• Title/Summary/Keyword: Cure Process

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Development of Pilot-Scale Manufacturing Process of SiC Fiber from Polycarbosilane Precursor with Excellent Mechanical Property at Highly Oxidation Condition and High Temperature (폴리카보실란 전구체로부터 고온 산화성분위기서 기계적물성이 우수한 파이롯-규모의 탄화규소섬유 제조공정 개발)

  • Yoon, B.I.;Choi, W.C.;Kim, J.I.;Kim, J.S.;Kang, H.G.;Kim, M.J.
    • Composites Research
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    • v.30 no.2
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    • pp.116-125
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    • 2017
  • The purpose of this study is to develop silicon carbide fiber showing an excellent mechanical properties under highly oxidative conditions at high temperature. Polycarbosilane(PCS) as a preceramic precursor was used for making the SiC fiber. PCS fiber was taken by melt spinning method followed by melting the PCS at $300{\sim}350^{\circ}C$ in N2 gas. The Curing of PCS fiber was carried out in air oxygen chamber, prior to high temperature pyrolysis. Degree of cure was calculated by characteristic peak's ratio of Si-H to $Si-CH_3$ in FT-IR spectra before and after curing of PCS fiber. The properties of SiC fiber was affected greatly by the degree of cure. The SiC fiber produced by controlling fiber tension during heat treatment showed good properties. The SiC fiber exposed to $1000^{\circ}C$ at air from 1 min. up to maximum 50 hrs showed around 60% reduction in tensile strength. We found that large amount of carbon content on the fiber surface after long-term exposure has resulted in lower tensile strength.

Effect of Polyethylene Glycol Treatment on the Wrinkle Resistance and the Dyeability of Cotton Fabrics (PEG 처리가 면질물의 방춘성 및 염색성에 미치는 영향)

  • 권영아
    • Journal of the Korean Society of Clothing and Textiles
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    • v.20 no.6
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    • pp.992-1001
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    • 1996
  • The binding of polyethylene glycol (PEG, average molecular weight 600) to cotton fabrics was achieved by using pad-dry-cure process in the presence of citric acid, MgCl3·6H3O, DMDHEU, and TEAHCL. Treated fabrics were dyed with direct, acid, and basic dye. Wrinkle recovery angles, durable press rate, wettability, dyeability and color fastness to washing of all treated cottons were evaluated. The results of this study were as follows: 1. The wrinkle resistance of the PEG treated cottons was increased by increasing PEG and DMDHEU concentration. 2. The wettability of the PEG treated cottons was decreased by increasing PEG and DMDHEU concentration, increased by increasing TEAHCL concentration. 3. PEG/DMDHEU/TEAHCL treated cottons had greater affinity on direct, acid, and basic dye than untreated cottons, and dyeability of the modified cottons was improved compare to untreated fabrics. 4. Color fastness to washing of the PEG/DMDHEU/TEAHCL treated cottons was good except for the wash fastness of the direct dye.

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A Study on the Development of Rolled Dry Floor Heating System for Improving Workability (현장 시공성 개선을 위한 롤타입 건식바닥난방시스템 개발)

  • Lee, Gyu-Dong;Kim, Jun-Ho;Jeong, Chang-Ho;Kim, Dong-Woo;Ogawa, Keiichiro
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2012.11a
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    • pp.177-180
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    • 2012
  • Korea residential housing generally use wet floor heating system 'Ondol' which consist of insulation cushioning, lightweight foamed concrete, hot water pipe and mortar on top of reinforced concrete slab. Wet floor heating system's installation process is too complicate and difficult to supervise field for continuing assurance quality. Also, this method has a huge impact on the progress of construction because it take a long time to cure finishing mortar and lightweight foamed concrete. Therefore, it is considered a disturbance factor of reduction of construction duration for enhancing competitiveness. In this study, we conducted an experiment about the radiant heat performance and temperature difference on upper panel of rolled dry floor heating systems which is jointly developed by Kolon global and Sumisho Metalex for remodeling housing, studio apartment and the urban-life housing.

