• Title/Summary/Keyword: Chemical experiment

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A Study on Specific Qualities of Gold Alloy and its Components (금합금의 특수성질 및 성분에 관한 연구)

  • Shin, Mu-Hak
    • Journal of Technologic Dentistry
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    • v.2 no.1
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    • pp.11-15
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    • 1980
  • This study was aimed at obtaining an ideal gold alloy for dental prothetic. The experiment was on physical characteristics of gold alloy and mixing proportion for proper appliance to living tissues. The most frequently used material in the past for dental prothetic was gold, but recently used are mictures or precious metals and non-precious, which are proved to affect on oral tissues. The experiment was to examine gold alloy over its physical and chemical qualities and to make an ideal type of gold alloy by means of statistic and laboratory research.

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The Chemically Induced Hot Electron Flows on Metal-Semiconductor Schottky nanodiodes During Hydrogen Oxidation

  • Lee, Hyosun;Lee, Youngkeun;Lee, Changhwan;Kim, Sunmi;Park, Jeong Young
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.152-152
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    • 2013
  • Mechanism of energy conversion from chemical to electrical during exothermic catalytic reactions at the metal surfaces has been a fascinating and crucial subject in heterogeneous catalysis. A metal-semiconductor Schottky nanodiode is novel device for direct detection of chemically induced hot electrons which have sufficient energy to surmount the Schottky barrier. We measured a continuous chemicurrent during the hydrogen oxidation under of 760 Torr of O2 and 6 Torr of H2 by using Pt/Si and Pt/TiO2 nanodiodes at reaction temperatures and compared the chemicurrent with the reaction turnover rate. The thermoelectric current was measured by carrying out an experiment under O2 condition for elimination of the background current. Gas chromatograph and source meter were used for measurement of the chemical turnover rate and the chemicurrent, respectively. The correlation between the chemicurrent and the chemical turnover rate under hydrogen oxidation implies how hot electrons generated on the metal surface affect hydrogen oxidation.

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Development and Application Effect of Gas Concentration Measure Experiment for the Improvement of Elementary School Teachers' Concept on Combustion (초등교사의 연소 개념 향상을 위한 기체 농도 측정 실험 개발 및 적용 효과)

  • Kim, Eun-Young;Kim, Youngshin;Shin, Ae-Kyung
    • Journal of the Korean Chemical Society
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    • v.59 no.4
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    • pp.296-307
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    • 2015
  • The purposes of this study were to develop the experiment for gas concentration measure during combustion of a candle and to investigate the application effect of the experiment. For this study, 15 elementary school teachers were selected by considering their gender, career, 6th grade science teaching experience, and 6th grade science teaching experience according to 2007 revised s cience curriculum. The experiment using MBL is designed to confirm gas concentrations visually during the combustion of a candle which burns in an acrylic container. The experiment method is as follows. 1) Make two sets of holes in the container and then insert oxygen sensors and carbon dioxide sensors in the holes. 2) Burn a candle in the container and observe the changes in the burning of the candle. The experiment has checked oxygen concentration and carbon dioxide concentration in real-time and displays gas concentration changes by graphs. The results of the application effect of the experiment are as follows. Most elementary school teachers who had not had scientific concepts on combustion got acquainted with scientific concepts about ‘the reason why a candle is blown out when it is covered with a bottle’, and ‘the concentrations of oxygen and carbon dioxide before and after combustion’. In addition, about half of elementary school teachers got acquainted with scientific concepts about ‘the definition of combustion’, and ‘distribution of carbon dioxide during combustion’. Thus, the experiment to measure gas concentrations during combustion is helpful to improve elementary school teachers’ concepts on combustion.

The Effect of Organic Fertilizer According to the Duration and Amount of Soil Chemical Changes on Yield Components of Rice (유기질비료의 사용기간과 사용량에 따른 토양화학성변화와 벼의 수량구성요소에 미치는 영향)

  • Oh, Tae-Seok;Kim, Sung-Min;Kim, Chang-Ho
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.59 no.3
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    • pp.209-215
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    • 2014
  • The purpose of this study is identify chemical changes in yield components of soil using organic fertilizer for cultivating rice and establish reasonable methods of fertilization. In chemical change, comparing the control plot, the soil using organic fertilizer consistently for three years for cultivating rice showed an increase in pH and available phosphate in the experiment plots provided by the organic fertilizer, increase in spikelet number and 1000 grain weight in terms of yield components, and increase in yield in the three-year experiment plots. As for the quality of brown rice, the rate of head rice showed no difference when compared to that of the control plots. As for protein content, it was difficult to identify a statistical significance between the control plots and the experiment plots in 2009, but since 2010, the protein content of the experiment plots has been lower than that of the control plot, indicating that fertilization of organic fertilizer was effective in terms of rice quality. In conclusion, long-term use of organic fertilizer improved the chemical properties of soil and increased yield when compared to practical fertilization. Reasonable fertilization was identified to fertilize the nitrogen component of organic fertilizer to be a level of 12kg/10a.

