• Journal of the Korean Society for Nondestructive Testing
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• v.29 no.2
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• pp.104-107
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• 2009

It was verified that the effect of the distance between current input point and output point on direct current potential drop(DCPD) in the material with two-dimensional surface notch. If the distance between potential drop measuring points was fixed at a certain distance, the potential drop was decreased with increasing the distance between current input and output points. Hence it is the effect way to increase sensitivity in DCPD that the current input and output points should be located near the potential measuring points. DCPD was a useful method for surface crack sizing because the potential drop was proportional to the length of notch. When the current input and output points are located near the potential measuring points, even small length crack can be measured by DCPD technique.

• Composites Research
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• v.31 no.2
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• pp.57-62
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• 2018

Interfacial and mechanical properties of neat and two sizing agents coated glass fiber (GF)/polydicyclopentadiene (p-DCPD) composites were evaluated at room and low temperatures, $25^{\circ}C$ and $-20^{\circ}C$. Sizing agents of GFs were extracted using acetone and compared via FT-IR. Surface energy and work of adhesion between GFs and p-DCPD were calculated by dynamic contact angle measurement. Mechanical properties of different GFs were determined using single fiber tensile test and interfacial properties of single GF reinforced DCPD strip were determined using cyclic loading tensile test. Mechanical properties of GFs/p-DCPD composites at room and low temperatures were determined using tensile, compressive, and Izod impact tests. Interfacial and mechanical properties were different with sizing agents of GFs and the optimized condition of sizing agent was found.

• Corrosion Science and Technology
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• v.12 no.2
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• pp.93-101
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• 2013

The object of this work is to establish an electrochemical noise(EN) measurement technique combined with a direct current potential drop(DCPD) method for monitoring of localized corrosion cracking of nickel-based alloy, and to analyze its mechanism. The electrochemical current and potential noises were measured under various conditions of applied stress to a compact tension specimen in a simulated primary water chemistry of a pressurized water reactor. The amplitude and frequency of the EN signals were evaluated in both time and frequency domains based on a shot noise theory, and then quantitatively analyzed using statistical Weibull distribution function. From the spectral analysis, the effect of the current application in DCPD was found to be effectively excluded from the EN signals generated from the localized corrosion cracking. With the aid of a microstructural analysis, the relationship between EN signals and the localized corrosion cracking mechanism was investigated by comparing the shape parameter of Weibull distribution of a mean time-to-failure.

• Proceedings of the Materials Research Society of Korea Conference
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• 2009.11a
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• pp.35.2-35.2
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• 2009

최근 전세계적으로 저탄소, 녹색성장으로 인하여 원자력발전이 주목받고 있다. 또한 에너지의 고효율로 인한 발전소의 설비가 대형화가 됨에 따라 발전소의 수명평가와 건전성평가가 중요해지고 있다. 일반적으로 구조물 내에 존재하는 균열의 크기와 형상을 파악하여 피로균열전파속도를 평가함으로써 건전성평가를 확인하고 있다. 그리고 고온, 고압에서의 피로균열전파속도는직류전위차 (Direct Current Potential Drop : DCPD)법을 사용하고 있다. DCPD법은 균열의 정밀한 측정방법으로써 측정시 오차가 발생하기 때문에 ASTM에서 제시된 incremental polynomial 법을 권고하고 있다. 따라서 본 연구에서는 피로균열전파전파속도의통계적처리를 통해서 합리적인 곡선을 구하여 건전성평가에 활용하고자 한다. 실험에 사용된 시편은 두께 5mm, 폭 25.4mm CT시편을 사용하였으며, 1mm의 예비균열을 주었다. 그리고 실험온도는 상온에서 실시 하였으며, 주파수는 10Hz를 주었다. 그리고 DCPD 측정을 위해 5A의 전류를 주었으며, 이때 측정된 전압값을 ASTM에 제시된 관계식에넣어 균열길이로 환산하였으며, 데이터처리는 ASTM에 제시된 incremental polynomial법을 기본적으로 사용하였다. 또한 ASTM에 제시된 2n+1을 이용하여 데이터의 수 n을 1~7 까지 변화를 주어 3~15 point 까지 데이터를 처리하여곡선을 제시하였다. 분석결과 $R^2$값이 1을 기준으로 했을 때 3~7 point 까지는큰 차이를 보이지 않았지만 9-point 이후부터는 $R^2$ 감소함을 알 수 있었다. 또한 적용된 데이터의수에 따라 피로군열전파속도 곡선에서 측정된 Paris law의 n값과 C 값은 큰차이를 보이지 않았다.

• Transactions of the Korean hydrogen and new energy society
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• v.30 no.6
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• pp.629-634
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• 2019

Dicyclopentadiene is a low viscosity resin which forms a poly-dicyclopentadiene rapidly through ring opening metathesis polymerization (ROMP). This poly-dicyclopentadiene has outstanding properties of low-temperature, water and impact resistances. Due to these advantages, military and offshore structures try to apply the DCPD composites by using liquid composite molding process. In this study, 14%, 38% volume fraction fiber glass strand mat reinforced p-DCPD composites processed by structural reaction injection molding (S-RIM) which has resin-catalsyt mixing head and glass fiber preform in the mold. Additionally, S-RIM numerical analysis was conducted to predict the process time depending on fiber volume fraction and mold temperature. The process time is shorter when it has the lower fiber volume fraction or the higher mold temperature. At higher mold temperature, it is necessary to set the maximum mold temperature considering the resin curing time.

