• Composites Research
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• v.17 no.6
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• pp.52-57
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• 2004

In this study, mechanical tensile properties of carbon fiber reinforced polymeric (CFRP) composite cycled with thermo-mechanical loading under cryogenic temperature (CT) were measured using cryogenic environmental chamber. Thermo-mechanical tensile cyclic loading (up to 10 times) was applied to graphite/epoxy unidirectional laminate composites far room temperature (RT) to $-50^{\circ}C$, RT to $-100^{\circ}C$ and RT to $-150^{\circ}C$. Results showed that tensile stiffness obviously increased as temperature decreased while the thermo-mechanical cycling has little influence on it. Tensile strength, however, decreased as temperature down to CT while the reduction of strength showed little after CT-cycling. For the analysis of the test results, coefficient of thermal expansion (CTE) of laminate composite specimen at both RT and CT were measured and the interface between fiber and matrix was observed using SEM images.

• Composites Research
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• v.26 no.2
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• pp.129-134
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• 2013

The strength of adhesive joints employed in composite structures under cryogenic environments, such as LNG tanks, is affected by thermal residual stress generated from the large temperature difference between the bonding process and the operating temperature. Aramid fibers are noted for their low coefficient of thermal expansion (CTE) and have been used to control the CTE of thermosetting resins. However, aramid composites exhibit poor adhesion between the fibers and the resin because the aramid fibers are chemically inert and contain insufficient functional groups. In this work, electrospun meta-aramid nanofiber-reinforced epoxy adhesive was fabricated to improve the interfacial bonding between the adhesive and the fibers under cryogenic temperatures. The CTE of the nanofiber-reinforced adhesives were measured, and the effect on the adhesion strength was investigated at single-lap joints under cryogenic temperatures. The fracture toughness of the adhesive joints was measured using a Double Cantilever Beam (DCB) test.

• Korean Journal of Materials Research
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• v.31 no.9
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• pp.519-524
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• 2021

The impact properties of two austenitic Fe-23Mn-0.4C steels with different Al contents for cryogenic applications are investigated in this study. The 4Al steel consists mostly of austenite single-phase microstructure, while the 5Al steel exhibits a two-phase microstructure of austenite and delta-ferrite with coarse and elongated grains. Charpy impact test results reveal that the 5Al steel with duplex phases of austenite and delta-ferrite exhibits a ductile-to-brittle transition behavior, while the 4Al steel with only single-phase austenite has higher absorbed energy over 100 J at -196 ℃. The SEM fractographs of Charpy impact specimens show that the 4Al steel has a ductile dimple fracture regardless of test temperature, whereas the 5Al steel fractured at -100 ℃ and -196 ℃ exhibits a mixed fracture mode of both ductile and brittle fractures. Additionally, quasi-cleavage fracture caused by crack propagation of delta-ferrite phase is found in some regions of the brittle fracture surface of the 5Al steel. Based on these results, the delta-ferrite phase hardly has a significant effect on absorbed energy at room-temperature, but it significantly deteriorates low-temperature toughness by acting as the main site of the propagation of brittle cracks at cryogenic-temperatures.

• Journal of the Society of Naval Architects of Korea
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• v.58 no.2
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• pp.66-72
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• 2021

As the demand for natural gas that satisfies environmental regulations increases, the quantities of natural gas cargo that carrier can load is also increasing. Natural gas is transported in a liquefied state at -163 ℃ to increase loading efficiency. Among several LNG CCS types, MARK-III types are generally adopted in terms of loading efficiency. The secondary barrier adhesives of the MARK-III, nevertheless, is subjected to tensile stress due to thermal contraction and tension in the environment. In terms of these reasons, local analysis of the adhesive to evaluate the stress state must be carried out. According to previous studies, local analysis is unavailable since material properties for secondary barrier adhesives have not been reported. Thus, in this study, the cryogenic tensile test and coefficient of thermal expansion of epoxy and polyurethane (PU15, PU45), which are most widely used at cryogenic temperatures, were experimentally analyzed. At cryogenic temperature, the mechanical behavior of the polyurethane adhesive was better than epoxy of the adhesive. the joint of FSB and epoxy adhesive of the secondary barrier has the maximum coefficient of thermal expansion difference at 25 ℃ and minimum at -150 ℃, respectively.

• Composites Research
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• v.20 no.4
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• pp.1-8
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• 2007

In this study, carbon fiber reinforced polymeric (CFRP) composites with different resin composition were manufactured and resin formulation in composite materials were presented through tensile tests for cryogenic use. Thermo-mechanical cyclic loading (up to 6 cycles) was applied to CFRP unidirectional laminate specimens from room temperature to $-150^{\circ}C$. Tensile tests were then performed at $-150^{\circ}C$ using an environmental test chamber. In addition, matrix-dominant properties such as the transverse and in-plane shear characteristics of each composite model were measured at $-150^{\circ}C$ to examine the effects of resin formulation on their interfacial properties. The tensile tests showed that the composite models with large amounts of bisphenol-A epoxy and CTBN modified rubber in their resin composition had good mechanical performance at cryogenic temperature (CT).

