• Title/Summary/Keyword: Delamination

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Evaluation of Brinell Hardness of Coated Surface Using Finite Element Analysis: Part 3 - Application to Multilayer Coatings (유한요소해석에 의한 코팅면의 브리넬 경도 평가: 제3보 - 다층 코팅에 적용)

  • Park, TaeJo;Kang, JeongGuk
    • Tribology and Lubricants
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    • v.37 no.6
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    • pp.240-245
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    • 2021
  • Ceramic coatings with high hardness and excellent chemical stability have been successfully applied to various machine elements, tools, and implants. However, in the case of monolayer coating on soft substrates, a high-stress concentration at the interface between the coating and the substrate causes delamination of the coating layer. Recently, to overcome this problem, multilayer coatings with a metal layer with a low modulus of elasticity added between the ceramic and the substrate have been widely applied. This study presents the third part of a recent study and focuses on the effect of the number of coating layers on the Brinell hardness of multilayered coating with TiN/Ti, following the two previous studies on a new Brinell hardness test method for a coated surface and on the influence of substrate and coating thickness. Indentation analyses are performed using finite element analysis software, von Mises stress and equivalent plastic strain distributions, load-displacement curves, and residual indentation shapes are presented. The number of TiN/Ti layers considerably affect the stress distributions and indentation shapes. Moreover, the greater the number of TiN/Ti layers, the higher is the Brinell hardness. The stress and plastic strain distributions confirm that the multilayer coatings improve the wear resistance. The results are expected to be used to design and evaluate various coating systems, and additional study is required.

Evaluation of electromechanical properties in REBCO CC tapes under transverse compression using anvil test method

  • Diaz, Mark Angelo;Shin, Hyung-Seop
    • Progress in Superconductivity and Cryogenics
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    • v.24 no.3
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    • pp.57-61
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    • 2022
  • One of the major applications of REBCO coated conductor (CC) tapes is in superconducting magnets or coils that are designed for high magnet fields. For such applications, the CC tapes were exposed to a high level of stresses which includes uniaxial tensile or transverse compressive stresses resulting from a large magnetic field. Thus, CC tapes should endure such mechanical load or deformation that can influence their electromechanical performance during manufacturing, cool-down, and operation. It has been reported that the main cause of critical current (Ic) degradation in CC tapes utilized in coil windings for superconducting magnets was the delamination due to transversely applied stresses. In most high-magnetic-field applications, the operating limits of the CC tapes will likely be imposed by the electromechanical properties together with its Ic dependence on temperature and magnetic field. In this study, we examined the influence of the transverse compressive stress on the Ic degradation behaviors in various commercially available CC tapes which is important for magnet design Four differently processed REBCO CC tapes were adopted to examine their Ic degradation behaviors under transverse compression using an anvil test method and a newly developed instantaneous Ic measurement system. As a result, all REBCO CC tapes adopted showed robustness against transverse compressive stresses for REBCO coils, notably at transverse compressive stresses until 250 MPa. When the applied stress further increased, different Ic degradation behaviors were observed depending on the sample. Among them, the one that was fabricated by the IBAD/MOCVD process showed the highest compressive stress tolerance.

Mo,Cu-doped CeO2 as Anode Material of Solid Oxide Fuel Cells (SOFCs) using Syngas as Fuel

  • Diaz-Aburto, Isaac;Hidalgo, Jacqueline;Fuentes-Mendoza, Eliana;Gonzalez-Poggini, Sergio;Estay, Humberto;Colet-Lagrille, Melanie
    • Journal of Electrochemical Science and Technology
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    • v.12 no.2
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    • pp.246-256
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    • 2021
  • Mo,Cu-doped CeO2 (CMCuO) nanopowders were synthesized by the nitrate-fuel combustion method aiming to improve the electrical and electrochemical properties of its Mo-doped CeO2 (CMO) parent by the addition of copper. An electrical conductivity of ca. 1.22·10-2 S cm-1 was measured in air at 800℃ for CMCuO, which is nearly 10 times higher than that reported for CMO. This increase was associated with the inclusion of copper into the crystal lattice of ceria and the presence of Cu and Cu2O as secondary phases in the CMCuO structure, which also could explain the increase in the charge transfer activities of the CMCuO based anode for the hydrogen and carbon monoxide electro-oxidation processes compared to the CMO based anode. A maximum power density of ca. 120 mW cm-2 was measured using a CMCuO based anode in a solid oxide fuel cell (SOFC) with YSZ electrolyte and LSM-YSZ cathode operating at 800℃ with humidified syngas as fuel, which is comparable to the power output reported for other SOFCs with anodes containing copper. An increase in the area specific resistance of the SOFC was observed after ca. 10 hours of operation under cycling open circuit voltage and polarization conditions, which was attributed to the anode delamination caused by the reduction of the Cu2O secondary phase contained in its microstructure. Therefore, the addition of a more electroactive phase for hydrogen oxidation is suggested to confer long-term stability to the CMCuO based anode.

