• Title/Summary/Keyword: Cyclic treatment

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The Effects of Cyclic Heat Treatment Process for Fine Microstructure of TiAl Cast Alloy (주조용 TiAl 합금의 조직 미세화를 위한 반복열처리 공정 조건에 관한 연구)

  • Kong, Man-Sik;Yang, Hyunseok
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.5
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    • pp.195-200
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    • 2019
  • For expanding the applications and workability of TiAl alloy, elongation is very important property. Fine microstructure is needed for elongation and physical properties of TiAl alloys. In this study, The effects of cyclic heat treatment process for fine microstructure of Ti-46Al-Nb-W-Cr-Si-C alloy, which was made by VAR (vacuum arc remelting) and VIM(vacuum induction melting) centrifugal casting process, was investigated. Cycle heat treatment process was very effective for recrystallization of this TiAl system, which has microstructure size of $50{\sim}100{\mu}m$ through pre-heat treatment, cyclic heat treatment in ${\alpha}+{\gamma}$ phase region and solution heat treatment respectively. Refined grain size was finally confirmed by photos of optical microscope and scanning electron microscope.

Changes of Low Cycle Fatigue Behavior of AI-Mg-Si Alloy with Severe Plastic Deformation and Heat Treatment (강소성 가공 및 열처리에 의한 Al-Mg-Si합금의 저주기 피로특성변화)

  • Kim, W.H.;Kwun, S.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.22 no.4
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    • pp.217-222
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    • 2009
  • The effects of severe plastic deformation by equal channel angular pressing (ECAP) and subsequent heat treatment on the low cycle fatigue behaviors of Al-Mg-Si alloy were investigated. The specimens which were peak aged at $175^{\circ}C$ after solution treatment showed cyclic hardening at all strain amplitudes, while the specimens ECAPed after solution treatment showed cyclic softening at all strain amplitudes during fatigue. The specimens aged at $100^{\circ}C$ after ECAP showed slight cyclic hardening. Various changes of cyclic fatigue behavior after severe plastic deformation and/or heat treatment were discussed in terms of the microstructural changes and precipitation conditions.

Fatigue Behavior of 23Cr26Ni Heat Resistant Steel (23Cr26Ni 내열강의 피로 특성)

  • Lee, H.W.;Kwun, S.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.24 no.2
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    • pp.92-98
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    • 2011
  • The influence of the cooling condition after solution treatment on the high temperature fatigue resistance of 23Cr-26Ni heat resistant steel was investigated. Two different cooling conditions were applied to the steel after solution treatment at $1200^{\circ}C$ for 3 hours. One specimen was water quenched immediately after the solution treatment. The other one was furnace cooled at a rate of $0.5^{\circ}C/min$ down to $750^{\circ}C$ after the solution treatment. Then, both specimens were aged at $750^{\circ}C$ for 5 hours. Under two different heat treatment conditions, the low cycle fatigue (LCF) test was performed at $600^{\circ}C$ and room temperature (RT). Only cyclic hardening continued from the beginning until fracture at all strain amplitudes during LCF at $600^{\circ}C$. This phenomenon was attributed to the increase in the dislocation density due to cyclic deformation, which resulted in the interaction between the newly created dislocations and precipitates. Cyclic hardening followed by saturation and cyclic softening was observed at RT. Cyclic softening was attributed to the dislocation annihilation rate exceeding the dislocation generation rate. Other probable factor for cyclic softening was some cavities formed around grain boundaries after 20 cycles. WQ and FC have a similar LCF behavior at RT and $600^{\circ}C$ as shown in the cyclic stress response curves.

A Case Report of Cyclic Vomiting Syndrome in childhood by Sasang Constitution (주기성 구토 증후군 환아에 대한 증례보고)

  • Lee, Ji-Young;Jeong, Min-Jeong;Lee, Seung-Yeon
    • The Journal of Pediatrics of Korean Medicine
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    • v.20 no.1
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    • pp.85-91
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    • 2006
  • Objectives : The objectives of this study is a case report of Cyclic Vomiting Syndrome in childhood Methods : We experienced a child who ha diagnosed as Cyclic Vomiting Syndrome. We treated the patient with herb medicine, acupuncture and alimentotherapy of Sasang Constitution. Results : After the treatment of oriental medicine, the patient recovered from Cyclic Vomiting. Conclusions : We report one case of Cyclic Vomiting Syndrome in childhood the recovered after the treatment of Sasang Constitution. We think that the more follow-up is needed.

