• Journal of the Korean Chemical Society
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• v.37 no.6
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• pp.585-589
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• 1993

A fluorimetric method for the determination of Fe(Ⅲ) using N,N'-oxalylbis(2-pyridyl-3'-sulphobenzoyl hydrazone)(OPSH) as a emission reagent has been developed. Determination has been performed by measuring the fluorescence intensity of Fe(Ⅲ) complex at 367 nm in aqueous solution (pH 3) with 290 nm excitation. There was a linear relationship between Fe(Ⅲ) concentration and fluorescence intensity over the range 2000∼10 ng/ml. The method has been applied to the determination of Fe(Ⅲ) in synthetic mixtures and tap water

• YAKHAK HOEJI
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• v.31 no.5
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• pp.315-321
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• 1987

A high performance liquid chromatographic method was developed for the determination of glycyrrhetinic acid contained in licorice powder. Glycyrrhetinic acid which is hydrolysate of glycyrrhizin extracted from licorice powder, was determined with good result by HPLC using 2-bromoacetyltriphenylene labeling reagent. The glycyrrhetinic acids were labeled with 2-bromoacetyltriphenylene in acetonitrile using 18-crown-6-ether and KOH as a catalyst. Derivatized glycyrrhetinic acids were separated from the extracted licorice powder on a reversed-phase column (chemopak $C_{18}$) using 100% acetonitrile as a mobile phase and monitored by an UV-detector at 268nm. Linearity of calibration curve was obtained between 5 ng and 20 ng, and the lower limit of detection was 2 ng. The recovery of glycyrrhetinic acid to licorice powder was about 99.3%. This method was sensitive, reliable and useful for, determination of glycyrrhetinic acid.

• Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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• v.11 no.2
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• pp.17-26
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• 1993

This study aims to develop an effective model of the optimum route determination by using digital terrain model. So in this study I select testing areas and analyse comparing the usual method with the digital terrain model method. And then I present one of the optimum route determination models by analysing an anticipated view and other roads according to the development plan. In usual method, the selected area was analysed by using panoramic terrestrial and aerial photograph. But in this study I represent the present terrain by using digital terrain materials which was acquired by a check form map of the selected area, and predict the route line according to the view points by using basic development plan. As a result of using the digital terrain model method in the optimum route determination with terrestrial photograph, it is possible to explain the terrain in detail when the present conditions terrain is analysed. As we can anticipated many sided road in large scale development plan with digital terrain materials which was used in analysing the present terrain, it is possible to lead to more effective route planning, landers planning and the optimum road determination than the usual method in the basic plan.

• The Journal of the Acoustical Society of Korea
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• v.14 no.6
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• pp.27-31
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• 1995

In this paper, the determination method of available bandwidth for automation of the split-spectrum processing(SSP) has been studied. The SSP is used for the visibility enhancement of the ultrasonic signal with grain noise. Even though the SSP has proved useful in signal-to-noise ratio enhancement, its application and automation have been limited due to ambiguity in the determination of available bandwidth. Until recently, it is the usual practice to optimize the available bandwidth by trial and error. The spectral histogram is the statistical distribution of the spectral windows that is selected by the minimization algorithm with the whole band of the spectrum of the received ultrasonic signal. Since the available bandwidth can be determined adaptively using spectral histogram, this method can be used for automation of the SSP. In order to evaluate the determination technique of the available bandwidth using spectral histogram, this method is applied to experimental ultrasonic data. The experimental results show that the spectral histogram is an efficient method for determination of the available bandwidth and automation of the SSP.

• The Journal of Korean Institute of Communications and Information Sciences
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• v.40 no.1
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• pp.165-170
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• 2015

The topic of this paper is the advanced absolute altitude determination for 3-D positioning using barometric altimeter and the reference station. Barometric altimeter does not provide absolute altitude because atmosphere pressure always varies over the time and geographical location. Also, since Global Navigation Satellites system such as GPS, GLONASS has geometric error, the altitude information is not available. It is the reason why we suggested the new method to improve the altitude accuracy. This paper shows 3-D positioning algorithm using absolute altitude determination method and evaluates the algorithm by real field tests. We used an accurate altitude from RTK system in Seoul as a reference data and acquired the differential value of pressure data between a reference station and a mobile station equipped in low cost barometric altimeter. In addition, the performance and advantage of the proposed method was evaluated by 3-D experiment analysis of PNS and CNS. We expect that the proposed method can expand 2-D positioning system 3-D position determination system simply and this 3-D position determination technique can be very useful for the workers in the field of fire-fighting and construction.