• Aerospace Engineering and Technology
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• v.12 no.2
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• pp.83-90
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• 2013

In this paper, the energy flows related to cryogenic propellant tank ullage were understood and pressurization efficiency of the tank was calculated using propellant feeding test data with the help of calculation program. The related energy flow terms and calculation method of each terms were described. Three test data of different tank pressure and incoming pressurant temperature were used. Under the test conditions, the pressurization efficiency was low in the range of 13.9%~19.3%. The proportion of energy loss to the incoming pressurant energy was in the range of 55.2%~67.6%. The energy loss to the propellant tank wall was the biggest one. If the temperature of incoming pressurant was the same, the rates of each energy flows to the incoming energy were almost the same regardless of the propellant tank pressure. The collapse factor of propellant tank was calculated using test data, and the relation of it to the heat loss rate was observed.

• Advances in materials Research
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• v.13 no.3
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• pp.183-194
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• 2024

D3 tools steel and 440C stainless steel (SS) are normally being employed for application such as knife blade and cutting tools. These steels are iron alloys which have high carbon and high chromium content. In this study, lab work focused on the microstructural and corrosion behavior of D3 tools steel and 440C SS after went through heat treatment processes. Heat treatments for both steels were started with normalizing at 1020 ℃, continue with hardening at 1000 ℃followed by oil quenching. Cryogenic treatment was carried out in liquid nitrogen for 24 hours. The addition of cryogenic heat treatment is believed to increase the hardness and corrosion resistance for steels. Both samples were then tempered at two different tempering temperatures, 160 ℃ and 426 ℃. For corrosion test, the samples were immersed in NaCl solution for 30 days to study the corrosion behavior of D3 tool steel and 440C SS after heat treatment. The mechanical properties of these steels have been investigated using Rockwell hardness machine before heat treatment, after heat treatment (before corrosion) and after corrosion test. Microstructure observation of samples was carried out by scanning electron microscopy. The corrosion rate of these steels was calculated after the corrosion test completed. From the results, the highest hardness is observed for D3 tool steel which tempered at 160 ℃(54.1 HRC). In terms of microstructural analysis, primary carbide and pearlite in the as-received samples transform to tempered martensite and cementite after heat treatment process. From this research, for corrosion test, heat treated 440C SS sample tempered with 426 ℃possessed the excellent corrosion resistance with corrosion rate 0.2808 mm/year.

• Journal of the Korean Society of Propulsion Engineers
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• v.11 no.2
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• pp.9-17
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• 2007

The performance test of recirculation line in propellant feeding system was carried out. Liquid oxygen was used as cryogenic propellant and helium was used as recirculation promotion gas. Tests were done in cases at atmospheric pressure and at pressure of 4 barg in the ullage space of propellant tank. Liquid oxygen recirculation flowrate with helium injection flowrate and temperature distribution along the line were measured. There was appropriate helium injection flowrate for gas-lift recirculation system. Test data were used to make calculation program by test data correlation method. In this paper the procedure of calculation was presented and the results were compared to test data.

• Progress in Superconductivity and Cryogenics
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• v.19 no.1
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• pp.13-16
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• 2017

Water issue, especially water pollution, is a serious issue of 21st century. Being an significant technique for securing water resources, superconducting magnetic separation wastewater system was indispensable. A large bore conduction-cooled magnet was custom-tailored for wastewater treatment. The superconducting magnet has been designed, fabricated and tested. The superconducting magnet was composed of NbTi solenoid coils with an effective horizontal warm bore of 400 mm and a maximum central field of 2.56T. The superconducting magnet system was cooled by a two-stage 1.5W 4K GM cryocooler. The NbTi solenoid coils were wound around an aluminum former that is thermally connected to the second stage cold head of the cryocooler through a conductive copper link. The temperature distribution along the conductive link was measured during the cool-down process as well as at steady state. The magnet was cooled down to 4.8K in approximately 65 hours. The test of the magnetic field and quench analysis has been performed to verify the safe operation for the magnet system. Experimental results show that the superconducting magnet reached the designed magnetic performance.

• Journal of Welding and Joining
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• v.35 no.3
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• pp.82-87
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• 2017

Recent trends in shipbuilding and offshore industries are a huge increase in the ship size and the exploration and production of oil and natural gas in the arctic offshore region. High performance steel plates are required by these industrial trends. Also in IMO(International Maritime Organization) has begun to regulate of fuel of ship to environmental protection, therefore it is little bit difficult to use bunker-C oil to working ship. As the problem of environmental change such as global warming is emerged, the operation of the ship is considered to be involved in the environmental change problem, and the regulation of environmental pollution is gradually strengthened. As these environmental regulations are strengthened demand for LNG fuel ships is rapidly increasing. Currently, cryogenic steels used in LNG tanks include aluminum alloy, SUS 304, and 9%-Ni steel. Those steels are has high cost to construction of large LNG carrier. The new materials were suggested several steel mills to decrease construction cost and easy construction. The new cryogenic steel should be evaluate safety to applied real structure include LNG ship. Therefore, in this study, fracture toughness of weld joints were investigated with cryogenic steel for application of LNG tank.