• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2004년도 추계학술대회논문집
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• pp.211-214
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• 2004

적절한 가공조건을 통하여, 중 탄소강에서 SIDT를 적용하여 페라이트-시멘타이트 미세조직이 압연 직후에 얻어졌다. 또한 이와 같은 조건은 압하온도 $690^{\circ}C$, 높이 감소율 $70\%$ (변형량 1.2) 및 변형율 속도 1/s에서 가공하였을 때 얻어졌으며, 가공 직후 $730^{\circ}C$로 승온하여 약 30분간 유지 후 서냉한 조건에서 매우 연한 미세조직이 얻어짐을 알 수 있었다. 이는 기존 20 시간 이상의 구상화 열처리에 비해 매우 짧은 시간이며, 구상화 열처리를 통한 경험한 미세조직과 유사한 특성을 나타낼 것으로 예상된다.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2009년 추계학술발표대회
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• pp.68-68
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• 2009

최근에 자동차 차체 경량화를 목적으로 개발된 고장력강의 용접품질 향상을 위해 인버터 DC 점용접기가 많이 사용되어지고 있다. 본 연구에서는 국내에서 개발된 인버터 DC 용접기를 사용하여 자동차용 590MPa 고장력 냉연강판(CR, SPFC 590RA)과 아연 도금 강판 (GA- EZFFC 590RA)의 용접품질을 평가하였다. 용접에 사용된 기본 조건은 인장 전단 시험을 통하여 결정하였으며, 동저항, 압흔 자국과 너겟 지름, 인장강도와의 관계를 통계적 방법으로 분석하였으며, 이를 활용하여 고장력 강판의 동저항과 압흔 자국에 따라 너겟 지름과 용접강도를 예측하는 비파괴적 용접 품질 평가 방법을 제시하였다.

• 수산해양기술연구
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• 제21권2호
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• pp.151-156
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• 1985

본 연구에서는 양쪽크랙 인장시험편을 이용한 평면응력 파괴인성치 J 하(1C)를 검토하기 위하여, 두께 4.5mm 일반구조용 압연강판(SS41)을 균질화 및 연화처리하고 각각의 경우에 대하여 크랙비가 0.55, 0.65, 0.75인 시험편을 준비하여 J 하(1C) 및 저항곡선의 거동을 고찰하였다. 얻어진 결과를 요약하면 다음과 같다. 1) 양쪽 크랙 인장시험편을 사용하여 J 하(1C)를 구한 값은 한계하중에 의한 방법이 Rice가 제안한 방법보다 크게 나타남을 알 수 있다. 2) Rice가 제안한 방법으로 J 하(1C)는 실험한 크랙비 범위 0.55-0.75에서 거의 일정한 값을 나타내고 저항곡선의 기울기는 크랙비에 따라 증가하였다. 3) Rice가 제안한 방법으로 [SS41의 J 하(1C)의 평균값은 모재는 22.8kgf/mm, 균질화 처리재는 24.7kgf/mm, 연화처리재는 26.9kgf/mm를 얻었다

• 한국해양공학회지
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• 제27권2호
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• pp.33-38
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• 2013

In the past, a very popular method for reducing the corrosion on zinc involved the use of chemical conversion layer coatings based on $Cr^{+6}$. However, there is an important problem with using chromium salts as a result of restrictive environmental protection legislation. This study investigated the optimum condition for galvanized steel using an organic/inorganic solution with a Ti composition. In the case of a fixed heat treatment time, the corrosion resistance values of LR-0727(1) and LR-0727(2) were improved as the heat treatment temperature increased, and the optimum minimum temperature decreased with the heat treatment time. At the optimum heat treatment condition of two coating solutions, the heat treatment time of the LR-0727(1) solution was shorter than LR-0727(2) for the same heat treatment temperature. LR-0727(1) coated specimens did not show desquamation, and all of the specimens showed a good adhesive property. In contrast, in the case of the LR-0727(2) coated specimens, desquamation arose. Therefore, the adhesive property of LR-0727(1) was superior to that of LR-0727(2). The pencil hardness had a 3H average for all of the coating solutions and heat treatment conditions. In the case of a corrosion resistance test with boiling water, the coated specimens of LR-0727(1) were discolored, but LR-0727(2) was not. Finally, LR-0727(1) was more moisture proof than LR-0727(2).