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Effect of Special the Heat Treatment on the Strength and Toughness in a Multi-phase(Ferrite-Bainite-Martensite) Ductile Cast Iron (3상(相) 혼합조직(混合組織) 구상흑연주철(球牀黑鉛鑄鐵)의 강인화(强引化)에 미치는 특수열처리(特殊熱處理)의 영향(影響)에 관(關)한 연구(硏究))

  • Choi, Hyun-Soo;Kim, Sug-Won
    • Journal of Korea Foundry Society
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    • v.9 no.6
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    • pp.463-473
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    • 1989
  • This study is aimed to investigate the effect of cyclic heat treatment which is special heat treatment on the strength and toughness in Multi-phase(Ferrite-Bainite-Martensite) Ductile cast Irons. Spceimens were austenitized at eutectoid transformation temperature range(${\alpha}+{\gamma}$) for 30min and austempered at $300^{\circ}C$ and $400^{\circ}C$ for different holding times, and then quenched in ice water to obtain the multi-phase(Ferrite-Bainite-Martensite) structure from various prior structures, which was obtained by various cyclic heat treatments. As the number of cycle in cyclic heat treatment increased, volume fraction of pearlite increased and the its morphology was refined. As the number of cycle in cyclic heat treatment increased, the multi-phase(Ferrite-Bainite-Martensite) was dispersed in whole matrix as refined island phase. Particularly, martensite among the multi-phase gradually became a spherical shape. Good combination in impact energy and tensile strength was detained in $840^{\circ}C-300^{\circ}C-15min$ condition after 10 cycles in cyclic heat treatment, and its multi-phase volume fraction is Ferrite(50%)-Martensite(l3%)-Bainite(37%).

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Cyclic Creep Properties of Nicoseal(Fe-29Ni-17Co) Alloy (Nicoseal(Fe-29Ni-17Co) 합금의 Cyclic 크리프 특성)

  • Park, Yong-Gwon;Choi, Jae-Ha
    • Journal of the Korean Society for Heat Treatment
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    • v.18 no.3
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    • pp.177-182
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    • 2005
  • The steady state cyclic mechanism, and the behaviour of Nicoseal(Fe-29Ni-17Co) have been examined under the condition of square wave stress cyclic tension creep test at the temperature, stress and frequency range of $430{\sim}470^{\circ}C$($0.41{\sim}0.43T_m$), 353~383 MPa, and 3 cpm, respectively. Also, the relationship between cyclic creep and static creep have been examined. The stress exponents(n) for the static creep deformation of this alloy were 11.6, 10.0, 8.4 and 7.9 at the temperature of 430, 445, 460 and $470^{\circ}C$, respectively. The apparent activation energies (Q) for the static creep deformation were 54.2, 51.8, 49.7 and 46.8 kcal/mole for the stress of 353, 363, 373 and 383 MPa, From the above results, it could be considered that the cyclic creep accelaration phenomena was obtained and that the cyclic deformation for Nicoseal seemed to be controlled by dislocation climb over the range of experimental conditions. Nicoseal alloy under the cyclic creep conditions was obtained as P=(T+460)(logt+17). The failure plane observed by SEM showed up transgranular fracture at all range.

A Characteristic of microstructural evolution, microhardness and tensile properties in CrMoV rotor steel weldment experienced by the cyclic thermal aging heat treatment (CrMoV강 용접부의 주기적 열시효처리에 따른 미세조직, 미세경도 및 인장강도 특성)

  • Kim, G.S.;Koh, J.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.12 no.4
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    • pp.303-312
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    • 1999
  • An investigation of the CrMoV rotor steel weldment which experienced by cyclic thermal aging heat treatment and as-received condition was performed. This evaluation was carried out to confirm whether this type of weldment is appropriate for the service environment in terms of microstructural examinations, microhardness measurements and tensile tests. The cyclic thermal aging heat treatment, containing continuous heating and cooling thermal cycle was programmed to simulate the real rotor service condition. The heat treatment was performed for 40 cycles(5920hrs). The results indicated that the weldment was composed of 4 different regions such as heat affected zone of the base metal, butter weld(initial weld), full thickness weld(final weld) and the base metal. The double welding process was applied to eliminate the susceptibility of reheat cracking at heat affected zone of base metal. The grain refinement at the HAZ due to the welding process could reduce the possibility of cracking susceptibility, but its tensile properties was appeared to be low due to the weld metal in as-received condition. The benefit effect, grain refinement was extended with carbides coarsening during the cyclic thermal aging heat treatment. However the poor mechanical properties of the weldment was more degraded as undergoing the heat treatment.

