• Title/Summary/Keyword: Crystallinity rice

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Factors Affecting Gelatinization Temperature of Rice Starch (쌀 전분의 호화온도에 영향을 주는 요인들)

  • 이영은;오스만엘리자베쓰엠
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.20 no.6
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    • pp.646-652
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    • 1991
  • Factors affecting gelatinization temperature of rice starches from different varieties were investigated. Birefringence end-point temperature(BEPT), amylose content, granule size distribution and degree of crystallinity of rice starches showed the significant varietal differences at ${\alpha}\;=0.01$. Susceptibility of the granule to gelatininzation was dependent mainly on the degree of crystallinity, as indicated by the significant positive correlation between BEPT and the relative crystallinity(r=0.67, p<0.01). However, granule size distribution did not affect the GT(gelatinization temperature) range, nor did amylose electron microscopy (SEM). SEM also confirmed that there is no relationship between the size and the shape and the amylose content of the rice starch.

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Effect of Transplanting Time on the Physicochemical Properties of Starch in Different Mature Rice Varieties

  • Jong-Hee Shin;Chae-Min Han;Young-Un Song;Sang-Kuk Kim;Jung-Gi Ryu
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.68 no.2
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    • pp.35-46
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    • 2023
  • The transplanting period limit considering the rice yield in the Dague region, the inland plains of Gyeongsangbuk-do, was estimated to be July 15th for early and mid-maturing rice and July 5th for mid-late maturing rice. However, as the transplanting time was delayed, the characteristics of rice starch changed significantly. In the case of early and mid-maturing rice varieties, the starch granule size increased as the transplanting time was delayed; the opposite tendency was observed for mid-late maturing varieties. In all mature rice types, the late transplanting resulted in a longer pasting time and a higher pasting temperature. In addition, the peak viscosity, breakdown, and gelatinization temperature were significantly lowered, the relative crystallinity degree decreased, and the setback was significantly increased. In the case of Ilpum, a mid-late maturing rice variety, the distribution of amylopectin short chains tended to increase when rice was transplanted on June 30th.

Granular Morphology and Thermal Properties of Acid-Hydrolyzed Rice Starches with Different Amylose Contents (아밀로스 함량이 다른 쌀 전분으로 산 가수분해 처리된 입자의 형태적 및 열적 특성)

  • No, Junhee;Lee, Chae Eun;Shin, Malshick
    • Korean journal of food and cookery science
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    • v.33 no.3
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    • pp.307-315
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    • 2017
  • Purpose: To develop nano-sized starch particles for application as dietary fiber sources in liquid food system, the morphology and thermal properties of acid hydrolyzed rice starches with different amylose contents were evaluated. Methods: Rice starches purified from three Korean cultivars, including Goami, Hopyeong, and Hwaseonchal, were hydrolyzed with 2.2 N HCl solution in a $35^{\circ}C$ shaking water bath (100 rpm) for 7, 10 and 15 days. Results: Acid hydrolysis rates of rice starches increased with increasing hydrolysis duration, and rates for Goami, Hopyeong, and Hwaseonchal were 28.74-38.50%, 38.96-49.53%, and 40.24-48.88%, respectively. The granular size of acid hydrolyzed starches decreased to 122.4-479.9 nm, whereas granular aggregation increased with increasing hydrolysis duration. In particular, waxy rice starch of Hwaseonchal was composed of many tiny granules without aggregates. Gelatinization temperature and temperature range increased with increasing hydrolysis duration. All starches showed A type crystallinity using an x-ray diffractometer, regardless of acid hydrolysis. Conclusion: It is suggested that nanoparticles could be prepared by acid hydrolysis of rice starches, and waxy rice starch is the most preferred source for application.