• 한국표면공학회지
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• 제49권2호
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• pp.202-210
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• 2016

This study was intended to investigate the effect of the amount of magnesium addition and heat treatment in the Al-Mg coating film in order to improve corrosion resistance of aluminum coating. Al-Mg alloy films were deposited on cold rolled steel by physical vapor deposition sputtering method. Heat treatment was fulfilled in an nitrogen atmosphere at the temperature of $400^{\circ}C$ for 10 min. The morphology was observed by SEM, component and phase of the deposited films were investigated by using GDLS and XRD, respectively. The corrosion behaviors of Al-Mg films were estimated by exposing salt spray test at 5 wt.% NaCl solution and measuring polarization curves in deaerated 3 wt.% NaCl solution. With the increase of magnesium content, the morphology of the deposited Al-Mg films changed from columnar to featureless structure and particle size was became fine. The x-ray diffraction data for deposited Al-Mg films showed only pure Al peaks. However, Al-Mg alloy peaks such as $Al_3Mg_2$ and $Al_{12}Mg_{17}$ were formed after heat treatment. All the sputtered Al-Mg films obviously showed good corrosion resistance compared with aluminum and zinc films. And corrosion resistance of Al-Mg film was increased after heat treatment.

• 한국표면공학회지
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• 제45권3호
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• pp.106-110
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• 2012

Oblique angle deposition (OAD) is a physical vapor deposition where incident vapor flux arrives at non-normal angles. It has been known that tilting the substrate changes the properties of the film, which is thought to be a result of morphological change of the film. In this study, OAD has been applied to prepare single and multilayer TiN films by cathodic arc deposition. TiN films have been deposited on cold-rolled steel sheets and stainless steel sheet. The deposition angle as well as substrate temperature and substrate bias was changed to investigate their effects on the properties of TiN films. TiN films were analyzed by color difference meter, scanning electron microscopy, nanoindenter and x-ray diffraction. The color of TiN films was not much changed according to the deposition conditions. The slanted and zigzag structures were observed from the single and multilayer films. The relation between substrate tilting angle (${\alpha}$) and the growth column angle (${\beta}$) followed the equation of $tan{\alpha}=2tan{\beta}$. The indentation hardness of TiN films deposited by OAD was low compared with the ones prepared at normal angle. However, it has been found that $H^3/E^2$ ratio of 3-layer TiN films prepared at OAD condition was a little higher than the ones prepared at normal angle, which can confirm the robustness of prepared films.

• 한국강구조학회 논문집
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• 제16권1호통권68호
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• pp.33-42
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• 2004

SN 강재를 건축구조용으로 사용하기 위해서는 설계기준강도가 제정되어야 한다. 선행 연구로써, SN400B/490B 후판재로 재판한 SN400B/490B 원형강관과 SPAP235/325 및 SPAR295 각형강관의 물성을 평가하였다. SN400B/490B 후판재와 비교했을 때 STKN400B/490B 원형강관의 항복인장 및 인장강도는 상승하였지만, 제조 프로세스에 무관하게 STKN400B/490B 원형강관의 규격을 만족 하였다. 그러나 SPAP235/325 각형강관 모서리부에서의 항복인장 및 인장강도는 규격을 벗어났다. 이것은 SPAP235/325 각형강관 규격에서 정하고 있는 값이 모서리부에서의 값이 아니라 변에서의 값이기 때문이다. STKN490B 원형강관에 발생한 최대 인장잔류응력은 모재 항복강도 수준이며, 최대 압축잔류응력은 모재 항복강도의 40% 수준이었다. 또한 SPAP325 각형강관에 발생한 최대 인장잔류응력과 최대 압축잔류응력은 모두 모재 항복강도의 80% 수준이었다. 중심압축실험을 한 결과 STKN490B 원형강관의 좌굴강도는 제조 프로세스에 관계없이 별 차이를 보이지 않았다. 그러나 각형강관의 경우는 SPAP325 각형강관이 SN490B로 built-up한 각형강관보다 좌굴강도가 높게 나타났다.

