co and Ti.

Optimization of Crystallization Condition for Transparent LAS Glass-ceramic Via Differential Thermal Analysis (DTA를 통한 LAS계 투명 결정화 유리의 결정화 조건 최적화)

  • Moon, Yun-Gon;Lim, Tae-Young;Lee, Mijai;Kim, Jin-Ho;Jeon, Dae-Woo;Hwang, Jonghee
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • 제29권2호
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    • pp.101-105
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    • 2016
  • The basic characteristics of glass are highly fragile and brittle consequences the ultimate purpose of glass manufacturing is to make a transparent glass with complex shape. In order to solve this problem, mechanical properties of glass can be increased by crystallization of its amorphous glass. However, glass-ceramics has become opaque through crystallization process due to the distracted interface of glass by precipitated particles. This study has been investigated thermal processing conditions of LAS transparent glass-ceramic by using DTA (differential thermal analysis), in order to control size of precipitated particle and then fabricate transparent glass-ceramic. DTA indicated that crystallization peak area was declined with increased nucleation temperature. Subsequently, we have been established optimum temperature for crystallization depending on the nucleation temperature. The transmission and thermal expansion were measured after crystallization, and the size of precipitated particle was identified in range of 20~100 nm by FE-SEM. In addition, by setting the optimized crystallization condition, with high transmission and low thermal expansion glass was synthesized through this experiment.

Curing Kinetics of the No-Flow Underfill Encapsulant

  • Jung, Hye-Wook;Han, Sang-Gyun;Kim, Min-Young;Kim, Won-Ho
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 한국마이크로전자및패키징학회 2001년도 추계 기술심포지움
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    • pp.134-137
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    • 2001
  • The cure kinetics of a cycloalipatic epoxy / anhydride / Co(II) system for a no-flow underfill encapsulant, has been studied by using a differential scanning calorimetry(DSC) under isothermal and dynamic conditions over the temperature range of $160^{\circ}C ~220^{\circ}C$. The kinetic analysis was carried out by fitting dynamic/isothermal heating experimental data to the kinetic expressions to determine the reaction parameters, such as order of reaction and reaction constants. Diffusion-controlled reaction has been observed as the cure conversion increases and successfully analyzed by incorporating the diffusion control term into the rate equation. The prediction of reaction rates by the model equation corresponded well to experimental data at all temperature.

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Dynamic characteristics of a CSTR with MMA polymerization

  • Ahn, Jong-Pil;Rhee, Hyun-Ku
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 1992년도 한국자동제어학술회의논문집(국제학술편); KOEX, Seoul; 19-21 Oct. 1992
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    • pp.100-105
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    • 1992
  • A mathematical model is developed for a CSTR in which free radical solution polymerization of methyl methacrylate(MMA) takes place. It turns out that five ordinary differential equations are to be treated simultaneously in order to predict the reactor performance. Although the reaction proceeds under the conditions of relatively low temperature and pressure, the system shows very complex bifurcation features due to the diffusion limitation (gel effect) and the temperature dependence of the kinetic parameters and physical properties. The effects of various system parameters on the reactor performance as well as on the polymer properties are investigated by using the bifurcation analysis. The application of the singularity theory enables us to divide the parameter space into several different regions, in each of which the system takes a unique steady state structure. Under certain circumstances, complex dynamic features such as HB points and limit cycles are observed and these should be taken into consideration in the reactor design.

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Analysis of Thermal Distribution and Compensation of Error for Spindle of Machining Center (공작기계 스핀들 부위의 열분포 분석 및 오차 보정)

  • Ko, H.S.;Park, K.H.;Seo, H.R.;Ha, J.S.
    • Proceedings of the KSME Conference
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    • 대한기계학회 2004년도 춘계학술대회
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    • pp.1352-1357
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    • 2004
  • Thermal error compensation has been developed for CNC (Computer Numerical Control) machining center with moving heat sources. The thermal error in CNC machining center has an effect on machining accuracy more than the geometric error does. Thus, temperature distributions of a spindle unit have been analyzed numerically by a Finite Differential Method and experimentally by an infrared (IR) camera in this study. A multiple variable method has been derived to estimate the thermal deformation of the machine origin stably and effectively after measuring deformation and temperature data. The experimental results for a vertical machining center have shown that the thermal errors of the machine origins were reduced more than 30% by the developed method.

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A Resistance Deviation-To-Time Interval Converter Based On Dual-Slope Integration

  • Shang, Zhi-Heng;Chung, Won-Sup;Son, Sang-Hee
    • Journal of IKEEE
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    • 제19권4호
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    • pp.479-485
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    • 2015
  • A resistance deviation-to-time interval converter based on dual-slope integration using second generation current conveyors (CCIIs) is designed for connecting resistive bridge sensors with a digital system. It consists of a differential integrator using CCIIs, a voltage comparator, and a digital control logic for controlling four analog switches. Experimental results exhibit that a conversion sensitivity amounts to $15.56{\mu}s/{\Omega}$ over the resistance deviation range of $0-200{\Omega}$ and its linearity error is less than ${\pm}0.02%$. Its temperature stability is less than $220ppm/^{\circ}C$ in the temperature range of $-25-85^{\circ}C$. Power dissipation of the converter is 60.2 mW.