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Detoxification Properties of Surface Aminated Cotton Fabric (아민화 표면 처리된 면직물의 제독 성능 연구)

  • Kim, Changkyu;Kwon, Woong;Jeong, Euigyung
    • Textile Coloration and Finishing
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    • v.32 no.2
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    • pp.73-79
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    • 2020
  • Pursuing the fabric materials for military chemical warfare protective clothing with the improved detoxification properties, this study investigated the simple and effective cotton treatment method using pad-dry-cure process and 3-aminopropyltrimethox ysilane(APTMS) solution for surface amination. Detoxification properties of the untreated and treated cotton fabrics were evaluated via decontamination of chemical warfare agent simulant, DFP(diisopropylfluorophosphate). The surface aminated cotton fabric increased the rate of the hydrolysis of DFP by the factor of 3 and the decontamination ratio reached 88.2% after 24h. Therefore, the surface amination of the cotton fabric with APTMS can be an effective pathway to prepare the material for protective clothing against chemical warfare agents.

Shrinkproof Finish of Viscose Rayon Fabric (비스코스 레이온 직물의 방축가공)

  • 김성동;이인열;이종렬;김민정
    • Textile Coloration and Finishing
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    • v.10 no.6
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    • pp.20-26
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    • 1998
  • 100% viscose rayon fabric was treated with 1,2,3,4-butanetetracarboxylic acid (BTCA) by pad-dry-cure process in the presence of various catalysts. The dimensional stability, mechanical properties and hand values of fabric treated with BTCA were investigated. The ester-crosslinking reaction was influenced by the concentration of BTCA and type of catalyst. The fabric treated with BTCA was comparable or superior to that treated with conventional crosslinking agents such as dimethyloldihydroxyethyleneurea and 4,5-dihydroxy-1,3-dimethyl-2-imidazolidinone in respect of wrinkle recovery, shrinkproof property, retention of strength, and hand values. But in yellowing of fabric, the fabric treated with BTCA was inferior to that treated with conventional crosslinking agents. The fabric treated with BTCA/sodium formate was inferior to that treated with BTCA/sodium hypophosphite in respect of WRA, but had better strength retention and whiteness.

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The effect of micro/nano-scale wafer deformation on UV-nanoimprint lithography using an elementwise patterned stamp (다중양각스탬프를 사용하는 UV 나노임프린트 리소그래피공정에서 웨이퍼 미소변형의 영향)

  • 정준호;심영석;최대근;김기돈;신영재;이응숙;손현기;방영매;이상찬
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.1119-1122
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    • 2004
  • In the UV-NIL process using an elementwise patterned stamp (EPS), which includes channels formed to separate each element with patterns, low-viscosity resin droplets with a nano-liter volume are dispensed on all elements of the EPS. Following pressing of the EPS, the EPS is illuminated with UV light to cure the resin; and then the EPS is separated from several thin patterned elements on a wafer. Experiments on UV-NIL were performed on an EVG620-NIL. 50 - 70 nm features of the EPS were successfully transferred to 4 in. wafers. Especially, the wafer deformation during imprint was analyzed using the finite element method (FEM) in order to study the effect of the wafer deformation on the UV-NIL using EPS.

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Characterization of Stitched Multiaxial Warp Knit Fabric Composites and Channel Beam Manufacturing (Stitched 다축경편 복합재료의 기계적 특성 및 U 빔 성형)

  • 변준형;이상관;엄문광;김태원;배성우;하동호
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.10a
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    • pp.280-283
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    • 2002
  • In the manufacturing of large scale composite structures, the cost-effective processing and the enhancement of structural performance are critical. One of the most effective ways for this purpose is to use stitched multiaxial warp knitted (MWK) perform in the resin transfer molding process. This study reports the effect of stitching on the mechanical properties of MWK composites, and the feasibility processing of the thick U-beam structure utilizing the stitched preforms. Permeability of the preform, viscosity and cure property of the epoxy resin have been measured. The results of resin flow analysis has been used in determining the gate/vent locations of the RTM mold. Cross-sectional observation of the channel beam prototype demonstrated that the resin impregnation was almost complete, except for some surrounding area of stitched yarns.

