• 한국분말재료학회지
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• 제21권4호
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• pp.260-265
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• 2014

In this study, in order to increase surface ability of hardness and corrosion of magnesium alloy, anodizing and sealing with nano-diamond powder was conducted. A porous oxide layer on the magnesium alloy was successfully made at $85^{\circ}C$ through anodizing. It was found to be significantly more difficult to make a porous oxide layer in the magnesium alloy compared to an aluminum alloy. The oxide layer made below $73^{\circ}C$ by anodizing had no porous layer. The electrolyte used in this study is DOW 17 solution. The surface morphology of the magnesium oxide layer was investigated by a scanning electron microscope. The pores made by anodizing were sealed by water and aqueous nano-diamond powder respectively. The hardness and corrosion resistance of the magnesium alloy was increased by the anodizing and sealing treatment with nano-diamond powder.

• 한국표면공학회지
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• 제47권3호
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• pp.121-127
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• 2014

In this study, in order to improve corrosion resistance and wear resistance of aluminum, surface treatment was made by anodizing with oxalic acid solution and sealing with nano-diamond powder. Average size of nano-diamond powder was 30nm. Anodizing with oxalic acid made many pores in the aluminum oxide layer. Pore size and oxide thickness were investigated by scanning electron microscope (SEM). Pore size increased as temperature increased and voltage increased. It was possible to make oxide layer with pore diameter more than 50 nm. Oxide thickness increased as temperature and voltage and treatment time increased. Oxide layer with above $10{\mu}m$ thickness was made. Aluminum oxide layer with many pores was sealed by water with nano-diamond powder. Surface morphology was investigated by SEM. After sealing treatment with nano-diamond powder, corrosion resistance, wear resistance and hardness increased.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1309-1310
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• 2006

High-purity and super-hard nano-polycrystalline diamond has been successfully synthesized by direct conversion from high-purity graphite under static pressures above 15 GPa and temperatures above $2300^{\circ}C$. This paper describes research findings on the formation mechanism of nano-structure and on the contributing factor leading to high hardness.

• 한국분말재료학회지
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• 제21권2호
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• pp.114-118
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• 2014

In this study, an aluminum oxide layer for sealing treatment of nano-diamond powder was synthesized by anodizing under constant current. The produced pore size and oxide thickness were investigated using scanning electron microscopy. The pore size increased as the treatment time increased, current density increased, sulfuric acid concentration decreased, which is different from the results under constant voltage, due to a dissolution of the oxide layers. The oxide layer thickness by the anodizing increased as temperature, time, and current density increased. The results of this study can be applied to optimize the sealing treatment process of nano-diamond particles of 4-10 nm to enhance the resistances of corrosion and wear of the matrix.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2012년도 제43회 하계 정기 학술대회 초록집
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• pp.418-418
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• 2012

Synthesis of nanocrystalline diamond powder was investigated via a gas-to-particle scheme using the hot filament chemical vapor deposition. Effect of substrate surface seeding by nano diamond powder, and that of the electrical conductance of the substrate were studied. The substrate temperature, methane content in the precursor gas, filament-substrate distance and filament temperature were $670^{\circ}C$, 5% methane in hydrogen, 10 mm and $2400^{\circ}C$, respectively. The powder formation by gas-to-particle mechanism were greatly enhanced by the substrate seeding by the nano diamond powder. It was attributed to the removal of the electrostatic force between the substrate and the seeded nano diamond particle by the thermal electron shower from the hot filament, via the depolarization of the substrate surface or the attached diamond powder and subsequent levitation into the gas phase to serve as the gas-phase nucleation site. The powder formation was greatly favoured by the conducting substrate relative to the insulating substrate, which proved the actual effect of the electric static force in the powder formation.

• Journal of Advanced Marine Engineering and Technology
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• 제38권1호
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• pp.1-7
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• 2014

기본유체에 나노분말을 분산시킨 나노유체는 기본유체보다 높은 열전도도를 보인다. 이러한 특성으로 인해, 에너지 효율을 향상시키기 위한 대안으로서 나노유체가 주목받고 있으며, 고효율을 필요로 하는 열교환기의 작동유체로 적용하기 위한 많은 연구가 진행되고 있다. 본 연구에서는 상용 열교환기의 작동유체로서 많이 사용되고 있는 증류수, 에틸렌글리콜, 에틸알코올에 나노다이아몬드 분말을 적용한 나노유체의 열전도도를 측정하였다. 나노유체는 매트릭스 합성 분산법을 이용하여 제조하였으며, 나노다이아몬드의 혼합량은 0.1, 0.3, 0.5, 1vol%로 하였다. 측정결과 모든 기본유체 조건에서 나노유체의 열전도도가 증가하였으며, 특히 증류수에 분산된 1vol%의 나노유체에서 23%의 높은 열전도도 향상 경향을 보였다.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1148-1148
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• 2006

• Journal of Advanced Marine Engineering and Technology
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• 제38권9호
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• pp.1039-1044
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• 2014

가혹한 조건에서 작동하는 디젤엔진의 윤활성능을 향상시키기 위하여 많은 연구가 진행되고 있다. 본 연구에서는 특수윤활제로 사용되고 있는 나노다이아몬드를 포함한 윤활제를 디젤엔진에 적용하여 엔진성능에 미치는 영향을 분석하고자 한다. 매트릭스 합성분산법에 의하여 제조된 나노다이아몬드 윤활제를 농도별로 실험하여 기본윤활제와 비교하였다. 실험결과 마찰저감에 의한 효율의 향상과 일산화탄소, 스모크 등의 배기 저감의 효과를 확인하였다.

• 한국해양공학회지
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• 제23권6호
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• pp.99-104
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• 2009

PTFE has good mechanical and chemical stability at a wide range of temperatures and demonstrates a low friction coefficient value. PTFE is being used for self-lubricating parts in industry. But it shows a high wear rate. Thus, PTFE and nano-diamond powder were mixed into a composite and the wear properties of a PTFE coating layer on Al6061 was investigated. A ball-on-disk type of wear tester was used under a dry condition and different temperatures of oil. After the wear test, the wear track wasexamined by optical microscope. The PTFE-diamond showed the lowest friction coefficient (0.02) of all the lubricants in the experiments. The friction coefficient was shown to be directly related to the diamond powder in the PTFE coating. Adhesion estimations were performed by a scratch test, which is mainly used for coatings. The critical load between the coating and substrate was defined through analyses of the friction load, normal load curve, and acoustic emissions, along with optical microscope observations. The scratch test results showed that an import item (SWISS) gave the highest critical load values.

• 한국분말재료학회지
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• 제15권5호
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• pp.378-385
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• 2008

This article presents the successful consolidation of the mixed Co and Diamond powders for a drilling segment by the combined application of magnetic pulsed compaction (MPC) and subsequent sintering, and their properties were analyzed. Homogeneous hardness (Hv 220) and density (97%) of sintered bulks fabricated by MPC were obtained by the new technique, where higher pressure has been employed for short period of time than that of general process. A fine microstructure and homogeneous hardness in the consolidated bulk were observed without cracks. Relatively higher drilling speed of 9.61 cm/min and life time of 6.55 m were found to the MPCed specimens, whereas the value of the specimens fabricated by general process was 11.71 cm/min and 7.96 m, respectively. A substantial improvement of mechanical properties of segment was achieved through this study.