• Biotechnology and Bioprocess Engineering:BBE
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• v.7 no.6
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• pp.331-334
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• 2002

Culture conductivity and on-line NADH fluorescence were used to measure cellular growth in plant cell suspension cultures of Podophyllum hexandrum. An inverse correlation between dry cell weight and medium conductivity was observed during shake flask cultivation. A linear relationship between dry cell weight and culture NADH fluorescence was obtained during the exponential phase of batch cultivation In a bioreactor under the pH stat (pH 6) conditions. It was observed that conductivity measurement were suitable for biomass characterisation under highly dynamic uncontrolled shake flask cultivation conditions. However, if the acid/alkali feeding is done for pH control the conductivity measurement could not be applied. On the other hand the NADH fluorescence measurement allowed online-in situ biomass monitoring of rather heterogenous plant cell suspension cultures in bioreactor even under the most desirable pH stat conditions.

• Journal of Electrochemical Science and Technology
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• v.11 no.2
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• pp.165-171
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• 2020

The electrochemical preparation and spectroscopic characterisation of iridium-antimony (Ir-Sb) species is important owing to their potential applications as nanostructure materials. Nanostructures, i.e. nanoflower and nanodisk, of Ir-Sb were electrodeposited on conductive substrates using a practical electrochemical method based on the simultaneous underpotential deposition (UPD) of Ir and Sb from the IrCl₃ and Sb₂O₃ at a constant potential. Electrochemical UPD mechanism of Ir-Sb was studied using cyclic voltammetry and potential-controlled electrochemical deposition techniques. Herein, X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, X-ray photoelectron and Raman spectroscopy were used to determine the morphological and structural properties of the electrochemically-synthesised Ir-Sb nanostructures.

• Advanced Composite Materials
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• v.18 no.2
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• pp.167-185
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• 2009

Environmental problems caused by extensive use of polymeric materials arise mainly due to lack of landfill space and depletion of finite natural resources of fossil raw materials like petroleum or natural gas. The substitution of synthetic petroleum-based resins with natural biodegradable resins appears to be one appropriate measure to remedy the above-mentioned situation. This study presents the development of a composite that uses environmentally degradable starch-based resin as matrix and natural mineral basalt fibres as reinforcement, and investigates the fibre's and the composite's mechanical properties. The tensile strength of single basalt fibres was verified by means of single fibre tensile tests and statistically investigated by means of a Weibull analysis. Prepreg sheets were manufactured by means of a modified doctor blade system and hot power press. The sheets were used to manufacture specimens with fibre volume contents ranging from 33% to 61%. Specimens were tested for tensile strength, flexural strength and interlaminar shear strength. Composites manufactured during this study exhibited tensile and flexural strength of up to 517 MPa and 157 MPa, respectively.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2001.05a
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• pp.27-33
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• 2001

Linear harmonic analysis is a convenient and generally accurate method to use for the acoustic analysis of intake and exhaust silencers for IC engines. The major uncertainty in this form of modelling is the characterisation of the source, which is inherently nonlinear and time-variant. Experimental methods are generally used to determine the source characteristics, and in particular the indirect method is most suitable for an IC-engine source. With reference to an idealised linear time-variant source, it is found that the characteristics of a time-variant source as determined by the indirect method have no physical relevance. The direct method of experimental measurement appears to have some advantage over the indirect method, although in practice it is difficult to apply to an IC engine source. Again, an idealised linear time-variant source can be used to indicate that the characteristics of a time-variant source as determined by the direct method also have no physical relevance. Strangely, these meaningless measured source properties can nevertheless be used to accurately predict the radiated noise from an IC engine and silencer system.

• Smart Structures and Systems
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• v.4 no.2
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• pp.137-152
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• 2008

The work presented in this paper includes material characterisation and an investigation of suitability in seismic dampers for two commercially available NiTi-alloys, along with a numerical analysis of a new damper system employing composite NiTi-wires. Numerical simulations of the new damper system are conducted, using Brinson's one-dimensional constitutive model for shape memory alloys, with emphasis on the system's energy dissipation capabilities. The two alloys tested showed some unwanted residual strain at temperatures higher than $A_f$, possibly due to stress concentrations near inclusions in the material. These findings show that the alloys are not ideal, but may be employed in a seismic damper if precautions are made. The numerical investigations indicate that using composite NiTi-wires in a seismic damper enhances the energy dissipation capabilities for a wider working temperature range.

