• Restorative Dentistry and Endodontics
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• 제22권1호
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• pp.35-60
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• 1997

Physical properties of composite resins such as strength, resistance to wear, discoloration, etc, depend on the degree of conversion of the resin components. The clinical behavior of restorative resins varies brand to brand. Part of this variation is associated with the filler and differences in the polymer matrix. The polymer matrix of resins may differ because the involved monomers are dissimilar and because of variation in the catalyst system. The purpose of this study was to evaluate the degree of conversion of the composite resins according to the depth of cure and light curing time. 7mm diameter cylindrical aluminum molds were filled with each of five different hybrid light curing composite resins(Z-100, Charisma, Herculite XRV, Prisma TPH, Veridonfil) on the thin resin films. The molds were 1mm, 2mm, 3mm, 4mm, and 5mm in depth to produce resin films of various heights. Each sample was given 20sec, 40sec, and 60sec illumination with a light source. The degree of conversion of carbon double bonds to single bonds in the resin films was examined by means of Fourier Transform Infrared Spectrometer. The results were obtained as follows; 1. There was difference in the degree of conversion among five light curing composite resins according to the depth of cure for 20sec, 40sec, and 60sec illumination with light source with statistical significance(P<0.05). 2. Five light curing composite resins show lower degree of conversion at surface of the resin than depth of 1mm. 3. The degree of conversion of five light curing composite resins was siginificantly reduced from the maximum for the resin film when the light passed through as little as 1mm of each composite. 4. The degree of conversion of five light curing composite resins decrease significantly at the depth of 4mm, and polymerization was not occured at the depth of 5mm except for Prisma TPH. 5. The degree of conversion of five light curing composite resins was increased with increased light curing time, and there was no significant differences in the degree of conversion above 4mm in Z-100, 3mm in Charisma, and at depth of 5mm in Herculite XRV and Veridonfil(P>0.05).

• 대한소아치과학회지
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• 제29권3호
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• pp.423-429
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• 2002

최근 유동성 복합레진은 조작시 빠르고 간편하며 우수한 접근성으로 임상에서의 사용이 증가하고 있으나 각 제품간 그리고 혼합형 복합레진과의 물리적 성질이나 특성에 관한 비교 연구는 미흡한 실정이다. 이에 본 연구에서는 현재 임상적으로 자주 쓰이는 4종의 유동성 복합레진(Filtek Flow, Tetric Flow, Revolution, Palfique Esthelite LV high flow)의 압축 강도, 상대적 유동성, 방사선 불투과성을 측정하여 그 특성을 비교하여 다음과 같은 결론을 얻었다. 1. 압축강도에 있어서 4종의 유동성 복합레진 각 제품간의 유의한 차이는 없었으나 유동성 복합레진이 혼합형 복합레진(Z-100, 3M, USA)에 비하여 유의성 있게 낮은 압축강도를 나타내었다(p<0.001). 2. 각 제품간의 상대적 유동성은 Palfique Esthelite LV high flow, Revolution, Filtek Flow와 Tetric Flow 순으로 높았고(p<0.001), Filtek Flow와 Tetric Flow간에 유의한 차이는 없었으며, 모든 제품은 TeethmateF-1(Kuraray, Japan)에 비하여 유의성 있게 낮았다(p<0.001). 3. 유동성 복합레진 4종의 방사선 불투과성을 비교 분석한 결과 측정된 모든 유동성 복합레진은 상아질과 유사하거나 높은 방사선 불투과성을 나타내었고 각 제품간 유의한 차이가 있었다(p<0.001). 그 중 Tetric Flow와 Filtek Flow는 법랑질과 유사하거나 높은 방사선 불투과성을 나타내었다(p<0.001). 이상의 실험 결과는 4종의 유동성 복합레진은 혼합형 복합레진 보다 낮은 압축강도를 가지므로 임상에 적용 시 가해질 수 있는 응력을 고려하여야 하며, 각 제품간 유동정의 유의한 차이는 시술 시 재료의 선택에 고려사항이 될 수 있으리라 사료된다. 또한 4종의 유동성 복합레진의 방사선 불투과성은 모두 국제 인증 규격에 합당한 것으로 사료된다.

