• 제목/요약/키워드: Design of mixture experiments

검색결과 125건 처리시간 0.031초

실험계획법에 의한 $CF_4/O_2$ 플라즈마 에칭공정의 최적화에 관한 연구 (Experimental Analysis and Optimization of Experimental Analysis and Optimization of $CF_4/O_2$ Plasma Etching Process Plasma Etching Process)

  • 최만성;김광선
    • 반도체디스플레이기술학회지
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    • 제8권4호
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    • pp.1-5
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    • 2009
  • This investigation is applied Taguchi method and the analysis of variance(ANOVA) to the reactive ion etching(RIE) characteristics of $SiO_2$ film coated on a wafer with Experimental Analysis and Optimization of $CF_4/O_2$ Plasma Etching Process mixture. Plans of experiments via nine experimental runs are based on the orthogonal arrays. A $L_9$ orthogonal array was selected with factors and three levels. The three factors included etching time, RF power, gas mixture ratio. The etching rate of the film were measured as a function of those factors. In this study, the etching thickness mean and uniformity of thickness of the RIE are adopted as the quality targets of the RIE etching process. The partial factorial design of the Taguchi method provides an economical and systematic method for determining the applicable process parameters. The RIE are found to be the most significant factors in both the thickness mean and the uniformity of thickness for a RIE etching process.

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수소 동위원소 분리를 위한 77 K 극저온 파과 곡선 측정 시스템 제작 (Investigation of Cryogenic Breakthrough Curve Measurement System at 77 K for Hydrogen Isotopologue Separation)

  • 김수환;오현철
    • 한국재료학회지
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    • 제32권1호
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    • pp.36-43
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    • 2022
  • Breakthrough analysis has widely been explored for the dynamic separation of gaseous mixtures in porous materials. In general, breakthrough experiments measure the components of a flowing gas when a gaseous mixture is injected into a column filled with an adsorbent material. In this paper, we report on the design and fabrication of a breakthrough curve measurement device to study the dynamic adsorptive separation of hydrogen isotopologues in porous materials. Using the designed system, an experiment was conducted involving a 1:1 mixture of hydrogen and deuterium passed through a column filled with zeolite 13X (1 g). At room temperature, both hydrogen and deuterium were adsorbed in negligible amounts; however, at a temperature of 77 K, deuterium was preferentially adsorbed over hydrogen. The selectivity was different from that in the existing literature due to the different sample shapes, measurement methods, and column structures, but was at a similar level to that of cryogenic distillation (1.5).

Flowability and mechanical characteristics of self-consolidating steel fiber reinforced ultra-high performance concrete

  • Moon, Jiho;Youm, Kwang Soo;Lee, Jong-Sub;Yun, Tae Sup
    • Steel and Composite Structures
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    • 제43권3호
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    • pp.389-401
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    • 2022
  • This study investigated the flowability and mechanical properties of cost-effective steel fiber reinforced ultra-high performance concrete (UHPC) by using locally available materials for field-cast application. To examine the effect of mixture constituents, five mixtures with different fractions of silica fume, silica powder, ground granulated blast furnace slag (GGBS), silica sand, and crushed natural sand were proportionally prepared. Comprehensive experiments for different mixture designs were conducted to evaluate the fresh- and hardened-state properties of self-consolidating UHPC. The results showed that the proposed UHPC had similar mechanical properties compared with conventional UHPC while the flow retention over time was enhanced so that the field-cast application seemed appropriately cost-effective. The self-consolidating UHPC with high flowability and low viscosity takes less total mixing time than conventional UHPC up to 6.7 times. The X-ray computed tomographic imaging was performed to investigate the steel fiber distribution inside the UHPC by visualizing the spatial distribution of steel fibers well. Finally, the tensile stress-strain curve for the proposed UHPC was proposed for the implementation to the structural analysis and design.

Bailey Method를 이용한 아스팔트 혼합물 최적배합설계 평가 (Evaluation of Mix Design for Asphalt Mixtures by Bailey Method)

