• Title/Summary/Keyword: Dia Analysis

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X-ray diffraction analysis on sapphire wafers with surface treatments in chemical-mechanical polishing process (사파이어 웨이퍼 연마공정에서의 표면처리효과에 대한 X-선 회절분석)

  • 김근주;고재천
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.11 no.5
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    • pp.218-223
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    • 2001
  • The chemical-mechanical polishing process was carried out for 2"-dia. sapphire wafer grown by horizontalBridgman method on the urethane lapping pad with the silica sol. The polished wafer shows the full-width at halfmaximum of 200~400 arcsec in double-crystal X-ray diffraction, indicating that the slicing, grinding and lapping processes before the polishing process affected the crystalline structural property of the wafer surface by the mechanical residual stress. For the inclusion of surface treatments after chemical-mechanical polishing such as the thermal annealing at the temperature of $1,200^{\circ}C$for 4 hrs. and chemical etching, the crystalline quality was sigdicantly enhanced with the reduced full-width at half maximum up to 8.3 arcsec.arcsec.

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Bearing Capacity of Mid & Small dia Hellical Pile (중·소구경 헬리컬 파일의 지지력 특성)

  • Park, Jong-Bae;Park, Yong-Boo;Kwon, Young-Hwan
    • Land and Housing Review
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    • v.11 no.2
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    • pp.75-86
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    • 2020
  • As the urban regeneration project and the old housing maintenance project are actively progressing in Korea, small-scale building construction is being carried out in downtown areas. Small buildings in the downtown area are constructed on about 4 to 10 floors, and since they are carried out in small units in residential areas, it is difficult to enter large equipment to construct existing piles, and it is more vulnerable to complaints about noise and vibration. in this study, helical piles suitable for urban areas or small sites where it is difficult to enter large equipment, such as noise and vibration. Reliability analysis was performed on the results of the static load tests and dynamic load tests conducted at the LH site and the bearing capacity calculated by the hydrostatic method and the empirical formula (N value). As a result of comparing and analyzing the design formula and the results of static load test and dynamic load tests, the correlation between the design formula of the bored pile (Road bridge design standard) formula using N value and the design formula by the modified Davisson method frequently used by method commonly European helical file practitioners.

A Study for Acoustic Cues of Pyoung-An Do Dialect Using LPC (LPC를 이용한 평안방언의 음향지표에 관한 연구)

  • Song, Chul-Gyu;Lee, Myoung-Ho;Kim, Young-Bae
    • Journal of Biomedical Engineering Research
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    • v.13 no.3
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    • pp.195-200
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    • 1992
  • This paper deal with the acoustic cues of Pyoung-An Do dialect using linear prediction. Also, this paper descrbes a statistical comparison between standard tone speech data and Pyoung-An Do dia lects. The analysis done mainly focused on the distribution of formants and pitch periods accord to ac- cents variation. For the purpose of objective comparison, the experiments are performed by extracts for- mant LPC spectrum and pithch periods from average magnitude difference function waveforms. Summing up the results, In disyllable words (VCV pattern) , prepositioned vowels have longer phona lion time than postpositioned vowels and the intrin, iii phonation time is whore longer in the low vowels than in the high ones. The africative consonants show the mixed characteristics of the plosive and frlc ative consonants. The remarkable acoustic cues are the low frequency noise-like waves just before the 1st formants in the plosive consonants, the high frequency noise-like waves in the fricative consonants, and phonation time is not affected by the kinds of prepositioned or postpositioned vowels.

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Synthesis, Characterization, Thermal Stability and Conductivity of New Schiff Base Polymer Containing Sulfur and Oxygen Bridges (황과 산소를 함유하는 새로운 Schiff Base 고분자의 합성, 특성분석, 열적 안정성과 전도성)

  • Culhaoglu, Suleyman;Kaya, Ismet
    • Polymer(Korea)
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    • v.39 no.2
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    • pp.225-234
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    • 2015
  • In this study, we proposed to synthesize thermally stable, soluble and conjugated Schiff base polymer (SbP). For this reason, a specific molecule namely 4,4'-thiodiphenol which has sulfur and oxygen bridge in its structure was used to synthesize bi-functional monomers. Bi-functional amino and carbonyl monomers namely 4,4'-[thio-bis(4,1-phenyleneoxy)] dianiline (DIA) and 4,4'-[thiobis(4,1-phenyleneoxy)]dibenzaldehyde (DIB) were prepared from the elimination reaction of 4,4'-thiodiphenol with 4-iodonitrobenzene and 4-iodobenzaldehyde, respectively. The structures of products were confirmed by elemental analysis, FTIR, $^1H$ NMR and $^{13}C$ NMR techniques. The molecular weight distribution parameters of SbP were determined by size exclusion chromatography (SEC). The synthesized SbP was characterized by solubility tests, TG-DTA and DSC. Also, conductivity values of SbP and SbP-iodine complex were determined from their solid conductivity measurements. The conductivity measurements of doped and undoped SbP were carried out by Keithley 2400 electrometer at room temperature and atmospheric pressure, which were calculated via four-point probe technique. When iodine was used as a doping agent, the conductivity of SbP was observed to be increased. Optical band gap ($E_g$) of SbP was also calculated by using UV-Vis spectroscopy. It should be stressed that SbP was a semiconductor which had a potential in electronic and optoelectronic applications, with fairly low band gap. SbP was found to be thermally stable up to $300^{\circ}C$. The char of SbP was observed 29.86% at $1000^{\circ}C$.