• 대한치과보존학회:학술대회논문집
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• 대한치과보존학회 2001년도 추계학술대회(제116회) 및 13회 Workshop 제3회 한ㆍ일 치과보존학회 공동학술대회 초록집
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• pp.585.1-585
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• 2001

The use of flowable composite resins as liners in class II packable composite resins has been suggested by some manufacturers. However, the contributions of this technique are unproven. Objectives: The aim of this study was to compare the gingival microleakage in class II packable composite restorations with or without the use of flowable composite resins as liners.. Method: Slot cavities were prepared on both proximals of 80 extracted human molars and randomly assigned to 8 groups of 20 each.(중략)

• 대한치과기공학회지
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• 제41권2호
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• pp.87-92
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• 2019

Purpose: The Purpose of this study is to compare the fracture strength of 4 kinds of direct composite resins. Methods: his study performed experiments on the fracture strength of direct composite resins after polymerizing 4 kinds of direct composite resins on the MOD cavity standard specimens. Results: The fracture strength of Aelite(Bisco) was the highest at 176.26N(p<0.05). According to post-hoc study with Turkey honest significant difference by multiple comparison on fracture strength test results, there were statistically significant differences between all kinds of direct composite resin. But the statistical difference between Z350(3M) and Spectrum(DP) was not significant. Conclusion: Aelite(Bisco) scored the highest concerning the fracture strength.

• 대한치과기공학회지
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• 제35권4호
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• pp.333-341
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• 2013

Purpose: The purpose of this study was to evaluate the flexural strength of indirect composite resins with different polymerization conditions. Methods: Ten specimens ($2mm{\times}2mm{\times}25mm$) of each composite resins (Tescera (T), Gradia (S) and Sinfony (S)) were fabricated by two polymerization methods : manufacturers's and light heat pressure. Composite resins polymerized by manufacturers's method and light heat pressure served as control (TS, GS and SS) and experimental groups (TE, GE and SE), respectively. The composite resins were tested for flexural strength and the surface of composite resins were observed with scanning electron microscope (SEM) under X1,000 magnification. Results: The flexural strength values of cured composite resin decreased in the following order: TE (195.4MPa), TS (179.8MPa), GE (169.9MPa), SE (137.7MPa), SS (111.1MPa) and GS (100.9MPa) groups. Conclusion: The flexural strength values between the control and the experimental groups were not significantly different although experimental groups showed higher flexural strength values than control groups.

• Restorative Dentistry and Endodontics
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• 제29권4호
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• pp.353-364
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• 2004

The purpose of this study was to compare and to evaluate the combination use of 5 kinds of dentin adhesive systems and 5 kinds of composite resins using micro-shear bond test. Five adhesive systems (Prime & Bond NT (PBN). Onecoat bond (OC), Excite (EX), Syntac (SY), Clearfil SE bond (CS)) and five composite resins (Spectrum (SP), Synergy Compact (SC), Tetric Ceram (TC), Clearfil AP-X (CA), Z100 (Z1)) were used for this study ($5{\;}{\times}{\;}5{\;}={\;}25group$, n =14/group). The slices of horizontally sectioned human tooth were bonded with each bonding system and each composite resin, and tested by a micro-shear bond strength test. These results were analyzed statistically. The mean micro-shear bond strength of dentin adhesive systems were in order of CS (22.642 MPa), SY (18.368 MPa), EX (14.599 MPa). OC (13.702 MPa). PBN (12.762 MPa). The mean bond strength of self-etching primer system group (CS, SY) in dentin was higher than that of self-priming adhesive system groups (PBN, EX, OC) significantly (P<0.05). The mean bond strength of composite resins was in order of SP (19.008 MPa), CA (17.532 MPa). SC (15.787 MPa), TC (15.068 MPa). Z1 (14.678 MPa). Micro-shear bond strength of SP was stronger than those of other composite resins significantly (P < 0.05). And those of TC and Z1 were weaker than other composite resins significantly (P < 0.05). No difference was found in micro-shear bond strength of composite resin in self-etching primer adhesive system groups (CS, SY) statistically. However, there was significant difference of micro-shear bond strength of composite resin groups in self-priming adhesive systems group (PBN, EX, OC). The combination of composite resin and dentin adhesive system recommended by manufacturer did not represent positive correlation. It didn't seem to be a significant factor.

