• Transactions of the Korean Society of Mechanical Engineers A
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• v.22 no.1
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• pp.64-72
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• 1998

This paper was undertaken to develop the fracture toughness testing method using small and single specimen compared to the conventional method in evaluating elastic-plastic fracture toughness of the superconducting magnet structural material at cryogenic temperature. The elastic-plastic fracture toughness test was conducted by using the unloading compliance method recommended by ASTM E813-89 to accomplish the above purpose. And, the 20% side-grooved 0.5TCT and 1TCT specimens were used to evaluate the fracture toughness by using as possible as miniaturized CT specimen. The unloading compliance method was a very useful method in evaluating elastic-plastic fracture toughness at cryogenic temperature. It could be taken valid fracture toughness values by using 20% side-grooved 0.5TCT specimen recommended by ASTM E813-89.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.22 no.2
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• pp.343-351
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• 1998

This paper was investigated degradation of the fracture toughness caused by sensitizing heat-treatment of the cryogenic structural material JN1 base metal using unloading compliance method reported as useful a method in evaluating the elastic-plastic fracture toughness at cryogenic temperature. The specimens used in this paper were 20% side-grooved 0.5T-CT specimens which were machined in the JN1 base metal. Also, to investigate cryogenic fracture toughness of the fusion line region in the JN1 GTA weldments, it was also used 20% side-grooved 0.5T-CT specimens that was machined fusion line to located in the middle of the specimen. The cryogenic fracture toughness values of the JN1 base metal were significantly decreased with increasing the time and temperature of the heat treatment. The fracture toughness value obtained from the fusion line specimen was invalid, but it was lower value than that of the JN1 base metal. Especially, this value was approximately equal with that obtained from the JN1 650.deg. C-5h heat-treated material.

• Journal of Mechanical Science and Technology
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• v.15 no.1
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• pp.26-34
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• 2001

Most research to date concerning the cryogenic toughness of austenitic stainless steels has concentrated on the base metal and weld metal in weldments. The most severe problem faced on the conventional austenitic stainless steel is the thermal aging degradation such as sensitization and carbide induced embrittlement. In this paper, we investigate the cryogenic toughness degradation which can be occurred for austenitic stainless in welding. The test materials are austenitic stainless JN1, JJ1 and JK2 steels, which are materials recently developed for use in nuclear fusion apparatus at cryogenic temperature. The small punch(SP) test was conducted to detect similar isothermally aging condition with material degradation occurred in service welding. The single-specimen unloading compliance method was used to determine toughness degradation caused by thermal aging for austenitic stainless steels. In addition, we have investigated size effect on fracture toughness by using 20% side-grooved 0.5TCT specimens.

• Journal of Advanced Marine Engineering and Technology
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• v.35 no.6
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• pp.802-808
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• 2011

One of the important mechanical properties of cryogenic temperature structure material is fracture toughness. Research on normalization of fracture toughness test method is becoming very important issue with development of cryogenic structural elements. Specially, mechanical properties estimation by each micro-structure of welding department is important because it can cause unstable fracture when use under cryogenic environment in case of welding department. In this study, fracture toughness estimation test was carried out to unloading compliance method and sensitization heat-tread minimized test specimen at liquid nitrogen (77K), liquid helium (4K), 293K temperature to STS-316L base metal and weld metal.

• Journal of Welding and Joining
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• v.35 no.3
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• pp.82-87
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• 2017

Recent trends in shipbuilding and offshore industries are a huge increase in the ship size and the exploration and production of oil and natural gas in the arctic offshore region. High performance steel plates are required by these industrial trends. Also in IMO(International Maritime Organization) has begun to regulate of fuel of ship to environmental protection, therefore it is little bit difficult to use bunker-C oil to working ship. As the problem of environmental change such as global warming is emerged, the operation of the ship is considered to be involved in the environmental change problem, and the regulation of environmental pollution is gradually strengthened. As these environmental regulations are strengthened demand for LNG fuel ships is rapidly increasing. Currently, cryogenic steels used in LNG tanks include aluminum alloy, SUS 304, and 9%-Ni steel. Those steels are has high cost to construction of large LNG carrier. The new materials were suggested several steel mills to decrease construction cost and easy construction. The new cryogenic steel should be evaluate safety to applied real structure include LNG ship. Therefore, in this study, fracture toughness of weld joints were investigated with cryogenic steel for application of LNG tank.

