• Title/Summary/Keyword: Contents Analyzer

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Determination of Heavy Metal Concentration in Herbal Medicines by GF-AAS and Automated Mercury Analyzer

  • Kim, Sang-A;Kim, Young-Jun
    • Journal of Food Hygiene and Safety
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    • v.36 no.4
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    • pp.281-288
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    • 2021
  • This study was conducted to analyze and compare the concentrations of heavy metals in 430 different products of 20 types of herbal medicines available in the domestic market in Korea by Graphite Furnace-Atomic Absorption Spectrometry (GF-AAS) and automated mercury analyzer. The accuracy for lead (Pb), arsenic (As), cadmium (Cd), and mercury (Hg) was in the range 92.67-102.56%, and the precision was 0.21-6.00 relative standard deviation (RSD%), which was in compliance with the Codex acceptable range. Furthermore, the Food Analysis Performance Assessment Scheme (FAPAS) quality control (QC) material showed a recovery range of 96.7-102.0% and 0.33-4.93 RSD%. The average contents (㎍/kg) of Pb, As, Cd, and Hg in herbal medicines were 254.9 (not detected (N.D.)-2,515.2), 171.0 (N.D.-2,465.2), 99.2 (N.D.-797.1), and 6.0 (N.D.-83.6), respectively. Based on the quantitative analysis results, the heavy metal contents of 20 types of herbal medicines distributed in Korea are within the acceptable range according to the standards issued by the Ministry of Food and Drug Safety (MFDS). By using the manufacturer of herbal products as the standard for QC, the Pb, As, Cd, and Hg contents were investigated in the packaging process just before distribution to determine the actual conditions of residual heavy metals in herbal medicines. Thus, these result may contribute to monitoring the QC of herbal medicines distributed in Korea and could provide basic data for supplying safe herbal medicines to the public.

Developing A Medical Intelligence System in Medical Data Warehouse (의료 데이터 웨어하우스에서의 Medical Intelligence 시스템 개발)

  • Kim, Tae-Hun;Kim, Jong-Ho
    • IE interfaces
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    • v.17 no.4
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    • pp.426-439
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    • 2004
  • This research discusses knowledge contents needed to build an OLAP system for medical sector, OLAP functionalities from past studies, and a medical intelligence system which is a kind of OLAP. The knowledge requirements which consist of nine contents and OLAP fundamental functionalities are applied to the system. Most past studies have focused on developing a medical data warehouse rather than OLAP. The medical intelligence system supplies health care providers (i.e., doctors, clinicians, researchers and nurses) and non-providers (i.e., managers and business analysts) with multidimensional OLAP functionalities. The system can be used to gain a deeper understanding of specific medical issues. In this research, we focus not on medical data warehouse, but on the technical challenges of designing and implementing an effective medical intelligence system for health care information. An architecture is applied to developing the medical intelligence system for a medical center in order to illustrate its practical usage. Six packages in the developed system are discussed in this research: Explorer, Analyzer, Reporter, Statistician, Visualizer, and Meta Administrator packages. Evaluation of the system and ongoing research directions conclude the research.

Studies on Incombustibility Improvement of EPDM Rubber with $Al(OH)_3$ and $Sb_2O_3$ ($Al(OH)_3$$Sb_2O_3$의 첨가에 따른 EPDM계 고무의 난연성 향상 연구)

  • Kim, Jin-Yong;Lee, Won-Bok;Lim, Dae-Hyun;Suh, Hyuk;Rhee, Young-Woo
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2009.11a
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    • pp.449-452
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    • 2009
  • In order to improve incombustibility of EPDM(Ethylene propylene diene monomer)-based rubber, inorganic materials as $Al(OH)_3$ and $Sb_2O_3$ were added. The mechanical and thermal properties have been measured for vulcanized rubber loaded with different concentrations of $Al(OH)_3$ and $Sb_2O_3$. As inorganic material contents increases from 5phr to 30phr, the specific gravity and hardness increase while elongation at break decreases. This study performed incombustibility test and thermal analysis through TGA(Thermogravimetric Analyzer). As a results, incombustible and thermal properties of EPDM-based rubber were improved as $Al(OH)_3$ and $Sb_2O_3$ contents increase.