• Restorative Dentistry and Endodontics
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• 제19권1호
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• pp.194-204
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• 1994

The purpose of this study was to evaluate the surface hardness of composite resins according to heat treatment. storage condition and storage time. In this study. two kinds of composite resin inlays and one kind of conventional posterior composite resin were used as experimental materials. One hundred eighty composite resin specimens were constructed from composite resin inlays and conventional posterior composite resin. The conditions of this study were heat treatment. storage condition and storage time. Hardness readings were taken from the top surface of each samples using the Vickers microhardness tester(MHT-l. Matsuzawa. Japan}. The following results from this study were obtained: 1. Regardless of storage condition. both composite resin inlay and conventional posterior composite resin have a higher surface hardness under heat treatment than not. 2. Composite resins with heat treatment have a higher surface hardness under dry storage than under water immersion. 3. In case of Clearfil Photo Posterior and Brilliant Enamel with heat treatment. there was no significant difference with time. but Clearfil CR Inlay with heat treatment. there was statistical difference after 24 hours. 4. Surface hardness of composite resins with coarse hybrid type was higher than that of composite resin with fine hybrid type.

• 대한치과보철학회지
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• 제45권6호
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• pp.805-814
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• 2007

Statement of problem. Composite resin-veneered metal restorations can be used as an alternative to porcelain-fused-metal restorations. But, because of the relatively low bond strength of veneering composite to metal framework, various surface treatment methods have been introduced to improve the bond strength. Purpose. The object of this study was to compare the shear bond strength of different combinations of each of the two bonding systems and each of the two composite veneering resins to cp-Ti/Co-Cr alloy. Material and methods. Two resin bonding systems (metal conditioner containing MEPS monomer, tribochemical silicoating system) and two composite resins (Gradia, Sinfony) were tested on cp-Ti and Co-Cr alloy. Then, according to manufacturers' instructions, resin bonding systems and composite resins were applied. All test specimens were divided into four groups for each alloy; I) sandblast + Metal Primer II + Gradia (MG), II) sandblast + Metal Primer II + Sinfony (MS), III) Rocatec + Gradia (RG), IV) Rocatec + Sinfony (RS). The shear bond strength was determined using a universal testing machine and all data were statistically analyzed with Mann-Whitney test and Kruskal-Wallis test at the significance level of 0.05. Results. The mean (standard deviations) of shear bond strength according to the combinations of two bonding systems and two composite resins to cp-Ti arranged from 16.44 MPa to 17.07 MPa and the shear bond strength to Co-Cr alloy ranged from 16.26 MPa to 17.70 MPa. The result shows that the difference were not statistically significant. Conclusion. The shear bond strengths of composite resins to both cast cp-Ti and Co-Cr alloy were not significantly different between the metal conditioner and the tribochemical silicoating system. And no differences in bond strength were found between cp-Ti and Co-Cr alloy.

• Journal of Mechanical Science and Technology
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• 제15권6호
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• pp.727-734
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• 2001

The Tribological evaluation of commercial dental composite resins containing prepolymerized particle fillers was investigated. Composite resins such as Metafil, Silux Plus, Heliomolar, and Palfique Estelite were selected as specimens. In the wear tests, a ball-on-flat wear test method was used. The friction coefficient of Metafil was quite high. The wear resistance of Silux Plus and Palfique Estelite was better than that of Metafil and Heliomolar under the same experimental conditions. The main wear mechanism of the composite resins containing prepolymerized particle fillers was abrasive wear caused by the brittle fracture of the prepolymerized particles and the debonding of the filler and the matrix.

• 대한치과보철학회지
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• 제29권3호
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• pp.171-179
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• 1991

The purpose of this study was to investigate the color stability of 3 porcelain repair composite resins Twenty specimens of each composite resin were made and ten specimens were polished at 10 minutes after polymerization, and the others were polished at 48 hours after polymerization. For 60 days, the color characteristics were measured by fiber-optic colorimeter (Model Tc-6FX, Tokyo Denshoku Co.). The obtained results were as follows: 1. The changes of $a^*$ value and $b^*$ value in composite resin polished at 10min. after polymerization were greater than those of composite resins polished at 48 hrs. after polymerization. 2. The $a^*$ values of all composite resins were increased and the $b^*$ values were decreased. 3. The $L^*$ values were decreased in composite resin manufactured by K & B Co., which were polished at 10min. after polymerization, but increased in composite resin manufactured by K & M Co., polished at 48 hrs. after polymerization.