• Proceedings of the KWS Conference
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• 1997.05a
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• pp.87-90
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• 1997

• Journal of the Korean Society of Industry Convergence
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• v.26 no.2_2
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• pp.333-340
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• 2023

Environmental regulations are being strengthened worldwide to solve global warming. For this reason, interest in eco-friendly gas fuels such as LNG and hydrogen is continuously increasing. However, when adopting eco-friendly gas fuel, liquefying at a cryogenic temperature is essential to ensure economic feasibility in storage and transportation. Although austenitic stainless steel is typically applied to store cryogenic liquefied gas, structural steel can experience sudden heat shrinkage in the case of leakage in the loading and unloading process of LNG. In severe cases, the phase of the steel may change, so care is required. This study conducted Charpy impact tests on steel material in nine different temperature ranges, from room to cryogenic temperatures, to analyze the effects of cryogenic liquefied gas leaks. As a result of the study, it was not easy to find variations in ductile to brittle transition temperature (DBTT) due to the leakage of cryogenic liquefied gas. Still, the overall impact toughness tended to decrease, and these results were verified through fracture surface analysis. In summary, brittle fracture of the steel plate may occur when a secondary load is applied to steel for hull structural use exposed to a cryogenic environment of -40 ℃ or lower. Therefore, it needs to be considered in the ship design and operating conditions.

• 한국가스학회:학술대회논문집
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• 1998.09a
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• pp.340-349
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• 1998

• Korean Journal of Materials Research
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• v.31 no.9
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• pp.519-524
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• 2021

The impact properties of two austenitic Fe-23Mn-0.4C steels with different Al contents for cryogenic applications are investigated in this study. The 4Al steel consists mostly of austenite single-phase microstructure, while the 5Al steel exhibits a two-phase microstructure of austenite and delta-ferrite with coarse and elongated grains. Charpy impact test results reveal that the 5Al steel with duplex phases of austenite and delta-ferrite exhibits a ductile-to-brittle transition behavior, while the 4Al steel with only single-phase austenite has higher absorbed energy over 100 J at -196 ℃. The SEM fractographs of Charpy impact specimens show that the 4Al steel has a ductile dimple fracture regardless of test temperature, whereas the 5Al steel fractured at -100 ℃ and -196 ℃ exhibits a mixed fracture mode of both ductile and brittle fractures. Additionally, quasi-cleavage fracture caused by crack propagation of delta-ferrite phase is found in some regions of the brittle fracture surface of the 5Al steel. Based on these results, the delta-ferrite phase hardly has a significant effect on absorbed energy at room-temperature, but it significantly deteriorates low-temperature toughness by acting as the main site of the propagation of brittle cracks at cryogenic-temperatures.

• Journal of Welding and Joining
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• v.31 no.6
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• pp.50-57
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• 2013

Characterization of microstructures and cryogenic mechanical properties of electro beam (EB) welds between cast and forged Inconel 718 superalloys has been investigated. Optimal EBW condition was found in the beam current range of 36~39 mA with the constant travel speed of 12 mm/s and arc voltage of 120 kV for 10 mm-thick specimens. Electron beam current lower than 25 mA caused to occur the liquation microfissuring in cast-side heat affected zone (HAZ) of EB welds. The HAZ liquation microfissure was found on the liquated grain boundaries with resolidified ${\gamma}/Laves$ and ${\gamma}/NbC$ eutectic constituents. EBW produced welds showing a fine dendritic structure with relatively discrete Laves phase due to fast cooling rate. After post weld aging treatment, blocky Laves phase and formation of ${\gamma}^{\prime}+{\gamma}^{{\prime}{\prime}}$ strengtheners were observed. Presence of primary strengthener and coarse Laves particles in PWHT weld may cause to reduce micro-plastic zone ahead of a crack, leading to a significant decrease in Charpy impact toughness at $-196^{\circ}C$. Fracture initiation and propagation induced by Charpy impact testing were discussed in terms of the dislocation structures ahead of crack arisen from the fractured Laves phase.