• Journal of Korean society of Dental Hygiene
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• v.21 no.4
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• pp.481-489
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• 2021

Objectives: This study was conducted to understand the effect of learners' self-determination on class participation, focusing on the feedback type of educators. Methods: A survey was conducted from May 1 to May 31 2021 on dental hygiene students, and a total of 151 valid responses were analyzed. The questionnaire consisted of general characteristics, self-determination, class participation, and educator's feedback type. The analysis method used correlation analysis and hierarchical regression analysis. Results: In relation to self-determination, class participation, and feedback type of educators, self-determination was positive feedback (r=0.338, p<0.01), class participation was corrective feedback (r=0.418, p<0.01), and positive feedback was correction (r=0.742, p<0.01). As a result of the mediating effect of the educator's feedback type in the relationship between self-determination and class participation, it was found to be significant by partially mediating positive and corrective feedback. Conclusions: It was found that the right to self-determination influences class participation based on positive feedback and corrective feedback of educators. It relates to efforts to strengthen learners' self-determination and provide appropriate types of feedback from educators.

• Korean Journal of Veterinary Service
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• v.18 no.3
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• pp.13-28
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• 1995

This study was carried out to explore the most sensitive and useful method for simultaneous determination of five sulfa drugs(sulfamethazine, sulfamerazine, sulfamonomethoxine, sulfadimethoxine, sulfaquinoxaline) in livestock productions(pork muscle, bovine muscle, chicken muscle, milk ) by HPLC with UV detector and reverse phase column. The results obtained were as follows：1. For mobile phase acetonitrile-0.01M ammonium acetate (23：77) showed more applicable sensitivity and retention times than acetonitrile-1% acetic acid(23：77). Thus acetonitrile-0.01M ammonium acetate(23：77) selected and applied to the modification test, from which it was found pH 6.75 was the most adequate. 2. Optimal wavelength of UV for SMT(sulfamethazine), SMR(sulfamerazine), SMM(sulfamonomethoxine), SD(sulfadimethoxine), and SQ(sulfaquinoxaline) were 266, 266, 265, 269 and 250nm, respectively, and that for simultaneous application it was 263nm. 3. The average recovery rate by extractant(chloroform, dichloromethane, chlorform+dich-loromethane) in the classic method was not significantly different(p>0.05) but that by chloroform higher than the others. Thus chloroform was found to be adequate as extractant in this classic method. 4. The average recovery rate was 86.5% by the MSPD(matrix solid phase disperse) method, which was significantly higher than that by the classic method(p<0.05). Also the recovery rates by method were significantly different(p<0.05) in accordance with sample and type of drug. The MSPD method was much superior to classic method on clean-up.

• Journal of the Korean Chemical Society
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• v.36 no.1
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• pp.95-99
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• 1992

A spectrophotometric method for the determination of copper using N,N'-Oxalylbis(salicylaldehyde hydrazone) as a chromogenic reagent has been developed. Determination has been performed by measuring the absorbances of the copper complexes in solutions containing 60% dimethylformamide (pH 2) at 422 nm. The method allows the determination of 0.4${\sim}$1.8 ${\mu}$g/ml of copper and has been applied to its determination in synthetic mixtures and alloy samples.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 1998.03a
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• pp.35-39
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• 1998

Determination of effective EDM parameters is significant to increase productivity. However, With the complexity of EDM phenomena, a universal selection method of EDM parameters has not been established yet. Moreover, No attempt has been tried before to suggest a logical method in determining essential machining parameters for effective electrical discharge machining. Peak current, one of the most significant factors in EDM, is proportional to EDM area. This paper presents a method that can be Z-map modeling from CMM data, and calculate EDM area using Z-map.

• Journal of Industrial Technology
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• v.12
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• pp.69-76
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• 1992

An attempt has been made to determination the NC milling machine's tool-path through the adaptive parabolic interpolation method & the adaptive linear-parabolic interpolation method in consideration of the economical machining time. The algorithms for the above-mentioned interpolation methods have been designed and the numerical experiments for these methods have been conducted with the existing adaptive linear interpolation methods for comparision.