• Title/Summary/Keyword: Crystal size

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Control system with neural networks for product crystal size of sodium chloride

  • Shinto, Toshiharu;Ishimaru, Naoyuki
    • 제어로봇시스템학회:학술대회논문집
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    • 1994.10a
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    • pp.725-730
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    • 1994
  • A sodium chloride crystallizer shows oscillatory and nonlinear characteristics under its nucleating and growing process. Because these characteristics vary with operational condition, we can't control the product crystal size exactly with a PID controller or a sequence controller. Then, we make a model with threefold neural networks for the laboratory equipment that is a jet mixing crystallizer. We try to control the product crystal size with its neuro-model, and we reach the conclusion that our neuro-model is applicable to the practical crystallizer.

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Start-up dynamics in a CMSMPR crystallizer (CMSMPR 결정화기의 시동 특성 연구)

  • 신영준;이철수
    • 제어로봇시스템학회:학술대회논문집
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    • 1986.10a
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    • pp.200-204
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    • 1986
  • Particle size distribution in a Continuous Mixed Suspension Mixed Crystal Removal (CMSMPR) crystallizer has been analyzed using the Population Balance (PB) model. This method presents difficulties when the growth rate of crystal depends on the crystal size. Recent studies indicate that in many cases the growth rate is dependent on size when the crystal sizes are small. In this study, a Residence Time Distribution(RTD) model was proposed to take the size dependence into account together with an appropriate numerical scheme. When compared with the approximate results based on PB model, RTD model results showed improvements also a nucleation effect which is normally unimportant for steady state analysis. Start-up data for NaCl-Water-Ethanol system was compared with computed values.

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Preparation of particle-size-controlled SiC powder for single-crystal growth

  • Jung, Eunjin;Lee, Myung Hyun;Kwon, Yong Jin;Choi, Doo Jin;Kang, Seung Min;Kim, Younghee
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.27 no.1
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    • pp.57-63
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    • 2017
  • High-purity ${\beta}-SiC$ powders for SiC single-crystal growth were synthesized by direct carbonization. The use of high-purity raw materials to improve the quality of a SiC single crystal is important. To grow SiC single crystals by the PVT method, both the particle size and the packing density of the SiC powder are crucial factors that determine the sublimation rate. In this study, we tried to produce high-purity ${\beta}-SiC$ powder with large particle sizes and containing low silicon by introducing a milling step during the direct carbonization process. Controlled heating improved the purity of the ${\beta}-SiC$ powders to more than 99 % and increased the particle size to as much as ${\sim}100{\mu}m$. The ${\beta}-SiC$ powders were characterized by SEM, XRD, PSA, and chemical analysis to assess their purity. Then, we conducted single-crystal growth experiments, and the grown 4H-SiC crystals showed high structural perfection with a FWHM of about 25-48 arcsec.

The Influence of Food Hydrocolloids on Changes in the Physical Properties of Ice Cream

  • Park, Sung-Hee;Hong, Guen-Pyo;Kim, Jee-Yeon;Choi, Mi-Jung;Min, Sang-Gi
    • Food Science and Biotechnology
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    • v.15 no.5
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    • pp.721-727
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    • 2006
  • This study was carried out to investigate the effect of hydrocolloids on the changes in physical properties of a model ice cream. The model ice cream contained water, sugar, skin milk powder, com oil, and 4 different hydrocolloid stabilizers (gelatin, pectin, hydroxyethylstarch, locust bean gum), was manufactured in a batch type freezer. The following physical characteristics of ice cream were examined: flow behavior, overrun, air cell size, ice crystal size, and melt resistance. With regard to flow behavior, all of aged mixes had a lower apparent viscosity relative to the mix before aging, and ice cream mix containing locust bean gum had the highest viscosity. Air cell size was observed to range from 20 to $38\;{\mu}m$, and ice cream with locust bean gum showed the largest size. There was an inverse correlation between overrun and air cell size. The ice crystal sizes of all samples ranged from 25 to $35\;{\mu}m$. Ice cream with added pectin contained the smallest ice crystal size, which was significantly difference from other stabilizers (p<0.05), and resulted in superior melt resistance with increased melting time compared to other samples.

Effect of pH level and slurry particle size on the chemical mechanical planarization of langasite crystal wafer (pH level 및 slurry 입도가 langasite wafer의 chemical mechanical planarization에 미치는 영향)

  • Cho Hyun
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.15 no.1
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    • pp.34-38
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    • 2005
  • Effects of pH level and slurry particle size on material removal rate and planarization of langasite single crystal wafer have been examined. Higher material removal rate was obtained with lower pH level slurries while the planarization was found to be determined by average particle size of colloidal silica slurries. Slurries containing 0.045 ㎛ amorphous silica particles showed the best polishing effect without any scratches on the surface. Effective particle number has a strong effect on the surface planarization and the removal rate, so that the lower effective particle numbers produced low removal rate but the better planarization results.