  • 이동항;이관호
    • 한국산학기술학회논문지
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    • 제13권10호
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    • pp.4832-4836
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    • 2012
  • 일반적으로 아스팔트 혼합물 배합설계는 많은 시간과 실험이 필요하다. 또한, 정밀한 배합설계 결과는 실험하는 사람의 숙련도와 밀접한 상관관계가 있다. 이러한 문제점을 해결하기 위하여 Bailey는 아스팔트 혼합물용 골재입도에 대한 연구를 통해 골재입도곡선에서 특정한 크기의 골재의 입도 및 통과중량비가 중요함을 제시하였다. 본 연구에서는 Bailey가 제안한 방법을 이용하여 19mm 밀입도 아스팔트 혼합물 및 미연방도로국의 배수성포장(PA 20mm) 혼합물에 대한 배합설계를 시행하였다. Bailey 방법을 이용한 아스팔트 혼합물용 골재입도 결정방법은 기존에 시행착오를 통합 배합설계방법에 비해 좀더 짧은 시간에 최적배합설계를 수행할 수 있음을 확인하였다. 19mm 밀입도 아스팔트 혼합물의 CA, $FA_c$, $FA_f$는 0.724, 0.440 및 0.455로 기준값을 만족하였다. PA 20mm 아스팔트 혼합물의 계산된 CA, $FA_c$, $FA_f$는 0.646, 0.476 및 0.450으로 기준값을 만족하였다.

Nano-engineered concrete using recycled aggregates and nano-silica: Taguchi approach

  • Prusty, Rajeswari;Mukharjee, Bibhuti B.;Barai, Sudhirkumar V.
    • Advances in concrete construction
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    • 제3권4호
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    • pp.253-268
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    • 2015
  • This paper investigates the influence of various mix design parameters on the characteristics of concrete containing recycled coarse aggregates and Nano-Silica using Taguchi method. The present study adopts Water-cement ratio, Recycled Coarse Aggregate (%), Maximum cement content and Nano-Silica (%) as factors with each one having three different levels. Using the above mentioned control parameters with levels an Orthogonal Array (OA) matrix experiments of L9 (34) has selected and nine number of concrete mixes has been prepared. Compressive Strength, Split Tensile Strength, Flexural Tensile Strength, Modulus of Elasticity and Non-Destructive parameters are selected as responses. Experimental results are analyzed and the optimum level for each response is predicted. Analysis of 28 days CS depicts that NS (%) is the most significant factor among all factors. Analysis of the tensile strength results indicates that the effect of control factor W/C ratio is ranked one and then NS (%) is ranked two which suggests that W/C ratio and NS (%) have more influence as compared to other two factors. However, the factor that affects the modulus of elasticity most is found to be RCA (%). Finally, validation experiments have been carried out with the optimal mixture of concrete with Nano-Silica for the desired engineering properties of recycled aggregate concrete. Moreover, the comparative study of the predicted and experimental results concludes that errors between both experimental and predicted values are within the permissible limits. This present study highlights the application of Taguchi method as an efficient tool in determining the effects of constituent materials in mix proportioning of concrete.

Breakdown characteristics of SF6 and Imitation Air in Temperature Decline

  • Lim, Chang-Ho;Choi, Eun-Hyeok;Kim, Do-Seok;Kim, Young-Su;Park, Won-Zoo;Lee, Kwang-Sik
    • 조명전기설비학회논문지
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    • 제21권4호
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    • pp.115-121
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    • 2007
  • This paper describes experiments of the breakdown characteristics by temperature change of $SF_6$ gas and Imitation Air(I-Air) in model GIS(Gas Insulated Switchgear). From the results of the experiments, the breakdown characteristics classify the vapor stage of $SF_6$ according to Paschen's law, in which the stage of coexistence for gas & liquid of the voltage value increases. This results in large deviation and the breakdown of the voltage(VB) low stage as the interior of the chamber is filled with a mixture of $SF_6$ that is not liquefacted and remaining air that can not be ventilated. The ability of $SF_6$ liquid($LSF_6$) insulation is higher than high-pressurize $SF_6$ gas. The VB of the I-Air decreases as the temperature drops and the VB also drops. It is considered that the results of this paper are fundamental data for the electric insulation design of superconductor and cryogenic equipment that will be studied and developed in the future.

Wet Air Oxidation Pretreatment of Mixed Lignocellulosic Biomass to Enhance Enzymatic Convertibility

  • Sharma, A.;Ghosh, A.;Pandey, R.A.;Mudliar, S.N.
    • Korean Chemical Engineering Research
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    • 제53권2호
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    • pp.216-223
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    • 2015
  • The present work explores the potential of wet air oxidation (WAO) for pretreatment of mixed lignocellulosic biomass to enhance enzymatic convertibility. Rice husk and wheat straw mixture (1:1 mass ratio) was used as a model mixed lignocellulosic biomass. Post-WAO treatment, cellulose recovery in the solid fraction was in the range of 86% to 99%, accompanied by a significant increase in enzymatic hydrolysis of cellulose present in the solid fraction. The highest enzymatic conversion efficiency, 63% (by weight), was achieved for the mixed biomass pretreated at $195^{\circ}C$, 5 bar, 10 minutes compared to only 19% in the untreated biomass. The pretreatment under the aforesaid condition also facilitated 52% lignin removal and 67% hemicellulose solubilization. A statistical design of experiments on WAO process conditions was conducted to understand the effect of process parameters on pretreatment, and the predicted responses were found to be in close agreement with the experimental data. Enzymatic hydrolysis experiments with WAO liquid fraction as diluent showed favorable results with sugar enhancement up to $10.4gL^{-1}$.

