• Title/Summary/Keyword: DLC coating.

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Hydrocarbon Plasma of a Low-Pressure Arc Discharge for Deposition of Highly-Adhesive Hydrogenated DLC Films

  • Chun, Hui-Gon;Oskomov, Konstantin V.;Sochugov, Nikolay S.;Lee, Jing-Hyuk;You, Yong-Zoo;Cho, Tong-Yul
    • Journal of the Semiconductor & Display Technology
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    • v.2 no.1
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    • pp.1-5
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    • 2003
  • Plasma generator based on non-self-sustained low-pressure arc discharge has been examined as a tool for deposition of highly-adhesive hydrogenated amorphous diamond-like carbon(DLC) films. Since the discharge is stable in wide range of gas pressures and currents, this plasma source makes possible to realize both plasma-immersion ion implantation(PIII) and plasma-immersion ion deposition(PIID) in a unified vacuum cycle. The plasma parameters were measured as functions of discharge current. Discharge and substrate bias voltage parameters have been determined for the PIII and PIID modes. For PIID it has been demonstrated that hard and well-adherent DLC coating are produced at 200-500 eV energies per deposited carbon atom. The growth rates of DLC films in this case are about 200-300 nm/h. It was also shown that short(∼60$\mu\textrm{s}$) high-voltage(> 1kV) substrate bias pulses are the most favorable for achieving high hardness and good adhesion of DLC, as well as for reducing of residual intrinsic stress are.

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Friction, Wear and Scuffing Life of Piston Rings With Several Coating for Low Friction Diesel Enging (다양한 박막을 증착한 디젤 엔진용 피스톤링과 실린더 블록의 마찰 마멸 및 스커핑 수명 평가)

  • Ahn, Tae-Sik;Cho, Dae-Hyun;Oh, Chung-Soon;Lee, Young-Ze
    • Tribology and Lubricants
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    • v.23 no.4
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    • pp.170-174
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    • 2007
  • Wear and scuffing tests were conducted using friction and wear measurement of piston rings and cylinder blocks in low friction diesel engine. The frictional forces, wear amounts and cycles to scuffing in boundary lubricated sliding condition were measured using the reciprocating wear tester. The cylinder blocks were used as reciprocating specimens, and the piston rings with several coatings were used as fixed pin. Several coatings were used such as DLC, TiN, Cr-ceramic and TiAlN in order to improve the tribological characteristics. From the tests wear volume of piston ring surfaces applied various coatings were compared. During the tests coefficients of friction were monitored. Test results showed that DLC coatings showed good tribological properties. TiN and Cr-ceramic coated rings showed good wear resistance properties but produced high friction.

THE INFLUENCE OF ABUTMENT SCREW TIGHTENING TIMING AND DLC COATING OF CONICAL CONNECTION IMPLANT SYSTEM (일체형 지대주의 Diamond Like Carbon 표면 처리와 나사 조임 시기가 풀림 현상에 미치는 영향)

  • Kim, Ki-Hong;Koak, Jai-Young;Heo, Seong-Joo
    • The Journal of Korean Academy of Prosthodontics
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    • v.46 no.2
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    • pp.209-216
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    • 2008
  • Statement of problem: It is difficult about assessing the loosening tendency of conical connection type implant after cyclic loading with diamond like carbon coating one-piece abutments, and also about the retightening effect. Purpose: This study was performed to investigate the influence of one-piece abutment screw retightening after $5.0{\times}10^{4}$ cyclic loading and Diamond like coating Material and methods: Thirty two ITI implant were divided to 4 groups. Group 1,3-titanium abutment, group 2,4 - diamond like carbon coated abutment. Group 1,2 - $20.0{\times}10^{4}$ cyclic loading after $5.0{\times}10^{4}$ cyclic loading, Group 3,4- after $20.0{\times}10^{4}$ Cyclic loading. After cyclic loading, periotest values were taken and removal torque values of abutments were measured with a digital torque gauge. Results: 1. The removal torque of group 2 after $5.0{\times}10^{4}$ cyclic loading is slightly greater than the other groups but not significantly higher than others (P>0.05). 2. The final removal torque values after $20.0{\times}10^{4}$ cyclic loading of group 1 is bigger than group 3, and group 2 is bigger than group 4, but not significantly higher (P>0.05). 3. The final removal torque values after $20.0{\times}10^{4}$ cyclic loading of all groups are not significantly different (P>0.05).

