• Title/Summary/Keyword: Crack self-healing

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Importance of Impregnation and Polishing for Backscattered Electron Image Analysis for Cementitious Self-Healing Specimen (시멘트계 자기치유 시편에 대한 반사전자현미경 이미지 분석을 위한 함침과 연마의 중요성)

  • Kim, Dong-Hyun;Kang, Kook-Hee;Bae, Seung-Muk;Lim, Young-Jin;Lee, Seung-Heun
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.5 no.4
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    • pp.435-441
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    • 2017
  • Studies on self-healing have currently been diversified and the methods to evaluate the studies have become more diversified as well. Among them, the back-scattered electron (BSE) image acquired through the scanning electron microscope (SEM) is attempted as the means to evaluate the self-healing effect on cracks. In order evaluate by the BSE image, sophisticated pre-processing of specimen is critical and this injected inside the particle, pore and artificial crack of the hardener to stabilize the structure of the newly generated self-healing product and it enables to endure the stress on polishing without deformation. The impregnated specimen smoothen the surface to obtain the BSE image of high resolution that polishing is made for diamond suspension for wet polishing after dry polishing. As a result of evaluating the self-healing product on the impregnated and polished self-healing specimen, the generated product is formed from the surface of the artificial crack and the self-healing substances are confirmed as $Ca(OH)_2$ and C-S-H.

An Experimental Study on the Self-Healing Performance of Solid Capsules According to the Composition Ratio of Crystal Growth Type Inorganic Materials (결정성장형 무기재료 조성비에 따른 고상 캡슐의 자기치유 성능에 관한 실험적 연구)

  • Nam, Eun-Joon;Oh, Sung-Rok;Kim, Cheol-Gyu;Choi, Yun-Wang
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.25 no.2
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    • pp.16-22
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    • 2021
  • In this paper, a solid capsule was prepared using a crystal growth type inorganic material capable of hydration reaction. The solid capsules were mixed at 3, 5, and 10% according to the composition ratio of 8:2, 7:3, 6:4 based on the cement mass, and the self-healing mortar was mixed, Durable healing properties were evaluated through the water permeability test. As a result of the water level permeability test, the effect of optimally improving the natural healing performance was shown by mixing the solid capsules prepared in a composition ratio of 7:3 of the solid capsules. In the case of a crack width of 0.3mm or less, it is estimated that more than 90% of the self-healing performance can be secured. As a result, it was judged that the self-healing performance of the solid capsule had an effect on the durable healing properties through the water permeability test, It is judged that there is a tendency to improve self-healing performance according to the mixing of solid capsules.

The Experimental Study on Preparation Characteristics of Self-healing Microcapsules for Mixing Cement Composites Utilizing Liquid Inorganic Materials (액상 무기재료를 활용한 시멘트 복합재료 혼합용 자기치유 마이크로 캡슐의 제조 특성에 관한 실험적 연구)

  • Choi, Yun-Wang;Oh, Sung-Rok;Kim, Cheol-Gyu;Lim, Hak-Sang
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.6 no.4
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    • pp.236-244
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    • 2018
  • In this study, we tried to fabricate self - healing microcapsules using liquid inorganic materials which can be mixed directly with cement composites. The basic properties of the liquid inorganic material were evaluated and microencapsulation was performed. The focus of this paper is on the quality and manufacturing characteristics of cement composites rather than the healing effects of self - healing microcapsules according to mixed capsules. Test results, the self-healing microcapsules encapsulate liquid inorganic material which is stable at room temperature and has high crack followability, and the yield is over 90%. The size of self - healing microcapsule was able to change according to the synthetic agitation speed and it was able to secure more than 70% of target size. In addition, the loss of less than 10% was found to occur through the membrane strengthening of self - healing microcapsules, and it could be reduced by 50% compared with the case without membrane strengthening.

