• Journal of the Korean Recycled Construction Resources Institute
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• v.10 no.4
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• pp.514-522
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• 2022

In this study, as part of a study to improve the self-healing performance of concrete structures by applying self-healing capsules made of cementitious materials to cement composite materials, the engineering characteristics of mortars according to PCC(Powder Compacted Capsule) size and mixing ratio were compared and analyzed. For this, fluidity, compressive strength, reload test, carbonation, ultrasonic velocity, and water permeability characteristics were measured according to PCC size and mixing ratio of mortar. As a result of the measurement, the fluidity and compressive strength increased as the mixing ratio of PCC increased, and in the case of the load reload test, the healing ratio increased as the mixing ratio of PCC increased in the 03PC formulation. In the case of water permeability test, it was found that when PCC was used, the reduction ratio of water flow was up to 35 % higher than that of Plain, and when PCC with a size of 0.3 to 0.6 mm was mixed with 15 %, it was found to be effective in improving the crack healing ratio of the mortar.

• Journal of the Korean Recycled Construction Resources Institute
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• v.6 no.3
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• pp.222-227
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• 2018

Recently, due to the deterioration and various natural disasters caused by the passage of concrete pole for 20~30 years or more, damage and destruction of the poles have increased the demand for maintenance. In this paper, 10 flexural strength test specimens were fabricated by using crack self - healing concrete of Fly ash, GGBS, CA, etc. The compressive strength of the concrete with slag was found to be excellent, but the concrete with fly ash was slightly below the reference strength. In addition, the crack loadings of the specimens satisfied the criteria of KS F 4304. In the case of the load-deflection and strain relations, the behavior of the fly ash specimens was similar, but in the specimens containing the blast furnace slag, The results showed that a large amount of strain occurred.

• Journal of the Korean Recycled Construction Resources Institute
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• v.9 no.3
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• pp.389-396
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• 2021

In this paper, it was evaluated that the effect of self-healing microcapsules on the quality and healing properties of cement composites. In the mixing of microcapsules, the plastic viscosity and yield stress of the cement composites decreased due to the particle properties of the microcapsules, and decreased in proportion to the mixing ratio. The table flow showed a tendency to decrease as the core material acted as a stimulant due to the loss of microcapsules, and the compressive strength could be supplemented through unit quantity correction. As a result of evaluating the effect of microcapsule mixing on the healing properties of cement composites, it was found that the unit water flow rate decreased by the healing reaction immediately after crack initiation. When more than 3% of microcapsules were mixed, it was found that there was a healing rate of more than 95% at 7 days of healing age.

• Journal of the Korean Recycled Construction Resources Institute
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• v.8 no.1
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• pp.88-96
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• 2020

In this study, the effect of cyclic wetting-drying on the self-healing of cementitious materials containing superabsorbent polymers (SAPs) were experimentally evaluated. In each cycle, cracked cement paste specimens containing various SAP dosages were exposed to wet conditions for 1 h, during which the capillary water absorption tests and water flow tests were conducted, and then exposed to dry conditions for 47 h. The capillary water absorption test results showed that the sorptivity values of the specimen without SAPs, SAP 0.5%, SAP 1.0%, and SAP 1.5% specimens were decreased by approximately 22.9%, 36.8%, 42.8%, and 46.3%, respectively, after 8 cycles. In addition, the water flow test results showed that the amount of water runoff through the cracks of all cracked specimens gradually decreased over wet/dry cycles, especially the reduction ratio of the amount of water runoff increased with increasing SAP dosage. Furthermore, the swelling behavior of SAPs in cracks by in gress water was con firmed via X-ray computed tomography (CT) analysis. These results indicate that the effective crack width can be reduced as SAPs absorb water and swell, while the water absorbed in SAPs can be released to crack surfaces under dry conditions, further promoting healing product formation. This study demon strates that the in corporation of SAPs can in crease the water tightness of cracks, thereby improving the self-healing efficiency of cementitious materials.

• Elastomers and Composites
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• v.49 no.2
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• pp.134-143
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• 2014

Polymers are introduced to neat asphalt to prepare self-healing asphalt. The polymers are Surlyn, Nylon and polyethyleneterephtalate(PET). Since they are known as having high intermolecular force, they have high processing temperature. Therefore they are hardly introduced into the asphalt as bulk state. So in this study, they are introduced as solutions. Polymer-modified asphalts showed excellent modification effect and also healing effect. 5% polymer added asphalt showed more than 18% increased tensile strength. This tensile strength increment can be explained by polymer's intermolecular forces. Especially Surlyn interacts with asphalt molecules by hydrogen bonding and also with metals in asphalt by ionic bonding. When it comes to healing aspect the healing efficiency of Surlyn increased to 138% based on tensile strength. That of PET increased to 141% based on complex modulus and in case of Nylon it increased to 131% based on impact strength. This tells that in dealing with healing efficiency the important considering factors are not only the intermolecular forces of the polymers but also the interaction between the polymer and asphalt molecules.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2015.05a
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• pp.228-229
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• 2015

In this research, properties of new crack repair materials using organic and inorganic composites (OAI) were investigated under various crack conditions. Especially, this study aims to develop new composites repair materials as needed to follow the crack and its repair method. Crack repair methods such as injection method and surface treatment repair method using self-healing capability for the practical industrial application were examined in comparison with normal crack repair method as a epoxy injection. From these results, it was confirmed that the sealing and injection effects through the cracks from field tests could be improved by OAI.