Optical and Mechanical Properties of Diamond-like Carbon Film with Variation of Carbon Ratio (탄소비율에 따른 Diamond-like Carbon Film의 광학적 및 기계적 특성)

  • Yun, Deok-Yong;Park, Yong-Seob;Choi, Won-Seok;Hong, Byung-You
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.9
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    • pp.808-811
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    • 2008
  • Optical and mechanical properties of diamond-like carbon (DLC) films synthesized by RF plasma enhanced chemical vapor deposition were investigated as a function the C/H ratio in gas mixture. The C/H ratio was varied from 6 to 10 %, adjusting the amount of $CH_4$ and $H_2$ as the source gas. The optical and mechanical properties of DLC films were characterized by UV spectrometer, Ellipsometer and Nano-indenter. The change of the C/H ratio during synthesis of DLC films had many effects on the growth rate, transmittance, refractive index and hardness. The growth rate of the films increased exponentially with the increase in C/H ratio. The hardness of the films showed the tendency to improve with increasing C/H ratio, whereas the transmittance decreased. The refractive index was varied from 2.03 to 2.17, and these refractive indexes close to 2.0 indicates that it can be applied to Si-based solar cell.

SEM and PV Properties of WC Core Surface with DLC Coating (초경합금(WC) 코어면의 Re-Ir 코팅에 따른 표면 조도 특성)

  • Lee, Ho-Shik;Park, Yong-Pil;Cheon, Min-Woo
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2010.05a
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    • pp.828-829
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    • 2010
  • Rhenium-Iridium(Re-Ir) thin films were deposited onto the tungsten carbide(WC) molding core by sputtering system. The Re-Ir thin films on tungsten carbide molding core were analyzed by scanning electron microscope(SEM) and surface roughness. The Re-Ir coating technique has been intensive efforts in the field of coating process because the coating technique and process have been their feature, like hardness, high elasticity, adrasion resistance and mechanical stability and also have been applied widely the industrial and biomedical areas. In this report, tungsten carbide(WC) molding core was manufactures using high performance precision machining and the efforts of Re-Ir coating on the surface roughness.

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Corrosion Properties of Carbon-Coated Metallic Bipolar Plate for PEMFC (고분자 전해질 연료전지 금속 분리판 적용을 위한 탄소 박막의 증착과 내식성 평가)

  • Jang, Dong-Su;Lee, Jung-Joong
    • Journal of Surface Science and Engineering
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    • v.48 no.3
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    • pp.87-92
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    • 2015
  • Carbon thin films were deposited on STS 316L sheets by inductively coupled plasma enhanced magnetron sputtering with or without substrate bias voltage. Typical Raman spectrum for amorphous diamond-like carbon (DLC) was obtained, and the interfacial contact resistance (ICR) was measured to show its conductive nature. The electrochemical impedance spectroscopy (EIS) was used to investigate the corrosion mechanism of the carbon coating under the polymer electrolyte membrane fuel cell (PEMFC) condition. According to the pore-corrosion mechanism, the electrolyte penetrates the carbon coating through the pores and reacts with the substrate. As the substrate corrosion proceeds, the pore enlargement occurs and the surface area of the substrate exposed to the electrolyte. Applicability of the carbon coating for the PEMFC bipolar plate was evaluated by potentiodynamic polarization experiments. Finally, an adhesion problem was briefly considered.