An Experimental Study on the Healing Performance of Cement Composites According to Mixing Ratio of Self-Healing Hybrid Capsules (자기치유 하이브리드 캡슐 혼합율에 따른 시멘트 복합재료의 치유성능에 관한 실험적 연구)

  • Yun-Wang, Choi;Jun-Ho, Park;Yong-Jic, Kim;Sung-Rok, Oh
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.10 no.4
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    • pp.531-538
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    • 2022
  • In this study, the self-healing hybrid capsules were prepared, were mixed with 3 %, 5 %, and 7 % based on cement mass. The healing performance were evaluated according to mixing ratio self-healing hybrid capsule. As a result of the experiment, it was found that the crack healing performance improved as the mixing rate of the self-healing hybrid capsule increased, but the quality performance tended to decrease. Therefore, it is judged that using the mixing ratio of the hybrid capsule within 5 % reduces the quality performance to within about 10 % and secures about 90 % or more of the healing performance.

Characterization of crack self-healing of silicon carbide by hot press sintering (열간가압소결법으로 제조한 탄화규소의 균열자기치유 특성)

  • Kim, Seong-Hoon;Kim, Kyung-Hun;Dow, Hwan-Soo;Park, Joo-Seok;Kim, Kyung-Ja;Shim, Kwang-Bo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.26 no.2
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    • pp.62-66
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    • 2016
  • In this study, it was investigated that characteristic of crack-self-healing of hot-pressed SiC. SiC ceramics was sintered with $Al_2O_3$ and $Y_2O_3$ sintering additive by hot press. Sintering was performed in hot-press furnace in flowing argon (Ar), holding for 3 hr under $1950^{\circ}C$ and 50 MPa. The sintered SiC was machined into 3-point bending strength specimen of $3{\times}4{\times}40mm$, and introduced pre-crack by Vickers indentation at 49.6 N. Specimens were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), 3-point bending strength after heat treatment at $1200{\sim}1400^{\circ}C$ for 1~10 hr. The best crack-self-healing ability was achieved 770 MPa 3-point bending strength by heat treatment at $1300^{\circ}C$ for 5 hr.

Self Healing System for Concrete Surface Crack using Polymer based Coating Agent Incorporating Microencapsulated Healing Agent (마이크로캡슐을 함유한 폴리머 코팅제의 콘크리트 표면균열 자기치유시스템)

  • Shin, Ki-Su;Ryu, Byung-Chul;Wang, Xiao-Yong;Park, Ki-Bong
    • Journal of the Korea Institute of Building Construction
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    • v.15 no.6
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    • pp.579-587
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    • 2015
  • In this paper, microencapsulated healing agent was embedded in the polymer matrix to obtain self healing properties. Microencapsulation of methacrylate using polyurea-formaldehyde as a shell material and studied the effect of agitation rate on capsule characteristics such as size, shell thickness, and surface morphology. The formation of microcapsules was confirmed by FTIR and TGA, and capsule characteristics were studied by optical microscopy and SEM. The self-healing effect was evaluated using permeability measurements and further confirmed by surface analytical tools including optical microscope. According to the experimental results, the microencapsulated healing system has the self-heaing ability for artificial cracks.

Self-government Frame and Discourse Effect of 'Healing' Phenomenon in Korea (초기 힐링담론의 자기통치프레임과 담론효과)

  • Kim, Eunjune
    • Korean journal of communication and information
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    • v.74
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    • pp.38-71
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    • 2015
  • Based on the Foucault's governmentality, this study has described the self-government strategy that healing discourse is implemented during 2011-2013. Healing discourse's priority is the existence value of individual and full concentration about self is needed more than anything. In this process, people who need to heal and comfort are limit to de-politicized individuals. Healing discourse emphasizes that the current enhancement in order to become reflection and growth of self. Demands of reflection and growth is substitute the critics of the era and society, but also act as a specific code of conduct to individuals. While emphasizes the reflection and personal growth, healing discourse has top priority of the current value. However, in this process, criticism of the era issues and social structural factors are fundamentally excluded. People accepted healing discourse actively, decided empowering self by reflection and remorse. On the other hand, there is a crack and specificity in the dominant reception discourse likewise some subjects criticized that there is no realistic consolation, exposed the antipathy to the older generation, denied the way of problematized objectification. But this is a partial denial about healing as concrete technology, not fundamental resistance about neoliberal orders.

