• Asian-Australasian Journal of Animal Sciences
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• v.26 no.6
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• pp.864-873
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• 2013

In developing countries, biogas energy production is seen as a technology that can provide clean energy in poor regions and reduce pollution caused by animal manure. Laboratories in these countries have little access to advanced gas measuring equipment, which may limit research aimed at improving local adapted biogas production. They may also be unable to produce valid estimates of an international standard that can be used for articles published in international peer-reviewed science journals. This study tested and validated methods for measuring total biogas and methane ($CH_4$) production using batch fermentation and for characterizing the biomass. The biochemical methane potential (BMP) ($CH_4$ NL $kg^{-1}$ VS) of pig manure, cow manure and cellulose determined with the Moller and VDI methods was not significantly different in this test (p>0.05). The biodegradability using a ratio of BMP and theoretical BMP (TBMP) was slightly higher using the Hansen method, but differences were not significant. Degradation rate assessed by methane formation rate showed wide variation within the batch method tested. The first-order kinetics constant k for the cumulative methane production curve was highest when two animal manures were fermented using the VDI 4630 method, indicating that this method was able to reach steady conditions in a shorter time, reducing fermentation duration. In precision tests, the repeatability of the relative standard deviation (RSDr) for all batch methods was very low (4.8 to 8.1%), while the reproducibility of the relative standard deviation (RSDR) varied widely, from 7.3 to 19.8%. In determination of biomethane concentration, the values obtained using the liquid replacement method (LRM) were comparable to those obtained using gas chromatography (GC). This indicates that the LRM method could be used to determine biomethane concentration in biogas in laboratories with limited access to GC.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.18 no.9
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• pp.1-6
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• 2019

Preterm children require a controlled environment that is as close as possible to that inside the womb. Incubators are well equipped to fulfill this requirement; however, they are cumbersome and expensive, thereby restricting their portability and availability in less developed and rural areas. This research comprises the development and system validation of a portable incubator. The system consists of a collapsible baby enclosure that can be stowed inside the system base when not in use. The enclosure is made from acrylic such that it is easy to clean and allows unhindered visual observation of the occupant while being robust enough to withstand transit conditions. The system can be powered either by a mains supply or a 12-VDC automobile power supply. Additionally, it has an onboard battery to ensure a continuous supply during transit. A Peltier plate controlled using a microcontroller ensures the desired enclosure temperature irrespective of the ambient temperature. Built-in sensor probes can measure the skin temperature, pulse rate, blood oxygenation level, and ECG of the infant and display them on the system screen. The system function is validated by testing its peak power consumption and the heating and cooling performances of the environment control system.

• Korean Journal of Materials Research
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• v.29 no.7
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• pp.412-424
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• 2019

Global fitting functions for Fe-selective chlorination in ilmenite($FeTiO_2$) and successive chlorination of beneficiated $TiO_2$ are proposed and validated based on a comparison with experimental data collected from the literature. The Fe-selective chlorination reaction is expressed by the unreacted shrinking core model, which covers the diffusion-controlling step of chlorinated Fe gas that escapes through porous materials of beneficiated $TiO_2$ formed by Fe-selective chlorination, and the chemical reaction-controlling step of the surface reaction of unreacted solid ilmenite. The fitting function is applied for both chemical controlling steps of the unreacted shrinking core model. The validation shows that our fitting function is quite effective to fit with experimental data by minimum and maximum values of determination coefficients of $R^2$ as low as 0.9698 and 0.9988, respectively, for operating parameters such as temperature, $Cl_2$ pressure, carbon ratio and particle size that change comprehensively. The global fitting functions proposed in this study are expressed simply as exponential functions of chlorination rate(X) vs. time(t), and each of them are validated by a single equation for various reaction conditions. There is therefore a certain practical merit for the optimal process design and performance analysis for field engineers of chlorination reactions of ilmenite and $TiO_2$.