A Study on DLC Hard Coating in Ocular Lens(CR-39) (안경렌즈(CR-39)에의 DLC Hard 코팅에 관한 연구)

  • Lee, Won Jin
    • Journal of Korean Ophthalmic Optics Society
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    • v.6 no.1
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    • pp.87-91
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    • 2001
  • The a-C:H films have been grown on the glass substrate by PECVD method, where plasma was generated with a 60 Hz line power source. The carbonization is checked from peak intensities of D($sp^3$) and G($sp^2$) peaks in Raman spectra and is analyzed using the Gaussian convolution method of spectrum. Both the bonding strength of C-H and the ratio of $sp^3$ to $sp^2$ in bonding are found to be slightly dependent of partial pressure of $C_2H_2$.

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Hydrogen Free Diamond like Carbon Coating technology for tribological applications (트라이볼로지 응용을 위한 고경도 HF-DLC 코팅 기술 및 응용 사례)

  • Kim, Jong-Guk;Gang, Yong-Jin;Kim, Do-Hyeon;Jang, Yeong-Jun;Lee, Sang-Jin;Kim, Jae-Il
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2018.06a
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    • pp.36-36
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    • 2018
  • 4차 산업 혁명의 영향으로 인공지능, 로봇이 활발히 이용됨에 따라, 산업은 software 면에서 지능화 및 무인자동화로 빠른 변화를 일으키고 있다. 이에 따라 사용되는 hardware는 고신뢰성 및 고성능화를 필요로 하게 되고, 이들의 내구성 및 장수명화를 요구하고 있다. 하지만 장시간 사용 안정성, 사용 기계 부품의 내구성 향상은 사용부품의 소재, 사용 조건등의 변화를 요구하게 되고, 이들은 학문적 의미에서의 트라이볼로지적 특성 향상이 필연적으로 뒷받침되어야 한다. 본 발표에서는 트라이볼로지적 특성 향상을 위한 표면코팅처리 기술로, 자장여과아크방식을 활용하여 solid carbon을 이용한 무수소 DLC 증착 기술에 대하여 발표하고, 그 응용으로 자동차 부품 및 절삭공구 등에 적용한 사례를 소개하고자 한다.

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Conductive and Mechanical Properties Study of Ti-doped DLC (ta-C:Ti) Film on Semiconductor Probe through Taguchi Bobust Design (다구찌 강건 설계를 통한 반도체 Probe상 Ti 도핑된 DLC(ta-C:Ti) 코팅 막의 전도성 및 기계적 물성 연구)

  • Kim, Do-young;Shin, Jun-ki;Jang, Young-Jun;Kim, Jongkuk
    • Tribology and Lubricants
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    • v.38 no.6
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    • pp.274-280
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    • 2022
  • There is a problem that semiconductor probe pin has a short lifespan. In order to solve this problem, Ti having excellent conductivity was doped to tetrahedral amorphous carbon (ta-C) having excellent hardness and abrasion resistance. This experiment was planned through the Taguchi robust design to determine the effect of the control factor of the ta-C:Ti coating film. The effect and contribution of control factors such as Unbalanced Magnetron Sputter(UBM) discharge current, arc discharge current, temperature, and bias voltage on ta-C:Ti characteristics were analyzed from the perspective of electrical and mechanical characteristics. The UBM discharge current was set to 4, 6, and 8 A. The main control factor of thickness and resistance is the UBM discharge current, and the thickness increased and the resistance decreased as the current increased. The decrease in resistance is due to the increase in the Ti content of the ta-C:Ti coating film. The arc discharge current was set to 60, 80, and 100 A. The main control factor of hardness and wear is the arc discharge current, and as the current rises, the hardness increases and the wear area decreases. This is due to the increased ta-C content of the ta-C:Ti coating film. Since resistance and wear are important for Probe Pin, the optimal level is set from the perspective of resistance and wear and a confirmation experiment is conducted.