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Performance Evaluation Method of Self-Healing Concrete Using Gas Diffusion Experiment (기체확산 실험을 활용한 자기치유 콘크리트의 성능평가 방법)

  • Lee, Do-Keun;Shin, Kyung-Joon
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.8 no.1
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    • pp.143-151
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    • 2020
  • Recently, research on self-healing concrete has been actively conducted, and various methods have been attempted for use in the maintenance of structures. However, contrary to the technical development of self-healing concrete, the method for evaluating the performance is insufficient. Although surface observation and permeability experiments are widely used to observe the healing of cracks, microscopic observation of surface may be insufficient to assess the overall performance. Also, permeation experiments should consider the losses caused by the dissolution of self-healed product and viscosity of water. Although a gas diffusion experiment have been proposed to overcome the shortcomings of these two test methods, verification has not been made on specimens with actual healing. Therefore, in this study, gas diffusion experiments were performed on the mortar specimens that had healed, and the adequacy of self-healing evaluation by the gas diffusion experiment was verified.

Water Permeability Performance Evaluation of Mortar Containing Crack Self-healing Mineral Admixtures (균열 자기치유 재료 혼입 모르타르의 투수성능 평가)

  • Lee, Woong-Jong;Hwang, Ji-Soon;Ahn, Sang-Wook;Lee, Kwang-Myong
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.4
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    • pp.463-469
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    • 2016
  • In this paper, compressive strength and water permeability performance for two types of crack self-healing materials such as SH-PO-0 composed of mineral admixtures(expansive agent, swelling material and crystal growth agent) and SH-PO-(5, 15, 30) blended with SH-PO-0 and phosphate additive(PO) dissolving easily calcium ion, were evaluated. The test results show that the water flow of SH-PO-0 decreased steeply at the early age although compressive strength decreased about 9% at 28 days compared with OPC. The higher PO replacement ratio is, the lower compressive strength and more improved water permeability performance is, and thus, based on such results, adequate PO replacement ratio is 15%. It is also found that the self-healing performance of SH-PO-15 was quite improved at the early ages and however, the performance of SH-PO-15 is similar to one of SH-PO-0 at long-term ages, and 28 days compressive strength of SH-PO-15 decreased about 8% compared with SH-PO-0. In addition, it is confirmed from the analysis of SEM-EDS that calcium ions of SH-PO-15 were crystallized more than those of SH-PO-0.

Relationship between Crack Width and Gas Diffusion Coefficient of Cracked Acrylic Specimens (균열 아크릴 시편의 기체 확산계수와 균열폭의 관계)

  • Lee, Do-Keun;Lim, Min-Hyuk;Shin, Kyung-Jun
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.6 no.4
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    • pp.245-251
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    • 2018
  • Recently, as the importance of structural maintenance has been increased, studies on self - healing concrete technology are being actively carried out. On the other hand, test for evaluating the self-healing performance is not standardized yet. Although visual test is used as a basic method for measuring crack widths, it is difficult to observe the crack width inside the specimen, and there is a disadvantage that only the local measurement of the surface can be measured due to the inhomogeneous cracking characteristics. Although permeability test has been widely used as an indirect method for measuring crack width, there is a problem due to the viscosity of water, and also a possibility that the internal material of the specimen may be eluted during the test. In this study, we propose a crack width evaluation method using gas diffusion characteristics. Idealized straight cracks were fabricated by acrylic and the diffusion coefficients of specimens were analyzed with respect to crack width and thickness. The experimental results show that the crack width and the diffusion coefficient are in a linear relationship and that the thickness and diffusion coefficient are inversely related.