• Title/Summary/Keyword: Delamination

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Economic Analysis with Development of Rapid Setting Alumina-based Binder for Road Repair (알루미나계열 속경성 도로 보수재료 개발에 따른 경제성 분석)

  • Yang, Hee-Jun;Yang, Min-Jae;Hong, Sung-In;Ann, Ki-Yong
    • Journal of the Korea Concrete Institute
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    • v.29 no.1
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    • pp.3-10
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    • 2017
  • In case of Korea highways, about 60% of highways are paved by concrete and more than 50% of them were repaired due to reduction in required performance such as damage in pave or joint and delamination of cover pavement. However, repairing old material in such structure generally costs a lot of money and induces difficulty in maintenance. Thus, enhanced material for ensuring economic efficiency should be developed. The present study designed concrete mixtures with 3 levels of replacement using OPC (0, 10, 20%) in calcium aluminate cement and to evaluate material performance for load pavement, experimental works for setting time, compressive strength and flexural strength were carried out on those materials. As a result, 20% replacement for OPC was determined as an optimized material in terms of required physical performance and its unit price. Moreover, to determine cost in load pavement economy analysis using a program (CA4PRS) was conducted with widely used paving materials. Result showed that application for 20% replacement for OPC was the most efficient in economical aspect, arising from 4.052 and 1.577 billion won for total construction and user cost, respectively.

An Experimental Study on the Mechanical Properties of HPFRCCs Reinforced with the Micro and Macro Fibers (마이크로 및 매크로 섬유에 의해 보강된 고인성 시멘트 복합재료의 역학적 특성에 관한 실험적 연구)

  • Kim Moo-Han;Kim Jae-Hwan;Kim Yong-Ro;Kim Young-Duck
    • Journal of the Korea Concrete Institute
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    • v.17 no.2 s.86
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    • pp.263-271
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    • 2005
  • HPFRCC(High Performance Fiber Reinforced Cementitious Composite) is a class of FRCCs(Fiber Reinforced Cementitious Composites) that exhibit multiple cracking. Multiple cracking leads to improvement in properties such as ductility, toughness, fracture energy, strain hardening, strain capacity, and deformation capacity under tension, compression, and bending. These improved properties of HPFRCCs have triggered unique and versatile structural applications, including damage reduction, damage tolerance, energy absorption, crack distribution, deformation compatibility, and delamination resistance. These mechanical properties of HPFRCCs become different from the kinds and shapes of used fiber, and it is known that the effective size of fiber in macro crack is different from that in micro crack. This paper reports an experimental findings on the mechanical properties of HPFRCCs reinforced with the micro fiber(PP50, PVA100 and PVA200) and macro fiber(PVA660, SF500). Uniaxial compressive tests and three point bending tests are carried out in order to compare with the mechanical properties of HPFRCCs reinforced with micro fibers or hybrid fibers such as compressive strength, ultimate bending stress, toughness, deformation capacity and crack pattern under bending, etc.,

Preparation of Cellulose-Based Edible Film and its Physical Characteristics (Cellulose를 이용한 가식성(可食性) Film의 제조와 물리적 특성연구)

  • Song, Tae-Hee;Kim, Chul-Jai
    • Korean Journal of Food Science and Technology
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    • v.28 no.1
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    • pp.1-7
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    • 1996
  • Three formulations were used to prepare the cellulose-based edible films consisting of hydrocolloid and lipids; film A made by coating method, films B and C by emulsion method, which were formed in a thin layer glass plate and then dried. Films A, B and C were all approximately 0.03 mm thick with 1-3% moisture, 59-68% lipid, and almost whitish color. Film A was better in tensile strength, and lipids affected water vapor permeability on three films, in which films A and B did not differ significantly. Water vapor permeability of film A did not change but those of films B and C decreased significantly after storage for 8 weeks at $-15^{\circ}C$. Oxygen transmission rate and oxygen permeability of films A and C did not differ and changed significantly after 8-week storage at $-15^{\circ}C$. Under scanning electron microscope (SEM) observation on the structural characteristics of each film, film A indicated relatively uniform and smooth surface coatings of beeswax, while films B and C had individual lipid crystals and could be discerned. As a result, film A was better than films B and C in respect of physical properties, but the selection of useful film depended upon which physical property was more functional. Moreover, it was desirable in some cases for using films B and C because of their easiness of preparation and cold storage durability. It will be further needed to investigate how to formulate films B and C to have more unique surface characteristics, and to reduce water vapor and oxygen transmission rates.