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Synthesis of Tungsten Carbide Powders by SHS Method (SHS법에 의한 탄화텅스텐 분말 합성)

  • Jun, H.B.;Cho, D.H.;Lee, H.B.;Park, S.
    • Journal of the Korean Ceramic Society
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    • v.31 no.10
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    • pp.1159-1168
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    • 1994
  • We powders were synthesized from W powders in differnet particle sizes by Self-propagating High-temperature Synthesis process (SHS) using a chemical furnace. The effects of the mole ratio of chemical fuel content, pellet thickness and the mole ratio between carbon and tungsten (C/W Ratio) on synthesis were investigated with the tungsten powders have different particle size each other. Compositional and structural characterization of these powders was carried out by scanning electron microscope (SEM0 and x-ray diffractometer. Powder characterization was carried out by the measurement of particle size distribution with laser-particle size analyzer. The amounts of WC obtained by SHS process depend very much on the particle size of tungsten powder and heat contents given in a product, i.e. as the particle size of W powder is smaller, the amounts of WC produced increase. Also the more heat contents is given, the more amounts of WC increase. By optimizing the synthesis conditions, it is possible to fabricate WC powders which have little secondary phases (W2C, C).

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Pyrolysis of Waste Oriental Medicine Byproduct Obtained from the Decoction Process of Achyranthes Root (우슬(Achyranthes Root) 탕제 후 얻어진 폐한약재 부산물의 열분해)

  • Park, Ji Hui;Jeong, JaeHun;Lee, Ji Young;Kim, Young-Min;Park, Young-Kwon
    • Applied Chemistry for Engineering
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    • v.29 no.4
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    • pp.474-478
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    • 2018
  • Thermal decomposition of waste Achyranthes Root (WAR) emitted from its decoction process was investigated using a TG analyzer and a fixed-bed reactor. The WAR had the larger C and fixed carbon content than fresh AR (FAR) due to the extraction of hemicelluloses from FAR during decoction process. Thermogravimetric (TG) analysis results also revealed the elimination of hemicellulose by its decoction. Relatively high contents of the cellulose and lignin made high contents of their typical pyrolyzates, such as acids, ketones, furans, and phenols, in the pyrolysis of WAR using the fixed-bed reactor. The increase of pyrolysis temperature from 400 to $500^{\circ}C$ increased yields of oil and gas due to the more effective cracking efficiency of WAR at a higher temperature. The chemical composition of product oil was also changed by applying the higher pyrolysis temperature, which increased the selectivity to furans and phenols.

Determination of Ethanol in Alcoholic Beverages by Alcohol Oxidase Sensor (Alcohol oxidase 효소센서를 이용한 알코올 음료 중의 에탄올 정량)

  • Lee, Ok-Kyung;Kim, Tai-Jin;Noh, Bong-Soo
    • Korean Journal of Food Science and Technology
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    • v.27 no.2
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    • pp.266-269
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    • 1995
  • In order to measure alcohol contents with speed and accuracy, alcohol sensor was prepared. Alcohol sensor was made by connecting with oxygen electrode after immobilized alcohol oxidase on nylon net with glutaraldehyde. Alcohol was determined by changing the rate of dissolved oxygen consumption using D.O. analyzer. Alcohol contents in alcoholic beverages were determined under the optimum conditions. The results were 0.71% in low-alcohol beverage, $4{\sim}5%$ in beers, 10.06% in wine, 16.12% in chungju, 25.71% in soju, and 6.18% in takju, respectively. The values by alcohol sensor showed an excellent correlation(r=0.999) with GC method.

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The Effect on the Combustion and Emission Characteristics of HCNG Engine According to the High Purity Hydrogen Contents (고순도 수소함량에 따른 HCNG 연소특성 및 배출가스 영향 평가)

  • Lee, Jong-Tae;Lim, Yun-Sung;Kim, Hyung-Jun;Lee, Seong-Wook;Lee, Jang-Hoon;Kim, Jong-Geu
    • Journal of ILASS-Korea
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    • v.17 no.3
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    • pp.152-157
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    • 2012
  • This investigation decribes the effect of the combustion and emission characteristics of HCNG engine according to the high purity hydrogen contents. The HCNG fuel was made by the mixture with a high purity hydrogen ($H_2$) and a natural gas. The test vehicle was applied to the bi-fuel (Gasoline and CNG) system and this system was modified from the fuel supply and fuel tank. In addition, the three premixed HCNG fuels with mixed rate of 10, 20 and 30% of hydrogen were used to maintain the safety. In order to analyze the combustion characteristics of HCNG and CNG, the fuel was injected in the combustor with constant volume. The exhaust emission from light duty vehicle with bi-fuel system was analyzed by a chassis dynamometer and emission analyzer. From these results, the reduction rate of NOx emission increased in the HCNG fuel and emission amount of THC and CO shows a similar level with CNG fuel. This study can be utilized the basic data for the development of a new business plans related with HCNG engines.