• Food Science of Animal Resources
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• v.39 no.1
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• pp.93-101
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• 2019

Nucleotides play important roles in numerous intracellular biochemical processes and are used in infant formulas and other dairy products. However, domestic analytical methods for assessing nucleotide content in products have not yet been established, and therefore, methods for determining nucleotide content are urgently required. A rapid and simple analytical method for determining the content of five types of nucleotides in dairy products was improved using solid phase extraction clean-up and high-performance liquid chromatography with diode array detector. The extraction solvent used in the AOAC method was not well dissolved and was changed to hydrophilic EDTA-Na. In addition, the results obtained using the isocratic elution method and a single wavelength were similar to those obtained using the AOAC method, and the time taken for analysis was shortened from 40 min to 25 min. The process of method validation revealed the following parameters: accuracy (84.69%-102.72%), precision (1.51%-6.82%), linearity (0.999), and limit of detection (cytidine 5'-monophosphate, 0.09 mg/L; uridine 5'-monophosphate, 0.11 mg/L; adenosine 5'-monophosphate, 0.12 mg/L; guanosine 5'-monophosphate, 0.11 mg/L; and inosine 5'-monophosphate, 0.14 mg/L). The method was also used to determine the nucleotide concentration in 25 samples (infant formulas, 1.99-29.39 mg/100 g; and cow milk, 0.28-0.83 mg/100 g). The newly improved method was appropriate for analyzing nucleotides in infant formulas and other dairy products faster when compared to conventional methods.

• Journal of Environmental Science International
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• v.28 no.4
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• pp.455-464
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• 2019

BAT-AEL(Best Available Techniques Associate Emission Level) is the basis for establishing permissible emission standards for the workplace. Therefore, it is necessary to formulate a regulated BAT-AEL setting methodology that is generally applicable to all relevant industries. For the BAT-AEL settings, various factors should be considered such as the pollutants item, whether the workplace is subject to integrated pollution prevention and control, whether BAT is applicable, the basic data type, the emission classification system, and the suitability of the collected data. Among these factors, it is the most important factor to establish the classification system for the emitting facilities such that the emission characteristics of an industrial facility and its pollutants can be effectively reflected. Furthermore the target of the survey workplace should adhere to the BAT guidelines, even if it is a workplace that is subject to an the integrated environmental system. Certified data (SEMS, TMS, cleanSYS, WEMS, etc.) can be used to prioritize the classification system for the emission facility and the emission levels of pollutants. However, the self-measured data, daily logs, and questionnaire data from the workplace can also be used upon agreement of the relevant TWG. The collected data should only be used only when the facility is operating normally. Data that have been determined to be outliers or inappropriate validation methods should also be excluded. The BAT-AEL can be establish by adhering to the following procedure: 1) investigate all relevant workplaces with in the industry, 2)select workplaces for integrated management, 3)Identify BAT application, 4)identify whether BAT is generally applicable, 5)establish a classification system for emitting facilities, 6)collection available data, 7)verify conformity, 8)remove of outliers, 9)prepare the BAT-AEL draft, 10)deliberate, and 11) perform the confirmation procedure.

• Journal of KIBIM
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• v.10 no.4
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• pp.22-31
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• 2020

Shop drawing tasks conducted after finishing coordinated or engineering design have great influences on the quality and cost of a project. However, despite the development of commercial BIM applications, shop drawings have mainly produced manually in certain engineering fields. Incorrect shop drawings with human errors have occurred various problems such as cost overrun, time delay and reworks. An automated shop drawing publishing from BIM is expected to resolve these problems. Despite attempts for automate shop drawing production, the field of mechanical, electrical and plumbing (MEP) is yet regarded challenging due to complexity of components and connection. In this research, we develop a process for automated producing 3D MEP shop drawings in BIM environment as following steps: to analyze conventional MEP shop drawing process, to identify detailed process that can be automated, to classify existing MEP objects and assign codes usable in BIM, and to develop an application. The validation of automated process is conducted against 10 clean room projects in which MEP is more complex and its cost is higher than other projects in terms of productivity and workers' satisfaction. Results show that the number of manpower for shop drawing is reduced by 30%, and the working time is shortened by 31%. Personal opinions of involved practitioners is interpreted as positive as the average rate of agrement on practicability, easy-to-use and necessary retouch tasks is around 66%.