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A Study on the Shear Strengthening Characteristic of Reinforced Concrete T-shaped Beams (철근콘크리트 T형보의 전단 보강 특성에 관한 연구)

  • Kim, Jeong Sup;Shin, Yong Seok;Moon, Keum Hwan;Yoo, Myeong Hwan;Lee, Chang Hyun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.16 no.2
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    • pp.10-18
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    • 2012
  • Most of studies on existing strengthening methods were mainly on increase of stiffness and strength of shear strengthening to rectangular beam. As concrete of beam and slab is poured simultaneously on the characteristics of construction in reinforced concrete beam-slab structure, adjacent slab uniformed after hardening has T-shaped beam cross section which makes the flange of beam, enhances the stiffness of the beam and widens the area supporting compressive strength, but available data of flexural behavior of T-shaped beam are lacking. In this research the T-shaped beams would be made, then the reinforced effects and structural properties can be estimated according to the kinds of reinforced materials and reinforced position. The conclusions are shown as below. To sum up the experimental results, The specimen which was reinforce by CB embedded inside of concrete indicated excellent resistive behavior, internal force and stiffness when it was destroyed. The steel plate reinforced specimen of stiffness and internal force were increase but it expressed lower reinforce effects because of lowering anchored force between concrete. Fiber sheet strengthening showed superior effects but the interfacial delamination was found due to the lack of anchored force in destruction. So the measure is needed now.

HIGH HEAT FLUX TEST WITH HIP BONDED 35X35X3 BE/CU MOCKUPS FOR THE ITER BLANKET FIRST WALL

  • Lee, Dong-Won;Bae, Young-Dug;Kim, Suk-Kwon;Jung, Hyun-Kyu;Park, Jeong-Yong;Jeong, Yong-Hwan;Choi, Byung-Kwon;Kim, Byoung-Yoon
    • Nuclear Engineering and Technology
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    • v.42 no.6
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    • pp.662-669
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    • 2010
  • To develop the manufacturing methods for the blanket first wall (FW) of the International Thermonuclear Experimental Reactor (ITER) and to verify the integrity of the joint, Be/Cu mockups were fabricated and tested at the KoHLT-1 (Korea Heat Load Test facility), a graphite heater facility located at the Korea Atomic Energy Research Institute (KAERI). Since Be and Cu joining is the focus of the present study, the fabricated mockups had a CuCrZr heat sink joined with three Be tiles as an armor material, unlike the original ITER blanket FW, which has a stainless steel structure and coolant tubes. Hot isostatic pressing (HIP) was carried out at $580^{\circ}C$ and 100 MPa for 2 hours as the method for Be/Cu joining. Three interlayers, namely, $1{\mu}mCr/10{\mu}mCu$, $1{\mu}mTi/0.5{\mu}mCr/10{\mu}mCu$, and $5{\mu}mTi/10{\mu}mCu$ were applied as a coating to the Be tiles by a physical vapor deposition (PVD) method. A shear test was performed with the specimens, which were fabricated by the same methods as those used to fabricate the mockups. The average values were 125 MPa to 180 MPa, and the samples with the $1{\mu}mCr/10{\mu}mCu$ interlayer showed the lowest value. No defect or delamination was found in the joints of the mockups by the developed ultrasonic test using a flat-type probe with a 10 MHz frequency and a 0.25 inch diameter. High heat flux (HHF) tests were performed at $1.0\;MW/m^2$ heat flux for each mockup using the given conditions, and the results were analyzed by ANSYS-CFX code. For the test criteria, an expected fatigue lifetime about 1,000 cycles was obtained by analysis with ANSYS-mechanical code. Mockups using the interlayers of $1{\mu}mTi/0.5{\mu}mCr/10{\mu}mCu$ and $5{\mu}mTi/10{\mu}mCu$ survived up to 1,100 cycles over the required number of cycles. However, one of the Be tiles in the other two mockups using the $1{\mu}mCr/10{\mu}mCu$ interlayer was detached during the screening test, and others were detached by discharge after 862 cycles. The integrity of the joints using the proposed interlayers was proven by the HHF test, but the other interlayer requires more study before it can be used for the joining of Be to Cu. Moreover, it was confirmed that the measured temperatures agreed well with the analysis temperatures, which were used to estimate the lifetime and that the developed facility showed its capability of the long time operation.