• Korean Chemical Engineering Research
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• 제56권3호
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• pp.327-334
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• 2018

출발물질로서 테트라에톡시실란(TEOS)과 메틸트리메톡시실란(MTMS)을 사용하여 졸-겔법에 의해 발수성 코팅용액을 제조하였다. 이 용액을 냉연강판 위에 스핀 코팅하고 열처리하여 비불소계 발수 코팅 도막을 제조 하였다. 이 과정 중 MTMS/TEOS의 몰 비, 물 농도 및 암모니아 농도가 코팅 도막의 발수성에 미치는 영향을 연구하였다. MTMS/TEOS의 몰 비를 1~20으로 변화시켜 제조 한 코팅 도막의 접촉각은 MTMS/TEOS 몰 비가 10 일 때 최대 수치인 $108^{\circ}$를 나타내었다. 반면에 물의 첨가량을 증가시킴에 따라 코팅 도막의 접촉각이 증가하여 발수성이 향상되었다. 또한 암모니아의 첨가량이 커질수록실리카입자의 크기가커져 실리카입자의표면 거칠기가증가하므로 발수성이 증가하였다.

• 한국마린엔지니어링학회:학술대회논문집
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• 한국마린엔지니어링학회 2005년도 후기학술대회논문집
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• pp.192-193
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• 2005

Magnesium thin films were prepared on cold-rolled steel substrates by RF(Radio Frequency) magnetron sputtering technique.$^{1)}$ The crystal orientation and monitoring of the deposited films were investigated by using XRD(X-ray Diffraction) and EIS(Electrochemical Impedance Spectroscopy), respectively. The corrosion rates of Mg thin films deposited with different argon gas pressure and substrate bias voltage were monitored by AC impedance method under a cyclic wet-dry condition, which was conducted by exposure to alternate conditions of 1h immersion in 3%NaCl solution and 5h drying at 60% RH and 25$^{\circ}C$. The result of corrosion rate of Mg thin films deposited at various Ar gas pressures and substrate bias voltage under wet-dry cyclic exposure in chloride-containing solutions was showed the following conclusions. At the region I during the onset of the wet cycle, corrosion rate showed relatively low value. The increase in the Corrosion rate of region II is due to the increase in the chloride concentration. Corrosion rate of region III during the onset of the cycle zero and salt crystals remain on the metal surface.$^{2)}$

• Journal of Advanced Marine Engineering and Technology
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• 제20권5호
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• pp.103-113
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• 1996

The properties of the deposited film depend on the deposition condition and these, in turn depend critically on the morphology and crystal orientation of the films. Therefore, it is important to clarify the nucleation occurrence and growth stage of the morphology and orientation of the film affected by deposition parameters, e.g. the gas pressure and bias voltage etc. In this work, magnesium thin flims were prepared on cold-rolled steel substrates by a thermo-eletron activation ion plating technique. The influence of nitrogen gas pressure and substrate bias voltage on their crystal orientation and morphology of the coated films were investigated by scanning electron microscopy (SEM) and X-ray diffraction, respectively. The diffraction peaks of magnesium film became less sharp and broadened with the increase of nitrogen gas pressure. With an increase in nitrogen gas pressure, flim morphology changed from colum nar to granular structure, and surface crystal grain-size decreased. The morphology of films depended not only on gas pressure but also on bias voltage, i.e., the effect of increasing bias voltage was similar to that of decreasing gas pressure. The effect of crystal orientation and morphology of magnesium films on corrosion behaviors was estimated by measuring anodic polarization curves in deaerated 3%NaCl solution. Magnesium, in general, has not a good corrosion resistance in all environments. However, these magnesium films prepared by changing nitrogen gas pressure showed good corrosion resistance. Among the films, magnesium films which exhibited granular structure had the highest corrosion resistance. The above phenomena can be explained by applying the effects of adsorption, occlusion and ion sputter of nitrogen gas.