Comparison of Volatile Compounds in Plant Parts of Angelica gigas Nakai by Extracting Methods (추출법에 따른 참당귀의 부위별 정유성분 비교)

  • Lim, Sang-Hyun;Park, Yu-Hwa;Ham, Hun-Ju;Kim, Hee-Yeon;Jeong, Heat-Nim;Kim, Kyung-Hee;Ahn, Young-Sup
    • Korean Journal of Medicinal Crop Science
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    • v.17 no.6
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    • pp.427-433
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    • 2009
  • Volatile flavor compounds from the shoot and root of Angelica gigas Nakai were extracted by HE (Hydrodistillation extraction), SDE (Simultaneous steam distillation & extraction), and SFE (Supercritical fluid extraction system), and analyzed by GC-MS. The amount and the number of chemical components in essential oils from shoot and root by SFE was the higher than those by other extraction methods. Respectively, thirty one constituents were identified from the essential oil of the shoot and root by HE, twenty seven and twenty three constituents were identified from the essential oil of shoot and root by SDE, thirty one and forty five constituents were identified from the essential oil of shoot and root by SFE. The result showed large differences in extraction methods and in plant parts of Angelica gigas Nakai. Also, the bioactive compounds in root part was identified as nodakenin and decursinol (11.95% and 8.42%, respectively) by SFE. These results suggested that SFE was the best extraction method for the increasing of extraction yield, the determination of volatile components and the increasing of bioactive compounds in the shoot and root of Angelica gigas Nakai.

Hydorgen Production by Catalytic Decomposition of Propane Over Cabon-Based Catalyst (탄소계 촉매를 이용한 프로판 분해 반응에 의한 수소 생산)

  • Yoon, Suk Hoon;Han, Gi Bo;Lee, Jong Dae;Park, No-Kuk;Ryu, Si Ok;Lee, Tae Jin;Yoon, Ki June;Han, Gui Young
    • Korean Chemical Engineering Research
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    • v.43 no.6
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    • pp.668-674
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    • 2005
  • It is reported that a method for the hydrogen production from the propane decomposition using carbon black as a catalyst is more effective than from the methane decomposition. Since the by-products like CO and $CO_2$ are not produced by the direct decomposition of propane, it is considered as an environmentally sustainable process. In this study, hydrogen was produced by the direct decomposition of propane using either commercial activated carbon or carbon black at atmospheric pressure in the temperature range of $500-1,000^{\circ}C$. Resulting products in our experiment were not only hydrogen but also several by-products such as methane, ethylene, ethane, and propylene. Hydrogen yield increased as temperature increased because the amount of those by-products produced in the experiment was inversely proportional to temperature. The achieved hydrogen yield at $750^{\circ}C$ with commercial DCC N330 catalyst was 22.47% in this study.

Application of Pulsed Field Gradient Long-range COSY-NMR for the Assignment of Geminal Protons on Rigid System: supplemental method of NOE Experiment (NOE 실험의 대용으로 응용될 수 있는 PFG Long-range COSY NMR 실험)

  • Lee, Sueg-Geun
    • Analytical Science and Technology
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    • v.18 no.1
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    • pp.85-88
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    • 2005
  • Antiphase character of cross peaks in long-range COSY is modulated by changing the fixed delay time and used to assign diastereotopic methylene protons on rigid systems which could produce unpredictable NOE phenomena because of complicate coupling spins.

Properties of Precursor Pitch Derived from Petroleum Residue

  • Yu, Hae-Il;Lee, Gyu-Dong;Gwon, Yeong-Bae
    • 한국기계연구소 소보
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    • s.15
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    • pp.37-46
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    • 1985
  • Properties of Precursor pitch derived from petroleum residue were studied physical and chemical analysis method for investigation of production of pitch fiber. For preparing of those precursor pitches it was carried out a temperature and time variation experiment i reactor. It was demonstrated the precursor pitch prepared in this study to have a similar properties to Ashland precursor pitch capable of bulk mesophase formation from the results of the basic analysis, that is, molecular weight distribution, coking yield, carbon content, chemical composition, etc.

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Pulsation and Particle Motion (脈動과 粒子運動)

  • Woong Ki Kang;Yong Wook Kim
    • Journal of the Korean Chemical Society
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    • v.7 no.1
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    • pp.47-50
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    • 1963
  • The effect of the pulsation on the particle hold-up in a pulsed wetted column has been studied theoretically for the case of laminar region and experimentally for the cases of transient and turbulent regions. The experiment has been carried out by employing water as fluid medium and solid particles. The pulsation has been given by the reciprocating motion of a piston. The results of the investigation show that the pulsation would not give apparent effect on the particle hold-up but would increase the total travelling length of the particle.

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