Gamma/neutron classification with SiPM CLYC detectors using frequency-domain analysis for embedded real-time applications

  • Ivan Rene Morales;Maria Liz Crespo;Mladen Bogovac;Andres Cicuttin;Kalliopi Kanaki;Sergio Carrato
    • Nuclear Engineering and Technology
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    • v.56 no.2
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    • pp.745-752
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    • 2024
  • A method for gamma/neutron event classification based on frequency-domain analysis for mixed radiation environments is proposed. In contrast to the traditional charge comparison method for pulse-shape discrimination, which requires baseline removal and pulse alignment, our method does not need any preprocessing of the digitized data, apart from removing saturated traces in sporadic pile-up scenarios. It also features the identification of neutron events in the detector's full energy range with a single device, from thermal neutrons to fast neutrons, including low-energy pulses, and still provides a superior figure-of-merit for classification. The proposed frequency-domain analysis consists of computing the fast Fourier transform of a triggered trace and integrating it through a simplified version of the transform magnitude components that distinguish the neutron features from those of the gamma photons. Owing to this simplification, the proposed method may be easily ported to a real-time embedded deployment based on Field-Programmable Gate Arrays or Digital Signal Processors. We target an off-the-shelf detector based on a small CLYC (Cs2LiYCl6:Ce) crystal coupled to a silicon photomultiplier with an integrated bias and preamplifier, aiming at lightweight embedded mixed radiation monitors and dosimeter applications.

Mass Spectrometry Analysis of In Vitro Nitration of Carbonic Anhydrase II

  • Lee, Soo Jae;Kang, Jeong Won;Cho, Kyung Cho;Kabir, Mohammad Humayun;Kim, Byungjoo;Yim, Yong-Hyeon;Park, Hyoung Soon;Yi, Eugene C.;Kim, Kwang Pyo
    • Bulletin of the Korean Chemical Society
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    • v.35 no.3
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    • pp.709-714
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    • 2014
  • Protein tyrosine nitration is considered as an important indicator of nitrosative stresses and as one of the main factors for pathogenesis of inflammation and neuronal degeneration. In this study, we investigated various nitrosative modifications of bovine carbonic anhydrase II (CAII) through qualitative and semi-quantitative analysis using the combined strategy of Fourier transformation ion cyclotron resonance mass spectrometry (FT-ICR MS) and ion-trap tandem mass spectrometry (IT-MS/MS). FT-ICR MS and its spectra were used for the search of the pattern of nitrosative modifications. Identification of nitrosatively modified tyrosine sites were executed through IT-MS/MS. In addition, we also tried to infer the reason for the site-specific nitrosative modifications in CAII. In view of the above purpose, we have explored- i) the side chain accessibility, ii) the electrostatic environment originated from the acidic/basic amino acid residues neighboring to the nitrosatively modified site and iii) the existence of competing amino acid residues for nitration.

A RADIOGRAPHIC STUDY ON THE MUCOSAL CYST OF THE MAXILLARY SINUS (상악동 점액성 낭에 관한 방사선학적 연구)

  • Park Eung-Chun;Kim Jae-Duk
    • Journal of Korean Academy of Oral and Maxillofacial Radiology
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    • v.23 no.2
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    • pp.277-285
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    • 1993
  • This study was performed to evaluate the role of Waters' view and panoramic view for the interpretation of mucosal cyst of the maxillary sinus and to determine the radiographic features of that according to the sites and sizes. For this study, clinically 25 cases of mucosal cyst of the maxillary sinus were used, and experimentally with two dry skulls, rubber ball of 15mm in diameter for marked radiopacity, and two jelly balls of 8 and 20㎜ in diameter for the similar radiopacity to cyst were used. The 25 cases with 25 panoramic views and 15 Waters' views were first analyzed, and secondly, the radiographic features of artificial lesions attached to the each wall of the antrum on Waters' view and panoramic view were analyzed. The obtained results were as follows: At clinical analysis, 1. 4 cases of 13-14㎜, 4 cases of 15-19mm, 14 cases of 20-25㎜, 3 cases of over 30㎜ in dia- meter were found on panoramic views. And 24 cases of 25 cases showed no relationship with teeth, and only 1 case was associated with advanced periodontal disease 2. The majority of mucosal cysts appeared to arise the posterior portion of the floor of the sinus and were superimposed with the inominate line of zygoma and the horizontally linear image of hard palate on panoramic view. 3. Only 2 cases of 15 cases were identified on both films. At experimental analysis, 4. On Waters' view, the images of the artificial lesion of the anterior portion and midportion of the floor of the sinus were lessend in diameter compared with the real size. On panoramic views, the images of the lesion were more radiolucent with lessened diameter than images on Water' view. 5. The images of the lesion of the posterior wall and the posterior portion of the floor of sinus on panoramic view were well detected by the preeducated group but not or poorly detected by the non-preeducated observer group. 6. On Waters' view, both observer groups recognized that the cystic images of the posterior portion of the floor of the maxillary sinus were superimposed with the petrous portion of the skull.