• Journal of the Korean Ceramic Society
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• v.48 no.1
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• pp.26-33
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• 2011

The glass in the system of CaO-$SiO_2-P_2O_5$ and the corresponding glass-ceramics are prepared for bone cements and the behaviors of the hardening and hydroxyapatite formation were studied for the glass and glass-ceramic powders. The glass crystallized into apatite, $\alpha$-wollastonite and $\beta$-wollastonite depending on the glass composition when they were heat-treated at $950^{\circ}C$ for 4 h. A DCPD (dicalcium phosphate dihydrate : $CaHPO_4{\cdot}2H_2O$) was developed when the prepared glass and glass-ceramic powders were mixed with 3M-$H_3PO_4$ solution. The DCPD (Ca/P=1.0) transformed to HAp (Ca/P=1.67) when the bone cement was soaked in simulated body fluid (SBF), and this HAp formation strongly depended on the releasing capacity of $Ca^{2+}$ ions from the glass and glass-ceramic cements. The glass-ceramic bone cement containing $\alpha$-wollastonite crystals showed faster transformation of DCPD to HAp than other glass-ceramics containing $\alpha$- and $\beta$-wollastonite crystals. No hydroxyapatite was observed when the glass-ceramic bone cement containing apatite crystals (36P6C) was soaked in SBF even for 1 month, because no $Ca^{2+}$ ion can be released from the stable apatite crystals.

• Journal of Adhesion and Interface
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• v.15 no.4
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• pp.145-150
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• 2014

Dicyclopentadiene (DCPD)-based hydrocarbon resins are widely used as tackifiers in many applications. In particular, hydrogenated DCPD-based hydrocarbon resins are widely used in premium hot-melt-type adhesives such as hot melt adhesives (HMAs) and/or hot melt pressure-sensitive adhesives (HMPSAs), because are water-white in color and possess excellent stability to light and heat. This article discusses the adhesive performance of various hydrogenated DCPD resins when they are used as tackifiers in styrene-block-copolymer (SBC)-based HMPSAs. This article shows the correlation between the characteristics of tackifiers and the adhesive performance of SBC-based HMPSAs. The higher the softening point of the tackifier, the higher is the $T_g$, softening point, and crossover temperature of the PSAs. High aromatic H wt% content reduces the high-temperature resistance of PSAs, as suggested by the decrease in the crossover temperature and softening point of the PSAs.

• Journal of Pharmaceutical Investigation
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• v.6 no.1
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• pp.26-32
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• 1976

Dicalcium phosphate dihydrate (DCPD) is the most widely-used dentifrice abrasive in non-therapeutic tooth-paste requiring, low abrasive level, high stability and excellent compatibility with other formulation ingredients. One of the difficulties encountered in the use of this material in tooth-paste is that unless storage of the product is maintained at a relative low temperature there is a distinct tendency to lose water of crystallization. Another difficulty which has been encountered is that there is a tendency for the product to become lumpy. Various means have been proposed for increasing the stability and overcoming the lumping tendency, most of which means comprise the addition of stabilizing agent. But there is not any report about the relationships between the mechanism of dehydration, physical properties, structure and manufacturing condition. In this experiment, DCPD were manufactured by methods of Moss' patent, its two varied and J.P.VIII, these were studied by means of stability test, IR spectra, and DTA. According to the manufacturing conditions, DCPD has different physical properties and structures, i. e., monoclinic system of low drying temperature, triclinic system of high drying temperature. Dehydration of DCPD may be supposed one step debydration at about $100^{\circ}$ and it finaly converts to ${\gamma}-pyrophosphate$ at about $465^{\circ}$ and if the drying temperature is high it becomes DCP anhydrous. DCPD made by Moss' patent is thought of the best polishing agent of tooth-paste.

• Journal of the Korean Ceramic Society
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• v.42 no.11 s.282
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• pp.770-776
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• 2005

Hardening and hydroxyapatite(HAp) formation behavior of the bioactive cements in the system of $CaO-SiO_{2}-P_{2}O_{5}$ glasses and the corresponding glass-ceramics were studied. DCPD (Dicalcium Phosphate Dihydrate: $CaHPO_4{\cdot}2H_2O$) and DCPA (Dicalcium Phosphate Anhydrous: $CaHPO_4$) were developed when the prepared glass and glass-ceramic powders were mixed with three different solutions. The DCPD and DCPA transformed to HAp when the cement was soaked in Simulated Body Fluid (SBF), and this HAp formation strongly depended on the releasing capacity of $Ca^{2+}$ ions from the cements. The glass-ceramic containing apatite showed fast setting, but no HAp formation was observed because no $Ca^{2+}$ ions were released from this glass-ceramics. The compressive strength of the cements increased with reaction time in SBF until all DCPD and DCPA transformed to HAp.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2004.04a
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• pp.262-265
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• 2004

This study focused on the introduction of the self-healing technique for polymeric composites and evaluated the healing efficiency through the interlainar fracture toughness tests. The DCPD and ENB were used for a healing agent and the Grubbs' catalyst as a catalyst. The healing efficiency was evaluated by the use of mode I and the mode n fracture toughnesses. According to the results, the DCPD-ENB mixture with a suitable ratio revealed better healing efficiency than DCPD only.