Three-dimensional micro photomachining of polymer using DPSSL (Diode Pumped Solid State Laser) with 355 nm wavelength (355nm 파장의 DPSSL을 이용한 폴리머의 3차원 미세 형상 광가공기술)

  • 장원석;신보성;김재구;황경현
    • Korean Journal of Optics and Photonics
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    • v.14 no.3
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    • pp.312-320
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    • 2003
  • The basic mechanistic aspects of the interaction and practical considerations related to polymer ablation were briefly reviewed. Photochemical and photothermal effects, which highly depend on laser wavelength have close correlation with each other. In this study, multi-scanning laser ablation processing of polymer with a DPSS (Diode Pumped Solid State) 3rd harmonic Nd:YVO$_4$ laser (355 nm) was developed to fabricate a three-dimensional micro shape. Polymer fabrication using DPSSL has some advantages compared with the conventional polymer ablation process using KrF and ArF laser with 248 nm and 193 nm wavelength. These advantages include pumping efficiency and low maintenance cost. And this method also makes it possible to fabricate 2D patterns or 3D shapes rapidly and cheaply because CAD/CAM software and precision stages are used without complex projection mask techniques. Photomachinability of polymer is highly influenced by laser wavelength and by the polymer's own chemical structure. So the optical characteristics of polymers for a 355 nm laser source is investigated experimentally and theoretically. The photophysical and photochemical parameters such as laser fluence, focusing position, and ambient gas were considered to reduce the plume effect which re-deposits debris on the surface of substrate. These phenomena affect the surface roughness and even induce delamination around the ablation site. Thus, the process parameters were tuned to optimize for gaining precision surface shape and quality. This maskless direct photomachining technology using DPSSL could be expected to manufacture tile prototype of micro devices and molds for the laser-LIGA process.

Study on the Crack and Thermal Degradation of GFRP for UPE Gelcoat Coated Underground Pipes Under the High Temperature Water-Immersion Environment (고온 수침 환경에서 UPE 겔코트 코팅된 지중 매설 파이프용 GFRP의 열화 및 크랙 발생 특성에 관한 연구)

  • Kim, Daehoon;Eom, Jaewon;Ko, Youngjong;Lee, Kang-Il
    • Journal of the Korean Geosynthetics Society
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    • v.17 no.4
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    • pp.169-177
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    • 2018
  • Glass fiber reinforced polyester (GFRP) composites are widely used as structural materials in harsh environment such as underground pipes, tanks and boat hulls, which requires long-term water resistance. Especially, these materials might be damaged due to delamination between gelcoat and composites through an osmotic process when they are immersed in water. In this study, GFRP laminates were prepared by surface treatment of UPE (unsaturated polyester) gelcoat by vacuum infusion process to improve the durability of composite materials used in underground pipes. The composite surface coated with gelcoat was examined for surface defects, cracking, and hardness change characteristics in water-immersion environments (different temperatures of $60^{\circ}C$, $75^{\circ}C$, and $85^{\circ}C$). The penetration depth of cracks was investigated by micro CT imaging according to water immersion temperature. It was confirmed that cracks developed into the composites material at $75^{\circ}C$ and $85^{\circ}C$ causing loss of durability of the materials. The point at which the initial crack initiated was defined as the failure time and the life expectancy at $23^{\circ}C$ was measured using the Arrhenius equation. The results from this study is expected to be applied to reliability evaluation of various industrial fields where gelcoat is applied such as civil engineering, construction, and marine industry.