An Experimental Study on the Freeze Drying Process for Poly γ Glutamic Acid (폴리감마글루탐산의 동결 건조 과정의 실험적 연구)

  • Kang, Jisu;Sim, Yeon-Ho;Byun, Si-Ye;Chang, Young Soo;Kang, Byung Ha
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • 제27권12호
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    • pp.645-651
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    • 2015
  • This paper presents an experimental study on the freeze drying process for poly ${\gamma}$ glutamic acid. The physical properties of poly ${\gamma}$ glutamic acid are measured during the freeze-drying process. The moisture contents of poly ${\gamma}$ glutamic acid according to the glass transient temperature are obtained by DSC (Differential Scanning Calorimetry) analysis. The end point of primary drying for the poly ${\gamma}$ glutamic acid with a thickness of 3 mm is obtained by measuring the thickness of the dried layer, the amount of moisture evaporation, the moisture content, and the pressure in the drying vacuum chamber during the freeze-drying process. By considering the variation in the glass transient temperature with respect to the moisture content of the material, a control schedule for the heating plate temperature is suggested during the secondary drying process.

A Study on the Meter-Out and Meter-In Speed Control Characteristics in Pneumatic Cushion Cylinders (공기압 쿠션 실린더의 미터아웃/미터인 속도제어 특성에 관한 연구)

  • Kim, Do-Tae
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • 제22권1호
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    • pp.1-7
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    • 2013
  • Pneumatic cylinders are widely used to actuators in automatic equipments because they are relatively inexpensive, simple to install and maintain, offer robust design and operation, are available in a wide range of standard sizes and design alternatives. This paper presents a comparative study among the dynamic characteristics of meter-out and meter-in speed control of pneumatic cushion cylinders with a relief valve type cushion mechanism. Because of the nonlinear differential equations and a requirement for simultaneous iterative solution in a mathematical model of a double acting pneumatic cushion cylinder, a computer simulation is carried out to investigate pressure, temperature, mass flow rate in cushion chamber and displacement and velocity time histories of piston under various operating conditions. It is found that the piston velocity and pressure response in meter-in speed control are more oscillatory than with meter-out those when pneumatic cushion cylinders are driven at a high-speed. In meter-out speed control, the effective area of the flow control valve is larger than that of meter-in, and the supply pressure has to be much higher than the pressure required to move the load because it has also to overcome the back pressure in cushion chamber.

Development of a multiplex qRT-PCR assay for detection of African swine fever virus, classical swine fever virus and porcine reproductive and respiratory syndrome virus

  • Chen, Yating;Shi, Kaichuang;Liu, Huixin;Yin, Yanwen;Zhao, Jing;Long, Feng;Lu, Wenjun;Si, Hongbin
    • Journal of Veterinary Science
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    • 제22권6호
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    • pp.87.1-87.12
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    • 2021
  • Background: African swine fever virus (ASFV), classical swine fever virus (CSFV), and porcine reproductive and respiratory syndrome virus (PRRSV) are still prevalent in many regions of China. Co-infections make it difficult to distinguish their clinical symptoms and pathological changes. Therefore, a rapid and specific method is needed for the differential detection of these pathogens. Objectives: The aim of this study was to develop a multiplex real-time quantitative reverse transcription polymerase chain reaction (multiplex qRT-PCR) for the simultaneous differential detection of ASFV, CSFV, and PRRSV. Methods: Three pairs of primers and TaqMan probes targeting the ASFV p72 gene, CSFV 5' untranslated region, and PRRSV ORF7 gene were designed. After optimizing the reaction conditions, including the annealing temperature, primer concentration, and probe concentration, multiplex qRT-PCR for simultaneous and differential detection of ASFV, CSFV, and PRRSV was developed. Subsequently, 1,143 clinical samples were detected to verify the practicality of the assay. Results: The multiplex qRT-PCR assay could specifically and simultaneously detect the ASFV, CSFV, and PRRSV with a detection limit of 1.78 × 100 copies for the ASFV, CSFV, and PRRSV, but could not amplify the other major porcine viruses, such as pseudorabies virus, porcine circovirus type 1 (PCV1), PCV2, PCV3, foot-and-mouth disease virus, porcine parvovirus, atypical porcine pestivirus, and Senecavirus A. The assay had good repeatability with coefficients of variation of intra- and inter-assay of less than 1.2%. Finally, the assay was used to detect 1,143 clinical samples to evaluate its practicality in the field. The positive rates of ASFV, CSFV, and PRRSV were 25.63%, 9.36%, and 17.50%, respectively. The co-infection rates of ASFV+CSFV, ASFV+PRRSV, CSFV+PRRSV, and ASFV+CSFV+PRRSV were 2.45%, 2.36%, 1.57%, and 0.17%, respectively. Conclusions: The multiplex qRT-PCR developed in this study could provide a rapid, sensitive, specific diagnostic tool for the simultaneous and differential detection of ASFV, CSFV, and PRRSV.

Analysis of various MPPT algorithms for PCS (태양광 발전시스템의 MPPT 알고리즘 분석)

  • Shim, Jae-Hwe;Yang, Seung-Dae;Jung, Seung-Hwan;Choi, Ju-Yeop;Choy, Ick;An, Jin-Ung;Lee, Dong-Ha
    • Journal of the Korean Solar Energy Society
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    • 제31권2호
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    • pp.16-21
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    • 2011
  • Since the maximum power operating point(MPOP) of PCS alters with changing atmospheric conditions temperature conditions shadow conditions it is important to operate for PCS to keep maximum power point tracking(MPPT) continuously. This paper presents the results of modeling PV system by PSIM simulator and investigates the influence on the PV system from aspect of power quality i.e. voltage drop. This paper investigates four MPPT algorithms; Perturbation & Observation(P&O) Improved P&O Incremental Conductance(Incond) Differential coefficient method simulated with irradiation temperature change and shadow conditions.