Evaluation of Residual Strains under Pure Bending Loading for Colorless and Optically Transparent Polyimide Film for Flexible Display (유연 디스플레이용 무색 투명 폴리이미드 필름의 굽힘 잔류 변형률 평가)

  • Choi, Min-Sung;Park, Min-Seok;Park, Han-Yeong;Oh, Chung-Seog
    • Journal of the Semiconductor & Display Technology
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    • v.20 no.4
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    • pp.49-54
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    • 2021
  • The display industry is transitioning from traditional rigid products such as flat panel displays to flexible or wearable ones designed to be folded or rolled. Accordingly, colorless and optically transparent polyimide (CPI) films are one of the prime candidates to substitute traditional cover glass as a passivation layer to accommodate product flexibility. However, CPI films subjected to repetitive pure bending loads inevitably entail an accumulation of residual strain that can eventually cause wrinkles or delamination in the underlying component after a certain number of static and cyclic loading. The purpose of this study is to establish an experimental method to systematically evaluate the bending residual strain of CPI films. Films were monotonically and cyclically wrapped on mandrels of various diameters to ensure a constant strain in each. After unwrapping the wound CPI film, the residual radius of curvature remaining on the film was measured and converted into residual strain. The critical radius of curvature at which residual strain does not remain was about 5 mm, and the residual strain decreased in proportion to the log time. It is expected that flexible displays can be reliably designed using the data between the applied bending strain and the residual strain.

Evaluation of the Absorbing Performance of Radar-absorbing Structure with Periodic Pattern after the Low-velocity Impact (주기패턴 레이더 흡수 구조의 저속충격 후 흡수 성능 평가)

  • Joon-Hyung, Shin;Byeong-Su, Kwak
    • Composites Research
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    • v.35 no.6
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    • pp.469-476
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    • 2022
  • In this paper, the microwave absorbing characteristics after the impact of the radar-absorbing structure (RAS) consisting of periodic pattern sheet (PPS) and glass fiber-reinforced plastic (GFRP) were experimentally investigated. The fabricated RAS effectively absorbed the microwave in the X-band (8.2-12.4 GHz). In order to induce the damage to the RAS, a low-velocity impact test with various impact energy of 15, 40, and 60 J was conducted. Afterward, the impact damage was observed by using visual inspection, non-destructive test, and image processing method. Moreover, the absorbing performance of intact and damaged RAS was measured by the free-space measurement system. The experiment results revealed that the delamination damage from the impact energy of 15 J did not considerably affect the microwave absorbing performance of the RAS. However, fiber breakage and penetration damage with a relatively large damaged area were occuured when the impact energy was increased up to 40 J and 60 J, and these failures significantly degraded the microwave absorbing characteristics of the RAS.

Analysis of Crack characteristic on Concrete Cover for Subway Box Structure Due to Reinforcement Corrosion (철근부식으로 인한 지하철 박스구조물의 콘크리트 피복층 균열특성 분석)

  • Choi, Jung-Youl;Shin, Dong-Sub;Chung, Jee-Seung
    • The Journal of the Convergence on Culture Technology
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    • v.8 no.6
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    • pp.727-732
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    • 2022
  • Applying the calculated cross-sectional reduction due to the corroded rebar investigated in the field to the numerical analysis model, the damage pattern and delamination of concrete in the field showed a tendency relatively similar to the numerical analysis results. It was analyzed that when the expansion pressure due to corrosion of the reinforcing bar is greater than the tensile stress of the concrete, cracks are generated and the concrete cover can be fracture. As a result of this study, the correlation between the corrosion rate of reinforcing bars and the crack occurrence of the concrete cover of the subway box structure was verified based on the numerical analysis and field test results. To prevent rebar corrosion, the corrosion rate can be reduced by applying rust prevention to the reinforcing bar and changing the material. In the case of exposed to a corrosive environment, the tensile strength of the concrete is improved by adjusting the concrete compressive strength to secure durability against the expansion pressure caused by the corroded rebar.