Effects of Panicle Position and Planting Density on the Physicochemical Properties of Starch in Panicle Number Type Rice

  • Han, Chae-Min;Shin, Jong-Hee;Kwon, Jung-Bae;Kim, Sang-Kuk;Won, Jong-Gun;Ryu, Jung-Gi
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.67 no.3
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    • pp.155-163
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    • 2022
  • The tillering potential of panicle number type (PNT) rice greatly varies with planting density. Moreover, grain filling and ripening differ depending on the panicle position, which may further affect rice grain quality. The present study evaluated the grain quality of PNT rice sparsely planted to reduce production costs. The physicochemical characteristics of starch from the grains of PNT type rice 'Ilpum' planted at different densities (37, 50, 60, and 80 plants/3.3 m2) and at different positions of panicles (upper or lower on the culm) were determined. Overall, as the planting density decreased, the number of panicles increased but the starch content decreased, which further reduced the 1,000-grain weight. In particular, at the lowest density (37 plants/3.3 m2), protein content increased but particle size, enthalpy, and relative crystallinity decreased. The effects were more pronounced at lower than at upper panicle positions. These findings indicate that tillering potential differs with planting density, ultimately affecting the palatability of rice grains. Based on these findings, we propose restricting rice transplantation to a planting density of ≤37 plants/3.3 m2 to achieve the best quality of grains at lower costs and with less labor.

Interrelationship between Amylose Content and Physical Properties of Milled Rice (쌀의 아밀로스 함량과 물리적 특성간의 상호관계)

  • Kim, Sung-Kon;Chae, Je-Cheon;Lim, Moo-Sang;Ree, Jung-Haeng
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.30 no.3
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    • pp.320-325
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    • 1985
  • Relation between amylose and physical properties of milled rice was investigated. Amylose content was negatively and positively correlated with chalkiness and alkali solubility, respectively. No correlation was observed between amylose content and water uptake rate, cooked rice hardness or relative crystallinity. Relative crystallinity of the starch was negatively correlated with alkali solubility and water uptake rate.

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Effect of Aging on Physicochemical and Pasting Properties of Nonwaxy Rice Flour and its Starch (쌀의 저장기간에 따른 쌀가루와 생전분의 특성)

  • Kim, Wan-Soo
    • Korean Journal of Human Ecology
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    • v.14 no.6
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    • pp.1037-1046
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    • 2005
  • Using three consecutive years' harvested rices and their starches isolated from rice flours by alkaline method, it was found that no significant aging effect on rice flour and starch was observed based on following results. Proximate data of flours or starches showed in similarity, except high level of crude fat in rice flour and rice starch harvested in 2002. In SEM, the surface of aged rice flour had slightly layered shape due to possible abrasion during storage, and that of aged starch showed more smooth and less rigid polygonal shape. X-ray diffraction patterns of flours and starches were all A type, and crystallinity of rice starch harvested in 2000 had the smallest. From tristimulus colorimetry (Hunterlab Color), total color difference ($\Delta$E) calculated from L, a, and b gave less color difference with the darkest in 2002 harvested one among flours and the lightest in 2001 one among starches. WBCs of both 2002 rice flour and starch were the lowest among samples studied. At 80$^{\circ}C$, swelling power and solubility of rice starches harvested in 2000, 2001 and 2002 were 14.35, 9.75; 14.04, 9.6; and 12.49, 8.82, respectively. The highest peak viscosities measured by RVA were shown both in 2001 rice flour and in its starch. Starch and milled rice flour harvested in 2000 had higher hydrolytic $\alpha$-amylase, compared to other flour and starch samples.

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Physicochemical Properties of High Yielding Non-waxy Rice Flours Extruded with Different Moisture Contents (다른 수분함량으로 압출성형한 다수확 멥쌀가루의 이화학적 특성)

  • Jeong, So-Hee;Kang, Wie-Soo;Shin, Mal-Shick
    • Korean journal of food and cookery science
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    • v.27 no.6
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    • pp.745-754
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    • 2011
  • To improve the textural properties of gluten free rice flour based products, the physicochemical and pasting properties of extruded non-waxy rice flours using extruder were investigated. The high yielding Tongil type rice variety, Hanarum was used. Hanarum rice flour was prepared by dry milling from soaked and dried rice grain. The operation conditions of twin screw extruder were 250 rpm of screw speed, $160^{\circ}C$ of barrel temperature, and 24, 27, and 30% of moisture content. Hanarum extruded rice flour (HERF) were lower in crude lipid and ash contents, but higher in crude protein than Hanarum rice flour (HRF). The color values of HERF showed significantly different (p<0.05) with different moisture contents. Water binding capacities, apparent amylose contents, and damaged starch of HERF were higher than those of HRF. Moisture contents affected water binding capacities of HERF. Solubility increased with increasing heating temperature and solubilities of HERF differed significantly (p<0.05). X-ray crystallinity was changed after extrusion cooking and that of HERF showed sharp peaks at $2{\theta}=18-20^{\circ}$. The pasting viscosities of HERF kept lower values (~ 10 RVU) constantly.