• Journal of the Korean Chemical Society
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• v.54 no.6
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• pp.717-722
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• 2010

Two derivatives of star shaped compounds based on naphthylamine with symmetric trisubstituted benzene as core, methoxy and ethoxy as end substitutions are synthesized. The synthesized compounds are characterized by UV-visible, FT-IR and NMR spectrometric techniques. The electronic and thermal properties of the compounds are studied using cyclic voltametry (CV) and differential scanning calorimetry (DSC) respectively. The data's obtained have similarity with the arylamines that have been already used in optoelectronic devices. So these compounds are interesting materials for applications in such devices.

• Proceedings of the KSPS conference
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• 1996.10a
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• pp.399-403
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• 1996

This paper addresses issues of perceptual constancy in speech perception through the use of a spatial metaphor for speech sound identity as opposed to a more conventional characterisation with multiple interacting acoustic cues. This spatial representation leads to a correlation between phonetic, acoustic and auditory analyses of speech sounds which can serve as the basis for a model of speech perception based on the general auditory characteristics of sounds. The correlations between the phonetic, perceptual and auditory spaces of the set of English voiceless fricatives /f $\theta$ s $\int$ h / are investigated. The results show that the perception of fricative segments may be explained in terms of 2-dimensional auditory space in which each segment occupies a region. The dimensions of the space were found to be the frequency of the main spectral peak and the 'peakiness' of spectra. These results support the view that perception of a segment is based on its occupancy of a multi-dimensional parameter space. In this way, final perceptual decisions on segments can be postponed until higher level constraints can also be met.

• Structural Monitoring and Maintenance
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• v.1 no.3
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• pp.309-322
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• 2014

Detection of fatigue cracks at an early stage of their development is important in structural health monitoring. The breathing of cracks in a structure generates higher harmonic components of the exciting frequency in the frequency spectrum. Previously, the residual operational deflection shape (R-ODS) method was successfully applied to beams with a single crack. The method is based on the ODSs at the exciting frequency and its higher harmonic components which consider both amplitude and phase information of responses to map the deflection pattern of structures. Although the R-ODS method shows the location of a single crack clearly, its identification for the location of multiple cracks in a structure is not always obvious. Therefore, an improvement to the R-ODS method is presented here to make the identification process distinct for the beams with multiple cracks. Numerical and experimental examples are utilised to investigate the effectiveness of the improved method.

• Bulletin of the Korean Chemical Society
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• v.35 no.10
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• pp.2929-2934
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• 2014

The reaction between $[CdBr_2{\cdot}4H_2O]$ and anhydrous $[ZnCl_2]$ with N,N'-bidentate N-(pyridin-2-ylmethylene)-cyclopentanamine (impy) in ethanol yields dimeric $[(impy)Cd({\mu}-Br)Br]_2$ and monomeric $[(impy)ZnCl_2]$ complexes, respectively. The X-ray crystal structure of Cd(II) and Zn(II) complexes revealed that the cadmium atom in $[(impy)Cd({\mu}-Br)Br]_2$ and zinc in $[(impy)ZnCl_2]$ formed a distorted trigonal-bipyramidal and tetrahedral geometry, respectively. Both complexes showed moderate catalytic activity for the polymerisation of methyl methacrylate (MMA) in the presence of modified methylaluminoxane (MMAO), with polymethylmethacrylate (PMMA) syndiotacticity of about 0.70.

• Mycobiology
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• v.39 no.2
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• pp.71-78
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• 2011

The phylogenetic relationships of the most dominant and morphologically cryptic endophytic fungal isolates from each of five selected medicinal plants, namely Potentilla fulgens, Osbeckia stellata, Osbeckia chinensis, Camellia caduca, and Schima khasiana of the biodiversity rich state of Meghalaya, were assessed with random amplification of polymorphic DNA and PCR-restriction fragment length polymorphism profiles. Sequencing of the internal transcribed spacer 1, small subunit rRNA and partial ${\beta}$-tubulin gene fragments was also conducted to determine the phylogenetic relationships of these isolates with fungal sequences available in Genbank, NCBI. The identity of the fungal isolates is suggested based on the molecular phylogenetic data.