Syntheses, Solubilities and Thermal Properties of Polyamide-imides containing Bis(p-carbonylphenyl)diphenylsilane units (Bis(p-carbonylphenyl)diphenylsilane 단위를 함유한 폴리아미드-이미드의 합성과 용해도 및 열적성질에 관한 연구)

  • Un Sik Kim;Young Kiel Sung;Yoon Koo Sik
    • Journal of the Korean Chemical Society
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    • v.31 no.6
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    • pp.590-600
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    • 1987
  • Silicone-containing polyamide-imides were prepared from bis(p-chlorocarbonylphenyl)diphenylsilane (BCCDPS), pyromellitic dianhydride(PMDA) and diamines. The thermal characteristics of the above polymers had been carefully studied using a thermogravimetric analyzer. The thermal stability of polymer was decreased with increasing contents of bis(p-carbonylphenyl)diphenylsilane units(BCDPS). The effect of diamine on thermal stability of polymer led benzidine > m-phenylenediamine> 4,4'-diaminodiphenyl ether > 4,4'-diaminodiphenyl sulfone. The activation energy of degradation of polymer obtained by Friedman method increased as the contents of BCDPS in the polymer decreased. The degradation temperature of polymers generally increased as the activation energy increased. The solubility of polymer increased as the content of BCDPS increased except polymers prepared with benzidine.

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Influence of Carbon Black Contents and Rubber Compositions on Formation of Wear Debris of Rubber Vulcanizates

  • Choi, Sung-Seen;Yang, Seong Ryong;Chae, Eunji;Son, Chae Eun
    • Elastomers and Composites
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    • v.55 no.2
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    • pp.108-113
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    • 2020
  • Wear particles of the model tread compounds for bus and truck tires were made using a laboratory abrasion tester and characterized based on their size distributions, shapes, and crosslink densities. The influence of the carbon black contents and rubber compositions (NR= 100 and NR/BR= 80/20) on the production of wear particles was investigated. The wear particles were separated according to size using a sieve shaker. The shape properties of the wear particles were analyzed using an image analyzer and scanning electron microscopy (SEM). Their shapes were observed as tiny stick cookies or sausages with bumpy surfaces. The particle size distribution tended to be smaller with increasing carbon black content. Moreover, the particle size distributions of the NR = 100 samples were larger than that of the NR/BR blend samples. There were different filaments in the wear particles. The filament diameters tended to be thinner with increasing carbon black content. The crosslink density increased with increasing carbon black content, and the crosslink densities of the NR= 100 samples were lower than those of the NR/BR blend ones. The particle size distribution tended to be smaller with increasing crosslink density. Based on the experimental results, the wear particles can be produced by detaching debris from the main body through repetitive strain and recovery.

A Study on the Emission Characteristics of Syngas(H2/CO)-Air Premixed Flame according to the H2 contents (수소 함유량에 따른 합성가스(H2/CO)-공기 예혼합 화염의 배출특성 연구)

  • Jeong, Byeong;Choi, Jongmin;Lee, Keeman
    • 한국연소학회:학술대회논문집
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    • 2013.06a
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    • pp.9-10
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    • 2013
  • This study reports the results of an experimental investigation of emission and temperatures from the syngas-air premixed flame with a various mixture composition in the region of large equivalence ratios. The effects of hydrogen contents and equivalence ratios on the flame velocity, which reported before, and emission of syngas fuel are examined. In this study, representative syngas mixture compositions ($H_2:CO$) such as $H_2:CO=10:90$, 25:75, 50:50 and 75:25 and equivalence ratios from 0.5 to 5.0 have been conducted. The emissions of syngas fuel were measured by the high precision analyzer with enclosure configuration and the adiabatic temperatures are calculated by used Chemkin basis. The NOx emission level is coincided relatively well with the adiabatic temperature distributions in lean mixture conditions, but for rich mixture conditions NOx level was also increased again even though the adiabatic temperature decreases. Such an increasing characteristics in rich mixture conditions is coincided well with the tendency that rather the flue gas temperature increases.

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