• 제목/요약/키워드: Diamond Analysis

검색결과 365건 처리시간 0.023초

Measurement of the Thermal Conductivity of a Polycrystalline Diamond Thin Film via Light Source Thermal Analysis

  • Kim, Hojun;Kim, Daeyoon;Lee, Nagyeong;Lee, Yurim;Kim, Kwangbae;Song, Ohsung
    • 한국재료학회지
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    • 제31권12호
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    • pp.665-671
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    • 2021
  • A 1.8 ㎛ thick polycrystalline diamond (PCD) thin film layer is prepared on a Si(100) substrate using hot-filament chemical vapor deposition. Thereafter, its thermal conductivity is measured using the conventional laser flash analysis (LFA) method, a LaserPIT-M2 instrument, and the newly proposed light source thermal analysis (LSTA) method. The LSTA method measures the thermal conductivity of the prepared PCD thin film layer using an ultraviolet (UV) lamp with a wavelength of 395 nm as the heat source and a thermocouple installed at a specific distance. In addition, the microstructure and quality of the prepared PCD thin films are evaluated using an optical microscope, a field emission scanning electron microscope, and a micro-Raman spectroscope. The LFA, LaserPIT-M2, and LSTA determine the thermal conductivities of the PCD thin films, which are 1.7, 1430, and 213.43 W/(m·K), respectively, indicating that the LFA method and LaserPIT-M2 are prone to errors. Considering the grain size of PCD, we conclude that the LSTA method is the most reliable one for determining the thermal conductivity of the fabricated PCD thin film layers. Therefore, the proposed LSTA method presents significant potential for the accurate and reliable measurement of the thermal conductivity of PCD thin films.

팔꿉관절 부위에 적용한 다이아몬드 테이핑이 정상인의 파악력 수준별 손목 폄근의 근활성도에 미치는 영향 (Effect of Diamond Taping Applied to the Elbow Joint on Wrist Extensor Muscle Activity in Healthy Subjects)

  • 황천종;김선엽
    • 한국전문물리치료학회지
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    • 제27권2호
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    • pp.118-125
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    • 2020
  • Background: Lateral epicondylitis (LE) is the most common chronic musculoskeletal pain condition of the upper extremities. LE is often related to forceful grip activities that require isometric contraction of the wrist extensors. A previous study evaluated the effect of the diamond taping technique on grip strength and pain; however, there has been no report on the change in the electromyography (EMG) findings of wrist extensors. Objects: The aim of this study was to investigate the effect of diamond taping technique, using a rigid tape, on the EMG activities of the extensor carpi radialis (ECR) during grip activities. Methods: Twenty-four healthy subjects (mean age = 21.50 ± 2.76 years) volunteered to participate in this study. The subjects were instructed to perform forceful grip activities with and without diamond-type taping on the origin area of the ECR. Grip strength tests were performed at 100%, 75%, 50%, and 25% for maximal isometric contraction force. EMG data were collected from the ECR. Repeated measure analysis of variance was used to analyze the effect of grip force and taping (with and without). Statistical significance levels were set at α = 0.05. Comparison of the results with and without taping at different grip force were analyzed using independent t-test. Statistical significance levels were set at α = 0.01. Results: Statistically significant association was observed between the taping application and forceful grip activity as revealed by the EMG data of the ECR (p < 0.05). EMG of the ECR significantly reduced for all muscle strength levels (p < 0.01) after taping. Conclusion: This study shows an impressive effect of the diamond taping technique, using rigid tape, on wrist extensors during grip activities. Decreasing muscle activity via this taping approach could be utilized to enhance pain-free grip force and reduce pain in patients with LE. Our study suggested that this taping technique could be considered as an effective management strategy of LE.

FIB milling을 이용한 고정밀 다이아몬드공구 제작과 공정에 관한 연구 (A study on the fabrication and processing of ultra-precision diamond tools using FIB milling)

  • 위은찬;정성택;김현정;송기형;최영재;이주형;백승엽
    • Design & Manufacturing
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    • 제14권2호
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    • pp.56-61
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    • 2020
  • Recently, research for machining next-generation micro semiconductor processes and micro patterns has been actively conducted. In particular, it is applied to various industrial fields depending on the machining method in the case of FIB (Focused ion beam) milling. In this study, intends to deal with FIB milling machining technology for ultra-precision diamond tool fabrication technology. Ultra-precision diamond tools require nano-scale precision, and FIB milling is a useful method for nano-scale precision machining. However, FIB milling has a problem of Gaussian characteristics that are differently formed according to the beam current due to the input of an ion beam source, and there are process conditions to be considered, such as a side clearance angle problem of a diamond tool that is differently formed according to the tilting angle. A series of process steps for fabrication a ultra-precision diamond tool were studied and analyzed for each process. It was confirmed that the effect on the fabrication process was large depending on the spot size of the beam and the current of the beam as a result of the experimental analysis.

What is the changing frequency of diamond burs?