일회용 각종 송혈관의 관류압차에 대한 비교실험 (An Experiments Analysis of Comparison of Flow Gradients Across Disposable Arterial Perfusion Cannulas)

  • 김요한;김형묵
    • Journal of Chest Surgery
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    • 제19권1호
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    • pp.18-24
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    • 1986
  • The mean perfusion pressure produced by 20 different design and size of disposable aortic perfusion cannulas [size range: 18F to 20F] at flow rates of 1 to 5 L/min was compared. A roller pump with perfusion tubing 10mm in inner diameter was used with a mixture of 0.9% normal saline and 100% glycerin [mixing ratio of 6.72:13.28] to make the viscosity as normal blood in 20oC as the test solution. Line pressure in these cannulas at a flow rate of 3L/min ranged from 13.2$\pm$4.47 to 157$\pm$1 34 mmHg in a case of absence of resistance, and from 11.4$\pm$1.14 to 227.2$\pm$4.47 mmHg in a case of presence of resistances 14 cannulas had gradients of less than 100Hg at a flow rate of 3L/min and 9 cannulas less than 100mmHg at 4L/min. The following results were obtained from this experimental study: .1] A wide range of line pressure was observed in disposable aortic perfusion cannulas currently in clinical use; 2] Some cannulas currently used for cardiopulmonary bypass in adults generated excessive line pressure; 3] Both the material and design affect function, with some designs safer than others. Cardiac surgeons should base the choice of aortic perfusion cannula on the best performance and safest design available to avoid cannula-related problems during operation.

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실험계획법을 이용한 아크릴 점착제의 점착력 최적화 (Optimization of Peel Adhesion of Acrylic Pressure Sensitive Adhesive using Design of Experiments)

  • 이영상;하진국;이의수
    • 접착 및 계면
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    • 제9권1호
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    • pp.22-27
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    • 2008
  • 아크릴 점착제의 점착력을 목표 수준으로 향상시키기 위해 실험계획법을 이용하여, 2-ethyl hexyl acrylate (2-EHA), ethyl acrylate (EA), metha acrylic acid (MAA), acryl amide (AAm)를 라디칼 용액 중합하여 점착력을 측정하였다. 실험계획법은 반응표면분석법의 하나인 혼합물 설계를 이용하여 특수 3차 모형으로 분석하였으며, 그 적용은 상용프로그램인 MINITAB을 사용하였다. 수립된 실험계획에 의해 실험하고 분석한 결과, 목표하는 점착력을 얻기 위한 단량체 조성은 2-EHA (0.8861), EA (0.0639), MAA (0.03), AAm (0.02)로 나타났으며, 그 회귀분석 식은 다음과 같았다. $$y=54.8816x_1+80.7067x_2-44.4700x_3-99.0288x_1x_2+60.7706x_1x_3-441.030x_2x_3+974.341x_1x_2x_3$$.

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혼합물 실험계획법을 이용한 유색 EPDM의 첨가제 배합비에 따른 기계적 특성 분석 (Analysis of Mechanical Properties of Colored EPDM Based on Additive Mixing Ratio Using Mixture Design of Experimental Method)

  • 박윤아;전의식;김영신;이현승
    • 한국기계가공학회지
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    • 제21권8호
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    • pp.79-86
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    • 2022
  • With the recent increase in the demand for electric vehicles, it is necessary to identify the high current safety of automobile parts. Among the automobile parts, the EPDM parts required colored parts from the existing black; therefore, it was necessary to change the basic filler from carbon black to silica. The rubber used in automobile parts is flexible and exhibits basic characteristics of high strength and elongation. However, as the filler is changed to silica, its physical properties, such as tensile strength and elongation, are lower than those of the existing carbon black base. Therefore, it is necessary to evaluate the mechanical properties with the addition of the EPDM compound using silica as a base without degrading the physical properties of EPDM. In this study, an experiment based on the additive content was performed using the mixture experimental planning method to analyze the mechanical properties according to the additive type and mixing ratio of silica-based EPDM. The mixing ratio of the four additives was set using a simplex lattice design, and the tensile strength, elongation, modulus 300%, and permanent compression reduction rate were analyzed for mechanical characteristics, and rheometer experiments were performed for vulcanization characteristics. Through statistical analysis of the measured data, the main effects and interactions of the EPDM-blended rubber additives were analyzed. These results can be used to derive a mixing ratio of additives that satisfies the required characteristics of the EPDM compound.