Effect of Amino Modified Siloxanes with Two Different Molecular Weights on the Properties of Epoxy Composites for Adhesives for Micro Electronics (전자소재 접착제용 에폭시에 두 종의 다른 당량수를 갖는 아미노 변성 실록산이 미치는 영향)

  • Yu, Kihwan;Kim, Daeheum
    • Applied Chemistry for Engineering
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    • v.22 no.1
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    • pp.104-108
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    • 2011
  • In the non-conductive adhesives (NCAs) for adhesion of micro electro mechanical system (MEMS), there are some problems such as delamination and cracking resulting from the large differences of coefficients of thermal expansion (CTE) between NCAs and substrates. So, the addition of inorganic particles such as silica and nano clay to the CTEs composit have been applied to reduce the CTEs of the adhesives. Additions of the flexibilizers such as siloxanes have also been performed to improve the flexibility of epoxy composite. Amino modified siloxane (AMSs) were used to improve compatibility between epoxy and siloxane. In this study, glass transition temperatures (Tg) and moduli of those composites were measured to confirm the effects of AMS with two different equivalents on thermal/mechanical properties of AMS/epoxy composites. Tg of KF-8010/epoxy composites decreased from 148 to $122^{\circ}C$ and those of X-22-161A/epoxy composites decreased from 148 to $121^{\circ}C$. Moduli of KF-8010/epoxy composites decreased from 2648 to 2143 MPa by adding KF-8010 and moduli of X-22-161A/epoxy composites decreased from 2648 to 2014 MPa. In short, using long Si-O chain AMS leads to a greater decrease in moduli. However, haven't showed significant differences in Tg's.

A Study on Flux Immunity MUF for Improving Flip Chip PKG Reliability (Flip Chip PKG 신뢰성 향상을 위한 Flux Immunity 개선 MUF 구현 방안 연구)

  • Lee, Junshin;Lee, Hyunsuk;Kim, Minseok;Kim, Sungsu;Moon, Kiill
    • Journal of the Microelectronics and Packaging Society
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    • v.29 no.2
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    • pp.49-52
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    • 2022
  • As the difficulty of flip chip products increase, interest in stable PKG material technology from the viewpoint of reliability is increasing. Currently, the representative of poor reliability that are mainly occurring in flip chip PKG are Sn bridge and Cu dendrite. Two type defects are caused by void generated by the flux residue around the bump. In order to essentially minimize the risk of this type of reliability failure, the linkage between the composition of Molded Under-fill (MUF) and flux, which is related material, was reviewed. In this study, the correlation between base resin and filler, which is the main component of MUF, and flux, was defined, and the material composition design was carried out by refer to lesson learn. With the current material composition, it was confirmed that moisture absorption reliability 85%/85%/24hrs pass result and void did not occur during destructive analysis, and developed MUF has shown flux immunity improving result in flip Chip PKG. We think this study can be used in yield enhancement of flip chip process and give insights to study in compatibility between MUF and flux.

Mechanical evaluation of SiC-graphite interface of seed crystal module for growing SiC single crystals (탄화규소 단결정 성장을 위한 종자결정모듈의 탄화규소-흑연 간 접합계면의 기계적 특성 평가)

  • Kang, June-Hyuk;Kim, Yong-Hyeon;Shin, Yun-Ji;Bae, Si-Young;Jang, Yeon-Suk;Lee, Won-Jae;Jeong, Seong-Min
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.32 no.5
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    • pp.212-217
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    • 2022
  • Large thermal stress due to the difference between silicon carbide and graphite's coefficients of thermal expansion could be formed during crystal growing process of silicon carbide (SiC) at high temperature. The large thermal stress could separate the SiC seed crystals from graphite components, which bring about the drop of the seed crystal during crystal growth. However, the bonding properties of SiC seed crystal module has hardly reported so far. In this study, SiC and graphite were bonded using 3 types of bonding agents and a three-point bending tests using a mixed-mode flexure test were conducted for the bonded samples to evaluate the bonding characteristics between SiC and graphite. Raman spectroscopy, X-ray Photoelectron Spectroscopy, and X-ray Computed Tomography were used to analyze the bonding characteristics and the microstructures of the SiC-graphite interfaces bonded with the bonding agents. As results, an excellent bonding agent was chosen to fabricate SiC seed crystal module with 50 mm in diameter. An SiC single crystal with 50 mm in diameter was successfully grown without falling out during top seeded solution growth of SiC at high temperature.