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Development of PC-based Radiation Therapy Planning System

  • Suh, Tae-Suk;P task group, R-T
    • Proceedings of the Korean Society of Medical Physics Conference
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    • 2002.09a
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    • pp.121-122
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    • 2002
  • The main principle of radiation therapy is to deliver optimum dose to tumor to increase tumor cure probability while minimizing dose to critical normal structure to reduce complications. RTP system is required for proper dose plan in radiation therapy treatment. The main goal of this research is to develop dose model for photon, electron, and brachytherapy, and to display dose distribution on patient images with optimum process. The main items developed in this research includes: (l) user requirements and quality control; analysis of user requirement in RTP, networking between RTP and relevant equipment, quality control using phantom for clinical application (2) dose model in RTP; photon, electron, brachytherapy, modifying dose model (3) image processing and 3D visualization; 2D image processing, auto contouring, image reconstruction, 3D visualization (4) object modeling and graphic user interface; development of total software structure, step-by-step planning procedure, window design and user-interface. Our final product show strong capability for routine and advance RTP planning.

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A bibliographic study on the Talyoung-Siljeong(脫營失精) (탈영실정(脫營失精)의 문헌적(文獻的) 고찰(考察))

  • Ryu Hui-Yeong;Lee Seok-Jun
    • Journal of Oriental Neuropsychiatry
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    • v.1 no.1
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    • pp.21-38
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    • 1990
  • In this study, the bibliographic classification, pathogeny, symptoms, therapeutics and prescriptions of Talyoung-Siljeong(脫營失精) were researched. Reference to consult about its origin and the process of development showed the following results. 1. It was 1117 that the difference between Talyoung-Siljeong(脫營失精) began to appear for the first time in classical literatures. 2. In view of psychological side, it is suitable for siljeong(失精), the part of Talyoung-Siljeong(脫營失精), to be called Taljeong(脫精). 3. Taljeong-Siljeong(脫營失精) was broken out by the internal factors. 4. Silyoung(失營) and Silyoung jeo(失營疽) are the worse states of Talyoung(脫營) and result in the incurable diseases. 5. Hypochondria and diaster psychology can be cured by the therapeutics of Talyoung-Siljeong(脫營失精). 6. Prescription for Heoro-Talyoung(虛勞脫營) can be used in cure of Talyoung(脫營). Talyoung-Siljeoung(脫營失精) remarked in traditional oriental meicine is recognized to belong to the part of stress in mordern medicine. It is thought that the experimental investigation should be continued.

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An Estimation on Characteristics of SOG Film for MEMS Application (MEMS 응용을 위한 SOG 막의 특성 평가)

  • Kim, Hyoung-Dong;Lee, Seong-Jun;Pack, Seung-Ho;Kim, Chul-Ju
    • Proceedings of the KIEE Conference
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    • 1995.11a
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    • pp.609-611
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    • 1995
  • In this study, we experimented the properties of SOG film as sacrificials layers in surface micromachining and made $SiO_2$ films through spin, bake, cure process. When we culled SOG films once, SOG film thickness is 1000 $\sim$ 3000 ${\AA}$. Then we coaled 200-${\AA}$ SOG film on 9000 ${\AA}$-CVD oxide and then we fabricated test structure, cantilever and ring/beam structure. We estimated deformed structure by SEM. As the results, The deformation of the structure layer in the SOG-coated sacrificial layers is small compared with that or the structure layer on CVD oxide or PSG. In the future, we use multi coated SOG films, SOG film become adequate material as sacrificial layer.

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