  • Emir, Faruk;Ayyildiz, Simel;Sahin, Cem
    • The Journal of Advanced Prosthodontics
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    • 제10권2호
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    • pp.93-100
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    • 2018
  • PURPOSE. The purpose of this study was to determine the changing frequency of a diamond bur after multiple usages on 3 different surfaces. MATERIALS AND METHODS. Human premolar teeth (N = 26), disc shaped direct metal laser sintered CoCr (N = 3) and zirconia specimens (N = 3) were used in this study. Groups named basically as Group T for teeth, Group M for CoCr, and Group Z for zirconia. Round tapered black-band diamond bur was used. The specimens were randomly divided into three groups and placed with a special assembly onto the surveyor. 1, 5, and 10 preparation protocols were performed to the first, second, and third sub-groups, respectively. The subgroups were named according to preparation numbers (1, 5, 10). The mentioned bur of each group was then used at another horizontal preparation on a new tooth sample. The same procedure was used for CoCr and zirconia disc specimens. All of the bur surfaces were evaluated using roughness analysis. Then, horizontal tooth preparation surfaces were examined under both stereomicroscope and SEM. The depth maps of tooth surfaces were also obtained from digital stereomicroscopic images. The results were statistically analyzed using One-Way ANOVA, and the Tukey HSD post-hoc tests (${\alpha}=.05$). RESULTS. All of the groups were significantly different from the control group (P<.001). There was no significant difference between groups Z5 and Z10 (P=.928). Significant differences were found among groups T5, M5, and Z5 (P<.001). CONCLUSION. Diamond burs wear after multiple use and they should be changed after 5 teeth preparations at most. A diamond bur should not be used for teeth preparation after try-in procedures of metal or zirconia substructures.

인장 하중을 받는 무한 고체에 포함된 다수의 다이아몬드 형 함유체 문제 해석을 위한 체적 적분방정식법 (Volume Integral Equation Method for Problems Involving Multiple Diamond-Shaped Inclusions in an Infinite Solid under Uniaxial Tension)

  • 이정기
    • 대한기계학회논문집A
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    • 제36권1호
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    • pp.59-71
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    • 2012
  • 체적 적분방정식법(Volume Integral Equation Method)이라는 새로운 수치해석 방법을 이용하여, 서로 상호작용을 하는 등방성 또는 이방성 다이아몬드 형 함유체를 포함하는 등방성 무한고체가 정적 인장하중을 받을 때 무한고체 내부에 발생하는 응력분포 해석을 매우 효과적으로 수행하였다. 즉, 등방성 기지에 다수의 등방성 또는 이방성 다이아몬드 형 함유체의 중심이 1) 정사각형 배열 형태 또는 2) 정육각형 배열 형태로 포함되어 있는 경우에, 다양한 다이아몬드 형을 포함하는 원형 실린더 함유체의 체적비에 대하여, 중앙에 위치한 다이아몬드 형 함유체와 등방성 기지의 경계면에서의 인장응력 분포의 변화를 구체적으로 조사하였다. 또한, 체적 적분방정식법을 이용하여 구한 해의 정확도를 검증하기 위하여, 체적 적분방정식법을 이용한 해를 유한요소법을 이용한 해와 비교해 보았다.

Effects of dentin surface preparations on bonding of self-etching adhesives under simulated pulpal pressure

  • Chantima Siriporananon;Pisol Senawongse;Vanthana Sattabanasuk;Natchalee Srimaneekarn;Hidehiko Sano;Pipop Saikaew
    • Restorative Dentistry and Endodontics
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    • 제47권1호
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    • pp.4.1-4.13
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    • 2022
  • Objectives: This study evaluated the effects of different smear layer preparations on the dentin permeability and microtensile bond strength (µTBS) of 2 self-etching adhesives (Clearfil SE Bond [CSE] and Clearfil Tri-S Bond Universal [CTS]) under dynamic pulpal pressure. Materials and Methods: Human third molars were cut into crown segments. The dentin surfaces were prepared using 4 armamentaria: 600-grit SiC paper, coarse diamond burs, superfine diamond burs, and carbide burs. The pulp chamber of each crown segment was connected to a dynamic intra-pulpal pressure simulation apparatus, and the permeability test was done under a pressure of 15 cmH2O. The relative permeability (%P) was evaluated on the smear layer-covered and bonded dentin surfaces. The teeth were bonded to either of the adhesives under pulpal pressure simulation, and cut into sticks after 24 hours water storage for the µTBS test. The resin-dentin interface and nanoleakage observations were performed using a scanning electron microscope. Statistical comparisons were done using analysis of variance and post hoc tests. Results: Only the method of surface preparation had a significant effect on permeability (p < 0.05). The smear layers created by the carbide and superfine diamond burs yielded the lowest permeability. CSE demonstrated a higher µTBS, with these values in the superfine diamond and carbide bur groups being the highest. Microscopic evaluation of the resin-dentin interface revealed nanoleakage in the coarse diamond bur and SiC paper groups for both adhesives. Conclusions: Superfine diamond and carbide burs can be recommended for dentin preparation with the use of 2-step CSE.