A Molecular Simulation on the Adhesion Control of Metal Thin Film-Carbon Nanotube Interface based on Thermal Wetting (Thermal wetting 현상이 탄소나노튜브-금속박막 계면의 응착력에 미치는 영향에 관한 분자 시뮬레이션 연구)

  • Sang-Hoon Lee;Hyun-Joon Kim
    • Tribology and Lubricants
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    • v.39 no.1
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    • pp.8-12
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    • 2023
  • This study presents a molecular simulation of adhesion control between carbon nanotube (CNT) and Ag thin film deposited on silicon substrate. Rough and flat Ag thin film models were prepared to investigate the effect of surface roughness on adhesion force. Heat treatment was applied to the models to modify the adhesion characteristics of the Ag/CNT interface based on thermal wetting. Simulation results showed that the heat treatment altered the Ag thin film morphology by thermal wetting, causing an increase in contact area of Ag/CNT interface and the adhesion force for both the flat and rough models changed. Despite the increase in contact area, the adhesion force of flat Ag/CNT interface decreased after the heat treatment because of plastic deformation of the Ag thin film. The result suggests that internal stress of the CNT induced by the substrate deformation contributes in reduction of adhesion. Contrarily, heat treatment to the rough model increases adhesion force because of the expanded contact area. The contact area is speculated to be more influential to the adhesion force rather than the internal stress of the CNT on the rough Ag thin film, because the CNT on the rough model contains internal stress regardless of the heat treatment. Therefore, as demonstrated by simulation results, the heat treatment can prevent delamination or wear of CNT coating on a rough metallic substrate by thermal wetting phenomena.

Surface Fracture Behaviors of Unidirectional and Cross Ply Glass Fiber/Epoxy Lamina-Coated Glass Plates under a Small-Diameter Steel Ball Impact (일방향 및 직교형 유리섬유/에폭시 복합재로 피막된 판유리의 미소강구 충격에 의한 표면파괴거동)

  • Chang, Jae-Young;Choi, Nak-Sam
    • Composites Research
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    • v.22 no.4
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    • pp.33-40
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    • 2009
  • Fiber orientation effects on the impact surface fracture of the glass plates coated with the glass fiber/epoxy lamina layer were investigated using a small-diameter steel-ball impact experiment. Four kinds of materials were used: soda-lime glass plates, unidirectional glass fiber/epoxy layer(one ply, two plies)-coated, crossed glass tiber/epoxy layer (two plies)-coated glass plates. The maximum stress and absorbed fracture energy were measured on the back surface of glass plates during the impact. With increasing impact velocity, various surface cracks such as ring, cone, radial and lateral cracks appeared near the impacted site of glass plates. Cracks in the plate drastically diminished by glass fiber coating. The tiber orientation guided the directions of delamination and plastic deformation zones between the tiber layer and the glass plate. Impact surface-fracture indices expressed in terms of the maximum stress and absorbed energy could be used as an effective evaluation parameter of the surface resistance.

A Study on Degradation and Recovery Mechanisms of Composites under the Moisture Environment (복합재료의 수분에 의한 열화 및 회복 메커니즘에 관한 연구)

  • Kim, Yun-Hae;Kim, Kook-Jin;Han, Joong-Won;Jo, Young-Dae;Bae, Sung-Youl;Moon, Kyoung-Man
    • Composites Research
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    • v.21 no.2
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    • pp.8-14
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    • 2008
  • Decrease of strength in composite material is generally caused by water absorption. It makes fracture of material, and loss of money or human lives. The objective of this study is to investigate the causes of decrease in strength by water absorption. Mechanism of water absorption was supposed as three steps. This mechanism is consisted of absorption into resin, absorption between resin and surface treatment agent, and delamination between fiber and resin. Conditions of test were supplied differently; kinds of fiber and resin, immersion time etc. Both of reversible reaction and irreversible reaction occurred simultaneously. Most of decrease in strength was finished at 2.5% water absorption, and the strength was recovered. At 4% water absorption, most of decrease was caused by irreversible reaction, therefore, there was a tendency not to be recovered in strength.

Direct Numerical Simulation of Composite laminates Under low velocity Impact (저속충격을 받는 적층복합재료 평판의 직접 수치모사)

  • Ji, Kuk-Hyun;Kim, Seung-Jo
    • Composites Research
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    • v.19 no.1
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    • pp.1-8
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    • 2006
  • Prediction of damage caused by low-velocity impact in laminated composite plate is an important problem faced by designers using composites. Not only the inplane stresses but also the interlaminar normal and shear stresses playa role in estimating the damage caused. But it is well known that the conventional approach based on the homogenization has the limit in description of damage. The work reported here is an effort in getting better predictions of dynamic behavior and damage in composite plate using DNS approach. In the DNS model, we discretize the composite plates through separate modeling of fiber and matrix for the local microscopic analysis. In the view of microscopic mechanics with DNS model, interlaminar stress behaviors in the inside of composite materials are investigated and compared with the results of the homogenized model which has been used in the conventional approach to impact analysis. Also the multiscale model based on DNS concept is developed in order to enhance the effectiveness of impact analysis, and we present the results of multiscale analysis considering micro and macro structures simultaneously.