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The Microstructure Changes of Continuous Cast iron Rods According to the Heat-Treatment Conditions (열처리 조건에 따른 주철연속주조봉의 미세조직 변화)

  • Kim, Tae-Bong;Kim, Seon-Hwa;Park, Sang-Jun
    • Journal of Korea Foundry Society
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    • v.20 no.3
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    • pp.173-180
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    • 2000
  • The microstructure changes of the matrix and the graphites were observed by optical microscope and the average hardness number was investigated according to the heat-treatment conditions of the cast iron rods by the horizontal continuous casting process in 35 mm diameter. The three kinds of heat-treatments were introduced. The first treatment was performed at 900, 950, and $1000^{\circ}C$ for 2 hours and the second treatment was conducted during 5, 10, and 15 hours at $1000^{\circ}C$ respectively. The third treatments were the two-cyclic heat-treatment and the three-cyclic heat-treatment at $1000^{\circ}C$ during 2 hours. The matrix microstructure of the specimens to be treated at various temperatures for 2 hours was the ferrite to be transformed from the pearlite The hardness number of the center of the samples according to the heat treatment time at $1000^{\circ}C$ was higher than that of the surface area because of the martensite formation in the center. Also, in the cyclic heat-treatments, the hardness number of the two-cycle treatment specimens increased because of the martensite formation in the center.

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Removal Characteristics of Cyclic Ethers in Biological Wastewater Treatment System (고리형 에테르의 생물학적 처리 특성)

  • Lee, Sung-Ryul;Jeong, Yeon-Koo
    • Journal of Environmental Science International
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    • v.17 no.3
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    • pp.343-350
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    • 2008
  • The fate of two cyclic ethers, THF(Tetrahydrofuran) and 1,4-Dioxane, in conventional biological wastewater treatment plants was investigated using sequential activated sludge process. Removal efficiency of THF were about 86% in average, which was greater than that of 1,4-Dioxane, 30%. However, it was not clear whether the removal of cyclic ethers in biological system was caused by microbial activity or not. Thus treatability tests were conducted by batch experiments. The effects of mixing, aeration and the addition of activated sludge on the removal of cyclic ethers were investigated in batch experiments. THF was totally removed by mixing and aeration in 24 hours while removal ratio of 1,4-Dioxane was at most 30% for the same period. This results could be ascribed to the differences in Henry's law constants between the two chemicals. In addition, biological degradation including biosorption was not obviously observed in these batch tests.

Effect of Strengthening by Reverse Transformation of Ausformed Martensite and Marformed Martensite of Fe-31% Ni-0.2% C Alloy (Fe-31% Ni-0.2% C 합금(合金)의 오스폼드 마르텐사이트와 마르폼드 마르텐사이트의 역변태처리(逆變態處理)에 의한 강화효과(強化效果))

  • Kim, Byung Il
    • Journal of the Korean Society for Heat Treatment
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    • v.6 no.1
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    • pp.26-36
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    • 1993
  • In this study, the ausformed martensite and marformed martensite obtained from austenite with various deformation degrees in Fe-31% Ni-0.2%C alloy were transformed to revesed austenite at $510^{\circ}C$ by cyclic reverse martensite transformation. The effect of prior deformation, the rapid heating rate of reversion and number of cyclic transformation on the microstructure, mechanical properties of reversed austenite were investigated. The reverse austenite transformation is accomplised by the mechanism of shear type transformation. The structure of reversed austenite formed from ausformed martensite and marformed martensite with high deformation degrees is a fine structure of nearly equiaed grain containg a high density of dislocation tangles and was largely affected by the prior deformation applied before reversal transformation. The strength of reversed austenite is more increased with of cyclic transformation especially it is strength at the first cyclic transformation. The yield stress of revesed austenite of ausformed martensite is lower than that of marformed martensite.

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