CH3OH/H2O 가스의 기상활성법을 이용한 다이아몬드 박막성장 과정에서의 OES분석 (OES Analysis for Diamond Film Growth by Vapor Activation Method Using CH3OH/H2O Gas)

  • 이권재;고재귀;신재수
    • 한국재료학회지
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    • 제13권1호
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    • pp.31-35
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    • 2003
  • The intensity is measured as functions of both distance from filament to substrate and $CH_3$OH/($CH_3$OH+$H_2$O) ratio by OES(Optical Emission Spectroscopy) to investigate the effects of activation species such as $H_{\alpha}$, $H_{\beta}$, H$\Upsilon\;C_3$, CH on diamond film growth.$ H_{\alpha}$ increases as $CH_3$OH composition decreases, while CH increases as $CH_3$OH composition increases. The intensity of $H_{\alpha}$ decreases as the distance increases and that of CH increases as the distance increases. The intensities of other activation species of $H_{\beta}$, H$\Upsilon\;C_3$, do not vary as a function of measured position distance. It varies randomly. It means that various parameters for depositing diamond thin film can be explained by the intensity(density) change of activation species, as a function of the distance of the filament.

다이아몬드 터닝의 절삭력 측정용 tool holder를 이용한 미세절삭력 특성 연구 (Measurement of Cutting Force in Diamond Turning Process)

  • 정상화;김상석;도철진;홍권희;김건희
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2001년도 춘계학술대회 논문집
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    • pp.938-941
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    • 2001
  • A tool holder system has been designed and builted to measure cutting forces in diamond turning. This system design includes a 3-component piezo-electric tranducer. Initial experiments with tool holder system included verification of its predicted dynamic characteristics as well as a detailed study of cutting parameters. In this research, tool holder system is modeled by considering the element dividing, material properties, and boundary conditions using MSC/PATRAN. Mode and frequency analysis of structure is simulated by MSC/NASTRAN, for the purpose of developing the effective design. In addition, tool holder system is verified by vibration test using accelerometer. Many cutting experiments have been conducted on 6061-T6 aluminum. Tests have involved investigation of velocity effects, and the effects of depth and feedrate on tool force. Cutting velocity has been determined to have negligible effects between 4 and 21㎧.(6) Forces generally increase with increasing depth of cut. Increasing feedrate does not necessarily lead to higher forces. Results suggest that a sample model may not be sufficient to describe the forces produced in the diamond turning process.

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열처리온도에 따른 다이아몬드상 카본박막의 구조적 특성변화 (Structural Variation of Diamond-like Carbon Thin Film According to the Annealing Temperature)

  • 최원석;박문기;홍병유
    • 한국전기전자재료학회논문지
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    • 제19권8호
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    • pp.701-706
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    • 2006
  • In addition to its similarity to genuine diamond film, diamond-like carbon (DLC) film has many advantages, including its wide band gap and variable refractive index. In this study, DLC films were prepared by the RF PECVD (Plasma Enhanced Chemical Vapor Deposition) method on silicon substrates using methane $(CH_4)$ and hydrogen $(H_2)$ gas. We examined the effects of the post annealing temperature on the structural variation of the DLC films. The films were annealed at temperatures ranging from 300 to $900^{\circ}C$ in steps of $200^{\circ}C$ using RTA equipment in nitrogen ambient. The thickness of the film and interface between film and substrate were observed by surface profiler, field emission scanning electron microscopy (FESEM), high resolution transmission electron microscopy (HRTEM), respectively. Raman and X-ray photoelectron spectroscopy (XPS) analysis showed that DLC films were graphitized ($I_D/I_G$, G-peak position and $sp^2/sp^3$ increased) ratio at higher annealing temperature. The variation of surface as a function of annealing treatment was verified by a AFM and contact angle method.

Influence of neck width on the performance of ADAS device with diamond-shaped hole plates

  • Wu, Yingxiong;Lu, Jianfeng;Chen, Yun
    • Structural Engineering and Mechanics
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    • 제74권1호
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    • pp.19-32
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    • 2020
  • Metallic energy-dissipation dampers are widely used in structures. They are comprised of an added damping and stiffness (ADAS) device with many parallel, diamond-shaped hole plates, the neck width of which is an important parameter. However, no studies have analyzed the neck width's influence on the ADAS device's performance. This study aims to better understand that influence by conducting a pseudo-static test on ADAS, with three different neck widths, and performing finite element analysis (FEA) models. Based on the FEA results and mechanical theory, a design neck width range was proposed. The results showed that when the neck width was within the specified range, the diamond-shaped hole plate achieved an ideal yield state with minimal stress concentration, where the ADAS had an optimal energy dissipation performance and the brittle shear fracture on the neck was avoided. The theoretical values of the ADAS yield loads were in good agreement with the test values. While the theoretical value of the elastic stiffness was lower than the test value, the discrepancy could be reduced with the proposed modified coefficient.