Effect of chemical input during wet air oxidation pretreatment of rice straw in reducing biomass recalcitrance and enhancing cellulose accessibility

  • Morone, Amruta;Chakrabarti, Tapan;Pandey, R.A.
    • Korean Journal of Chemical Engineering
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    • v.35 no.12
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    • pp.2403-2412
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    • 2018
  • The present study was aimed at evaluating the effect of variable sodium carbonate ($Na_2CO_3$) loading during wet air oxidation (WAO) pretreatment of rice straw in reducing biomass recalcitrance. The research study was intended to increase the cellulose recovery, hemicellulose solubilization, lignin removal in the solid fraction and limiting the generation of inhibitors in the liquid fraction while reducing the chemical input. The operating condition of $169^{\circ}C$, 4 bar, 18 min and 6.5 g/L $Na_2CO_3$ loading resulted in maximum cellulose recovery of 82.07% and hemicellulose solubilization and lignin removal of 85.43% and 65.42%, respectively, with a total phenolic content of 0.36 g/L in the liquid fraction. The crystallinity index increased from 47.69 to 51.25 along with enzymatic digestibility with an increase in $Na_2CO_3$ loading from 0 to 6.5 g/L as a result of removal of barriers for saccharification via effective cleavage of ether and ester bonds cross-linking the carbohydrates and lignin as indicated by FT-IR spectroscopy. A further increase in the $Na_2CO_3$ loading to 9.5 g/L did not significantly increase the sugar release. Thus, it was concluded that 6.5 g/L $Na_2CO_3$ during WAO is sufficient to increase the delignification and deacetylation, leading to significant changes in apparent cellulose crystallinity inter alia improvement in cellulose accessibility and digestibility of rice straw.

Properties of Rice Flours Prepared from Domestic High Amylose Rices (국내산 고아밀로오스 쌀가루의 특성)

  • Choi, Sin-Young;Shin, Mal-Shick
    • Korean Journal of Food Science and Technology
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    • v.41 no.1
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    • pp.16-20
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    • 2009
  • To develop health functional foods using high amylose rice flours, the properties of flours prepared from domestic high amylose rice varieties, Goamy2 and Goamy, and imported rice from Thailand were investigated. After soaking the rice grains and drying, the dry-milled rice flours were passed through a 120-mesh sieve. The protein and total starch contents of the Goamy2 rice flour were lowest, but its crude lipid and ash contents were highest among the flours. In addition, apparent amylose content, water binding capacity, and total dietary fiber were highest in the Goamy2 flour (36.2, 255.0, and 9.2%, respectively). The Thai rice flour had the highest swelling power, whereas the Goamy2 flour had the lowest swelling power and solubility. By Rapid visco-analysis, the Thai flour showed the highest peak and total setback viscosities and lowest breakdown viscosity. The pasting pattern of the Goamy2 flour was different from that of the other flour, where low viscosity was maintained during heating and cooling. Goamy and Thai rice flours showed an A type crystallinity, but Goamy2 flour showed a B type crystallinity similar to high amylose maize starch. The Goamy2 flour presented a dull and yellowish color, and the lowest lightness (L) value and the highest yellowness (+b) value.

Effect of Defatting on Hydration of Akibare (Japonica) and Milyang 30 (J/lndica) Rice (탈지에 따른 아끼바레 및 밀양30호 쌀의 수화속도)

  • Kim, Soon-Mi;Kim, Kwang-Ok;Kim, Sung-Kon
    • Korean Journal of Food Science and Technology
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    • v.18 no.2
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    • pp.110-113
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    • 1986
  • Effect of defatting on the hydration rate of Akibare (Japonica) and Milyang 30 (J/lndica) rice was investigated. Relative crystallinity of rice starch and width of the rice grain were decreased by defatting, which was more pronounced for Milyang 30. The moisture gain at $10^{\circ}{\sim}40^{\circ}C$ for 80 min and the hydration rate of the defatted Milyang 30 rice were lower and higher than those of the defatted Akibare rice, respectively. The activation energy for hydration of rice was not affected by defatting.

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