• Journal of the Korea institute for structural maintenance and inspection
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• v.20 no.6
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• pp.10-19
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• 2016

The objective of this study is to investigate the self-healing properties of ternary blended cement(TBC) paste made with OPC, GGBFS and FA. The influence of OPC-GGBFS-FA on the self-healing ability of ternary blended cement paste was researched by ultrasonic pulse velocity(UPV) measurement. The TBC paste with GGBFS-FA replacement ratios of 20%, 40% and 60% were prepared having a constant water-cementitious materials ratios os 0.5. The research focuses on behavior after 28days(after loading). Four-point bending tests are used to pre-cracked the prismatic specimens at 28days. For specimens (uncracked and cracked) submerged in tap-water and sea-water until 60days. According to the experimental results, the TBC paste system has self-healing ability increased when the fraction of GGBFS increased. Because GGBFS and FA continues to hydrate after 28days, it is likely that hydrated products from GGBFS and FA may modify microstructures, seal these cracks. From these results, it is clear that the crack in all samples experience self-healing and that this occurs mostly in the first 30days of submerging. Futhermore, most of the healing for both specimens of submerged in sea-water and tap-water occurred during the first 30days. Sea-water submerged specimens healed cracks as fast as those in tap-water. Differences in healing effects of submerged in sea-water and tap-water may be attributed to the presence of specific sea-water ions. Therefore, self-healing effects considered age-effects was more strong effect occurred mostly in the first 30days, and then gradually weaken.

• Smart Structures and Systems
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• v.25 no.3
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• pp.337-343
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• 2020

In this paper, we focused on the self-healing concrete using new nano-capsules. Three types of nano-capsules with respect to availability, high strength and temperature tolerance are used; type 1 is URF and polyethylene (PE) as shell and nano titanium oxide (TiO₂) as core, type 2 is URF and PE as shell and nano silica oxide (SiO₂) as core, type 3 is PE as shell and nano silica oxide (SiO₂) as core. The concrete samples mixed by nano-capsules with three percents of 0.5, 1 and 1.5. Based on experimental tests and the compressive strength of samples, the URF-PE-SiO₂ is selected for additional tests of compressive strength before and after recovery, ultrasonic test, ion chlorine and water penetration depths. After careful investigation, it is concluded that the optimum value of URF-PE-SiO₂ nano-capsules is 0.5% since leads to higher compressive strength, ultrasonic test, ion chlorine and water penetration depths.

• Smart Structures and Systems
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• v.24 no.2
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• pp.157-171
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• 2019

This study investigated the effects of the geometric parameters of superelastic shape memory alloy (SE SMA) fibers on the pullout displacement recovering and self-healing capacity of reinforced cementitious composites. Three diameters of 0.5, 0.7 and 1.0 mm and two different crimped lengths of 5.0 and 10.0 mm were considered. To provide best anchoring action and high bond between fiber and cement mortar, the fibers were crimped at the end to create spear-head shape. The single fiber cement-based specimens were manufactured with the cement mortar of a compressive strength of 84 MPa with the square shape at the top and a dog-bone shape at the bottom. The embedded length of each fiber was 15 mm. The pullout test was performed with displacement control to obtain monotonic or hysteretic behaviors. The results showed that pullout displacements were recovered after fibers slipped and stuck in the specimen. The specimens with fiber of larger diameter showed better displacement recovering capacity. The flag-shaped behavior was observed for all specimens, and those with fiber of 1.0 mm diameter showed the clearest one. It was observed that the length of fiber anchorage did not have a significant effect on the displacement recovery, pullout resistance and self-healing capacity.

• Journal of the Korean Recycled Construction Resources Institute
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• v.10 no.4
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• pp.561-568
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• 2022

In this study, the mechanical properties and self-healing performance of cement mortar containing clinker binder, calcium sulfoaluminate(CSA), and sodium sulfate(Na₂SO₄) were evaluated. The mechanical properties of cement mortar were investigated by measuring compressive strength and flexural strength, and the healing performance was evaluated through hydrostatic water permeability test and gas diffusion test. In addition, the healing products precipitated in the cracks were visually observed through an optical microscope and a scanning electron microscope(SEM). As a result, the incorporation of the clinker binder-based inorganic additives improved the initial and 28-day strength by about 20 %. Depending on the healing performance evaluation method, there was a difference in the healing rate, and the healing rate showed a tendency to be underestimated. Nevertheless, CaCO₃ was precipitated as the main healing product inside the 0.3 mm crack when the inorganic additives were mixed with cement mortar, improving the self-healing performance.