• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2002년도 추계학술발표대회 논문집
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• pp.60-63
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• 2002

Metal/intermetallic laminated composites have been manufactured by SHS reactions between Ni and Al elemental metal foils. Microstructure showed that the intermetallic volume fraction was 55%, 45%, 35% in the 1:1, 2:1, 4:1 thickness ratio(Ni:Al) specimen and the main phases of the intermetallic were transformed from $Ni_2Al_3$ to NiAl when the thickness ratio was increased. Tensile strength and elongation were increased when the volume fraction of Ni metallic phase was increased. Under assumptions of isostrain condition, the tensile strength of metal/intermetallic laminated composites didn't obey the ROM due to the thermal residual stress and this was confirmed by X-ray residual stress analysis. Fracture toughness results by the SENB test showed R-curves with upward curvature based on LSB condition. Bridging stress based on LSB condition was determined by the curve fitting analysis, In-situ observed microstructure during fracture test showed that the various bridging mechanism such as crack bridging, crack branching and ductile failure of metallic layer were occurred

• 한국재료학회지
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• 제16권10호
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• pp.656-662
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• 2006

We fabricated thermal evaporated 10 nm-$Ni_xCo_{1-x}$ (x=0.2, 0.5 and 0.8) /(poly)Si films to form nanothick cobalt nickel composite silicides by a rapid thermal annealing at $700{\sim}1100^{\circ}C$ for 40 seconds. A field emission scanning electron microscope and a micro-Raman spectrometer were employed for microstructure and silicon residual stress characterization, respectively. We observed self-aligned micro-pinholes on single crystal silicon substrates silicidized at $1100^{\circ}C$. Raman silicon peak shift indicates that the residual tensile strain of $10^{-3}$ in single crystal silicon substrates existed after the silicide process. We propose thermal stress from silicide exothermic reaction and high temperature silicidation annealing may cause the pinholes. Those pinholes are expected to be avoided by lowering the silicidation temperature. Our results imply that we may use our newly proposed composite silicides to induce the appropriate strained layer in silicion substrates.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 1998년도 추계학술대회 논문집
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• pp.273-278
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• 1998

In this paper, basic micro-mechanical properties of unidirectional CFRP composite shell such as bonding strength, fiber volume fraction and void fraction are measured and tensile strength test is performed with a fixture. And then fracture surfaces are observed by SEM. In case of basic micro-mechanical properties, bonding strength is reduce with decreasing of radius of each ply in a shell for the effect of residual stress, fiber volume fraction is smaller than plate, and void fraction is vise versa. For these reason, tensile strength of shell is smaller than plate fabricated with same prepreg. For failure mode shell has many splitted part along its length, and it is assumed that this phenomenon is caused by the difference of bonding strength for residual stress.

• Composites Research
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• 제31권6호
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• pp.404-411
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• 2018

복합재료는 주어진 경화 사이클(cure cycle)로 오토클레이브 공정이 진행됨에 따라 수지의 화학수축, 열팽창계수 등에 의한 제품 내 잔류응력(residual stress)이 발생한다. 이로 인해 spring-in, warpage와 같은 열 변형이 발생하고 최종 제품의 수치 정확성이 감소한다. 구조물의 정밀한 제작이 요구되는 항공우주분야에서는 열변형으로 인한 문제를 해결하는 것이 중요하다. 따라서 복합재료의 경화과정을 예측하고 이해하기 위한 연구가 활발히 이루어지고 있다. 본 연구에서는 공정과정에 따른 복합재료의 경화메커니즘을 유한요소해석을 통해 예측하였고, 공정에 의해 발생하는 열변형에 대한 화학수축의 영향을 열팽창계수와 비교하여 분석하였다.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2000년도 춘계학술발표대회 논문집
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• pp.49-52
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• 2000

A new composite manufacturing technique which combines winding and curing together is studied and analyzed. This method is especially suited to the manufacture of thick composite materials in which thermal spiking is a common problem. An experimental apparatus was designed and built for use with a filament winder to continuously cure a thick composite cylinder. A hoop-wound composite cylinder with 152 mm wall thickness was manufactured and embedded thermocouples and strain gages were monitored throughout the cure process. The experimental data were compared with analytical results.

• Steel and Composite Structures
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• 제33권4호
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• pp.489-507
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• 2019

In order to obtain high bearing capacity and good ductility simultaneously, a structural column with hybrid normal and high strength steel (HNHSS) welded box section has been developed. Residual stress is an important factor that can influence the behaviour of a structural member in steel structures. Accordingly, the magnitudes and distributions of residual stresses in HNHSS welded box sections were investigated experimentally using the sectioning method. In this study, the following four box sections were tested: one normal strength steel (NSS) section, one high strength steel (HSS) section, and two HNHSS sections. Based on the experimental data from previous studies and the test results of this study, the effects of the width-to-thickness ratio of plate, yield strength of plate, and the plate thickness of the residual stresses of welded box sections were investigated in detail. A unified residual stress model for NSS, HSS and HNHSS welded box sections was proposed, and the corresponding simplified prediction equations for the maximum tensile residual stress ratio (${\sigma}_{rt}/f_y$) and average compressive residual stress ratio (${\sigma}_{rc}/f_y$) in the model were quantitatively established. The predicted magnitudes and distributions of residual stresses for four tested sections in this study by using the proposed residual stress model were compared with the experimental results, and the feasibility of this proposed model was shown to be in good agreement.