Relationship between Surface Roughness and Crystal size of Li2O-Al2O3-SiO2(LAS) Glass-Ceramic System (Li2O-Al2O3-SiO2(LAS)계 결정화유리에서 결정크기와 표면조도 관계)

  • Kim Yu Jin;Hwang Seong Jin;Kim Hyung Sun
    • Korean Journal of Materials Research
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    • v.14 no.7
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    • pp.505-510
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    • 2004
  • The glass-ceramic based on LAS($Li_{2}O-Al_{2}O_3-SiO_{2}$) system was observed using SEM(Scanning Electric Microscopy) and AFM(Atomic Force Microscopy) and it was expected to get a correlation between the crystal size and the surface roughness through the result. At heat treatment conditions (the nucleation: $740\~800^{\circ}C$, the crystal growth: $900\~1150^{\circ}C$), the crystal size was increased from 72 to 450 nm so that the mean of surface roughness was also risen from 0.8 to 6.3 nm. Based on the results, the surface roughness of glass-ceramic is controlled by the factors, crystal size, crystallines, and the condition of heat treatment.

Preparation and Properties of a Complex Crystal for Nonlinear Optical Applications: Cadmium mercury Thiocyanate

  • Jiang, Minhua;Yuan, Dourong;Liu, Mingguo;Xu, Dong
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1996.06a
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    • pp.375-398
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    • 1996
  • A complex nonlinear optical crystal Cadmium Mercury Thiocyanate with size 18*18*20mm3 was grown. It possesses chemical stability below 247$^{\circ}C$, no cleavage, and high mechanical strength. Blue light second harmonic of diode laser was realized.

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A Study on Analysis for Bulk Forming of a Single Crystal Milli-Product (단결정 밀리 부품의 입체성형 해석에 관한 연구)

  • Lee Y. S.;Kim Y. I.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2001.05a
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    • pp.245-249
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    • 2001
  • This paper is concerned with numerical analyses for bulk forming of a single crystal milli-product, whose typical size ranges from a few hundreds ${\mu}m$ to a few mm. The numerical formulation invoked in this paper combines the crystal plasticity theory considering texture development and the ductile damage mechanics for growth of micro voids, since orientation development and growth of micro voids become the primary factors for bulk forming of milli-size products. As applications, milli-extrusion of a single crystal round bar and milli-rolling of a single crystal plate are simulated and the results are discussed in detail.

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Mechanical Behavior and Microstructure Evolution during Semi-Solid Squeeze Cast Processing of Ignition-Proof Mg-Zn-Ca-Zr Alloy

  • Chang, Si-Young;Choi, Jung-Chul
    • Journal of Korea Foundry Society
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    • v.17 no.5
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    • pp.502-509
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    • 1997
  • The mechanical behavior and microstructural evolution in the ignition-proof Mg-Zn-Ca-Zr alloy produced by the semisolid squeeze casting are clarified and the mechanical properties are also compared with those of squeeze cast Mg-Zn-Ca-Zr alloy. The tensile strength and elongation increase slightly as the solid fraction depending on temperature decreases, while the 0.2% proof stress decreases. The size of primary crystal increases with increasing holding time. The tensile strength and 0.2% proof stress of the semi-solid squeeze cast Mg-Zn-Ca-Zr alloy decrease as the size of primary crystal increases, indicating the dependence of strength on the size of primary crystal. The elongation of the semi-solid squeeze cast Mg-Zn-Ca-Zr alloy is two times as large as the squeeze cast Mg-Zn-Ca-Zr alloy and the tensile strength is unchanged despite the growth of primary crystal, resulting from the refining of the melted ${\alpha}Mg$ phase and the brittle eutectic compound as well as the reduction of solidification shrinkage and porosities.

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The Evaluation of Multiplane-Parallel Chamber Using Crystal Plate as Ionization Medium for Therapeutic Radiation Beams

  • Young W. Vahc;Park, Kyung R.;Kim, Sookil;Chul W. Joh;Kim, Tae H.
    • Progress in Medical Physics
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    • v.9 no.1
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    • pp.29-35
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    • 1998
  • There has been necessity of an air free ionization chamber using the gold-crystal-aluminium plates, henceforth called the crystal chamber. The crystal chamber formed of parallel plates is very small in size and has more response for absorbed dose of therapeutic radiation beams. The gold plate on the crystal facing the photon and electron beam acts as an intensifier of signals and crystal plate as an ionization medium respectively. Both the copper guard ring and the aluminum collecting electrode are connected to an electrometer. Using high energy photon (6, 15 MV) and electron (9, 12, 15, 18 MeV) beams, the responses of the crystal chamber are evaluated against a PTW Farmer-type chamber at a field size of 10${\times}$10cm$^2$ and 100 cm SSD. The responses of crystal chamber for therapeutic radiation electron and photon beams are greater in magnitude by several order than Farmer. The crystal chamber has good linearity without correction factor C$\_$t,p/ with respect to the signals, a reading reproduction with good accuracy and precision less than 0.5%, and has other useful functions in measuring radiation beams.

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