• Journal of the Korean Geotechnical Society
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• v.24 no.6
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• pp.37-44
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• 2008

At low normal stress levels, tensile strength of sand characteristically varies with either saturation or suction of soil in an up-and-down manner with a peak tensile strength that can occur at any degree of saturation. A theory that accurately predicts tensile strength of wet sand was presented in the previous study. In this study, the results of uniaxial tensile, suction-saturation and direct shear tests obtained from three sands (Esperance sand from Seattle, Washington, clean sand from Perth, Australia, and Ottawa sand) are used to validate the proposed theory. The closed form expression of the proposed theory can predict well the experimental data obtained from these sands in terms of the variation patterns of tensile strength over the entire saturation regimes, the magnitude of the tensile strength, its peak value, and the corresponding degree of saturation when the peak strength occurs.

• Journal of Food Hygiene and Safety
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• v.38 no.3
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• pp.79-88
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• 2023

Trifludimoxazin is a triazinone herbicide that inhibits the synthesis of protoporphyrinogen oxidase (PPO). The lack of PPO damages the cell membranes, leading to plant cell death. An official analytical method for the safety management of trifludimoxazin is necessary because it is a newly registered herbicide in Korea. Therefore, this study aimed to develop a residual analysis method to detect trifludimoxazin in five representative agricultural products. The EN method was established as the final extraction method by comparing the recovery test and matrix effect with those of the QuEChERS method. Various sorbent agents were used to establish the clean-up method, and no differences were observed among them. MgSO₄ and PSA were selected as the final clean-up conditions. We used LC-MS/MS considering the selectivity and sensitivity of the target pesticide and analyzed the samples in the MRM mode. The recovery test results using the established analysis method and inter-laboratory validation showed a valid range of 73.5-100.7%, with a relative standard deviation and coefficient of variation less than 12.6% and 14.5%, respectively. Therefore, the presence of trifludimoxazin can be analyzed using a modified QuEChERS method, which is widely available in Korea to ensure the safety of residual insecticides.

• The Korean Journal of Pesticide Science
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• v.19 no.4
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• pp.345-353
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• 2015

The aim of this study is to develop residue analysis method for fenoxanil, a MBI (melanin biosynthesis inhibitor) propionamide fungicide, had mainly been used to control rice blast, and disease of other crops, fruits, and vegetables by using GLC/NPD and GC/MS. Extraction with acetone and partition with n-hexane/dichloromethane (80/20, v/v) were performed from hulled rice, soybean, Kimchi cabbage, green pepper, and apple, then column clean-up with florisil was applied. Mean recoveries were 82.2%-109.1% with less than 7.2% of coefficients of variation and limit of quantitation was set at the concentration of 0.04 mg/kg from the five agricultural products through the determination by GLC/NPD equipped with DB-5 capillary column and single laboratory validation. As a confirmatory method, GC/MS selected ion monitoring (SIM) was set from m/z 125.0, 188.9, and 293.0. Developed method is expected to apply the single residue analysis of fenoxanil in agricultural products.

• Korean Journal of Food Science and Technology
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• v.46 no.1
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• pp.7-12
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• 2014

A sensitive and simple analytical method to identify flutianil residues in agricultural commodities was developed and validated using gas chromatography-electron capture detection (GC-ECD) and mass spectrometry (GC-MS). The flutianil residues were extracted with acetonitrile, partitioned with dichloromethane, and then purified using a silica solid-phase extraction (SPE) cartridge. The method was validated using pepper, sweet pepper, mandarin, hulled rice, soybean, and potato spiked with 0.02 or 0.2 mg/kg flutianil. The average recovery of flutianil was 76.5-108.0% with a relative standard deviation of less than 10%. The limit of detection and limit of quantification were 0.004 and 0.02 mg/kg, respectively. The result of recoveries and relative standard deviation were in line with Codex Alimentarius Commission Guidelines (CAC/GL 40). These results show that the method developed in this study is appropriate for flutianil identification and can be used to maintain the safety of agricultural products containing flutianil residues.