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Study on the Texture Characteristics and Effects of Antioxidants on Saury (Cololabis saira) Nuggets (꽁치 너겟의 텍스처 특성 및 지방산패에 따른 품질특성 연구)

  • Kim, Gi-Ryoon;Kim, Hyun-Ah;Lee, Kyung-Hee
    • Journal of the Korean Society of Food Culture
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    • v.25 no.5
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    • pp.625-632
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    • 2010
  • The purpose of this study was to investigate the appropriate water content in high omega-3 fatty acid Saury nuggets for the desirable texture. The approach was made with adding water and onion at various levels (0~20%). The main ingredients of the nuggets included saury mince, mild pizza cheese, and hydrated textured soy protein concentrate. The formulated products were molded (dia. 4.5, thickness 1.5 cm, 20 g), lightly battered, and flash fried for 4 min. at $160^{\circ}C$, and then frozen until tested. The frozen nuggets were cooked at $165^{\circ}C$ and subjected to sensory evaluations, texture analysis, and water content analysis during warming (0~60 min), as well as assessments of acid, peroxide, and TBA values (during 10 days of storage at $24^{\circ}C$). In the sensory evaluation, preference for texture was highest in the nuggets made with a 15% onion level. The hardness of the nuggets increased with increasing onion level. Moisture content was highest in the nuggets made with a 20% water level. Changes in hardness during warming (0~60 min) of Saury nuggets containing various water and onion levels increased in nuggets made with the 20% water level. The acid, peroxide, and TBA values of the Saury nuggets made with herbs and oriental herbal extracts decreased up to 10 days of storage.

Study on the Texture Characteristics of High Omega-3 Fatty Acid Saury Nuggets ($\Omega$-3계 지방산이 다량 함유된 꽁치 너겟의 텍스쳐 특성에 관한 연구)

  • Kim, Gi-Ryoon;Lee, Kyung-Hee
    • Journal of the East Asian Society of Dietary Life
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    • v.18 no.4
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    • pp.569-575
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    • 2008
  • The principal objective of this study was to determine the appropriate water content for optimal texture in high omega-3 fatty acid saury nuggets. The approach adopted in this study essentially involved variations in water levels(0{\sim}25%$). The main ingredients of the nuggets included saury mince, mild pizza cheese and hydrated textured soy protein concentrate. The formulated products were molded(dia. 4.5, thickness 1.5 cm, 20 g), battered lightly, flash-fried far 4 min at $160^{\circ}C$ and frozen until they were tested. The frozen nuggets were cooked to $65^{\circ}C$, then subjected to sensory evaluation, texture analysis at 80% deformation, and expressible fluid tests. The moisture contents in the nugget batter and the cooked nuggets were determined. In our sensory evaluation, nugget texture was adjudged the best in the nuggets prepared with a 20% water level(S5). The hardness and chewiness in the nuggets were reduced with increases in the water level. However, when the nuggets contain more than 15% water(S4, S5, S6), we noted no significant differences in the hardness values. The difference in moisture content between the uncooked nugget bat or and the cooked nugget was most profound in the nugget prepared with a water level 25%(S6). The nugget prepared with a water level 25% was also the highest in expressible fluids, and was also highest in internal moisture content. The texture preference of nuggets was correlated positively with moistness(r=0.881) and moisture content(r=0.827), and correlated negatively with firmness(r=-0.870) and cohesiveness(r=-0.839), and these correlations were significant.

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A Numerical Study on the Impeller Meridional Curvature of High Pressure Multistage Pump (고압 다단 펌프의 임펠러 자오면 곡선에 대한 수치 해석적 연구)

  • Kim, Deok Su;Jean, Sang Gyu;Mamatov, Sanjar;Park, Warn Gyu
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.41 no.7
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    • pp.445-453
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    • 2017
  • This paper presents the hydraulic design an impeller and radial diffuser of a high-pressure multistage pump for reverse osmosis. The flow distribution and hydraulic performance for the meridional design of the impeller were analyzed numerically. Optimization was conducted based on the response surface method by varying the hub and shroud meridional curvatures, while maintaining the impeller outlet diameter, outlet width, and eye diameter constant. The analysis results of the head and efficiency with the variation in the impeller meridional profile showed that angle of the front shroud near the impeller outlet (${\varepsilon}Ds$) had the highest effect on head increase, while the hub inlet length ($d_{1i}$) and shroud curvature (Rds) had the highest effect on efficiency. From the meridional profile variation, an approximately 0.5% increase in efficiency was observed compared with the base model (case 25).