• 한국재료학회지
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• 제23권9호
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• pp.531-536
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• 2013

This paper investigates the effect of prolonged high temperature exposure on concentric laminated $Al_2O_3-ZrO_2$ composites. An ultrafine scale microstructure with a cellular 7 layer concentric lamination with unidirectional alignment was fabricated by a multi-pass extrusion method. Each laminate in the microstructure was $2-3{\mu}m$ thick. An alternate lamina was composed of 75%$Al_2O_3$-(25%m-$ZrO_2$) and t-$ZrO_2$ ceramics. The composite was sintered at $1500^{\circ}C$ and subjected to $1450^{\circ}C$ temperature for 24 hours to 72 hours. We investigated the effect of long time high temperature exposure on the generation of residual stress and grain growth and their effect on the overall stability of the composites. The residual stress development and its subsequent effect on the microstructure with the edge cracking behavior mechanism were investigated. The residual stress in the concentric laminated microstructure causes extensive micro cracks in the t-$ZrO_2$ layer, despite the very thin laminate thickness. The material properties like Vickers hardness and fracture toughness were measured and evaluated along with the microstructure of the composites with prolonged high temperature exposure.

• 대한기계학회논문집A
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• 제26권7호
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• pp.1384-1392
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• 2002

Single fiber pull-out technique has been commonly used to characterize the mechanical behavior of interface in fiber reinforced composite materials. An improved analysis considering the effects of transversely isotropic properties of fiber and the effects of thermal residual stresses in both radial and axial directions along the fiber/matrix interface is developed for the single fiber pull-out test. Although the stress transfer properties across the interface is not much affected by considering the transversely isotropic properties of fiber, interfacial debonding is notably encouraged by the effect. The interfacial shear stress that plays an important role in interfacial debonding is very much affected by the component of axial thermal residual stress in the bonded region, which can induce a two-way debonding mechanism.

• 대한기계학회논문집A
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• 제30권2호
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• pp.120-127
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• 2006

The fatigue behavior of LIPCA was so sensitive to the manufacturing condition, the environmental factors and the change of the test apparatus. Therefore, we could be considering not only the relationship between the stroke range $({\Delta}h)$ and actuating frequency but also the relationship between the stroke range $({\Delta}h)$ and the total effective moment $(M^E)$. Thus, this study proposed the calculation method of the applying $M^E$ when the $({\Delta}h)$ of LIPCA was increased from 1.mm to 20mm. To estimate the relationship between the total effective moment $(M^E)$ and the Bernoulli-Euler bending moment (M) was reviewed. And the residual stress distribution of LIPCA and THUNDER using the CLT was evaluated. In conclusions, converting the $({\Delta}h)$ of LIPCA to the radius of curvature (p) and calculating the $(M^E)$, it was found that the p by the $M^E$ changed similarly as the $({\Delta}h)$. It was found that the $M^E$ was 2.2 times as the M. While CFRP and PZT of LIPCA, which had the superior compressive characteristic, had the compressive residual stress, GFRP was subject to the tensile residual stress. Since this reversed configuration between the compressive residuals stress and the tensile one was made, the requirement of the stroke range $({\Delta}h)$ increase was satisfied.

• 폴리머
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• 제35권1호
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• pp.1-6
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• 2011

사출성형은 고온의 수지를 고압으로 금형에 충전하고 냉각하여 제품을 만드는 공정으로 큰 온도차이와 고압에 의해 성형품에 잔류응력이 형성된다. 이러한 잔류응력은 시간이 지남에 따라 이완되면서 제품에 변형을 일으켜 형상 품질을 저하시킨다. 본 연구에서는 광탄성 장치를 이용하여 투명한 사출성형품의 잔류응력을 측정하는 방법을 연구하였다. 빛은 전자파처럼 진행하는데 편광필름을 통과하면 하나의 파장만이 진행하게 된다. 그 파장이 시편을 통과하면서 시편에 존재하는 잔류응력 때문에 복굴절이 형성되고 두 번째 편광필름을 통과하면서 다양한 색의 패턴을 보이게 된다. 이 색의 패턴을 이용하여 사출성형으로 제작된 사각평판의 잔류응력을 정량적으로 측정하였다. 또한 컴퓨터 해석을 통해 사출성형품의 광학적 특성을 예측하였으며 실험과 비교하였다.