• 대한기계학회논문집
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• 제17권6호
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• pp.1441-1455
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• 1993

본 연구에서는 최신기법에 의해서 제조된 HIP제 질화규소와 지르코니아를 실험재료로 하여 무윤활하에서의 미끄럼마찰·마멸실험을 수행하여 마찰·마멸특성을 규명하고, SEM을 이용한 마멸면의 미시적 관찰을 통해서 세라믹의 마멸기구를 조사하 여 세라믹마멸기구의 마멸모델을 제시하고자 한다. 제시된 마멸모델에서 파괴역학을 도입하여 이론해석과 고찰을 수행하여 보다 실용적인 세라믹의 마멸율울 평가할 수 있 는 새로운 무차원 파라메터를 제안하고자 한다.

• 대한치과보철학회지
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• 제40권6호
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• pp.572-576
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• 2002

This investigation was designed to estimate the biaxial flexure strength and fracture toughness of lithium disilicate glass-ceramics of IPS Empress 2 system pressed with as-received ingots and their sprue buttons. Two groups of the lithium disilicate glass-ceramics were prepared as follows: group 1 is ingot-pressed group; group 2 is sprue button-pressed group. A ball-on-three-ball test was used to determine biaxial flexure strength (BFS) of disks in wet environment. Scanning electron microscopy(SEM) analysis was conducted to observe the microstructure of the ceramics. Unpaired t-test showed that there were no differences in the mean biaxial Hem strength (BFS) and KIC values between group 1 and 2 (p > 0.05). Two groups showed similar values in the KIC and the strength at 5% failure probability. The SEM micrographs of the IPS Empress 2 glass-ceramic showed a closely packed, multi-directionally interlocking pattern of numerous lithium disilicate crystals protruding from the glass matrix. The lithium orthophosphate crystals could not be observed on the fracture surface etched. There was no a marked difference of the microstructure between group 1 and 2. Although there were no tests including color stability, casting accuracy, etc., the results of this study implied that we could reuse the sprue button of the pressed lithium disilicate glass-ceramic of IPS Empress 2 system.

• 한국분말재료학회지
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• 제26권5호
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• pp.415-420
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• 2019

SiAlON ceramics are used as ceramic cutting tools for heat-resistant super alloys (HRSAs) due to their excellent fracture toughness and thermal properties. They are manufactured from nitride and oxide raw materials. Mixtures of nitrides and oxides are densified via liquid phase sintering by using gas pressure sintering. Rare earth oxides, when used as sintering additives, affect the color and mechanical properties of SiAlON. Moreover, these sintering additives influence the cutting performance. In this study, we have prepared $Yb_{m/3}Si_{12-(m+n)}Al_{m+n}O_nN_{16-n}$ (m = 0.5; n = 0.5, 1.0) ceramics and manufactured SiAlON ceramics, which resulted in different colors. In addition, the characteristics of the sintered SiAlON ceramics such as fracture toughness and microstructure have been investigated and results of the cutting test have been analyzed.

• 한국분말재료학회지
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• 제28권5호
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• pp.381-388
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• 2021

Zirconia has excellent mechanical properties, such as high fracture toughness, wear resistance, and flexural strength, which make it a candidate for application in bead mills as milling media as well as a variety of components. In addition, enhanced mechanical properties can be attained by adding oxide or non-oxide dispersing particles to zirconia ceramics. In this study, the densification and mechanical properties of YSZ-TiC ceramic composites with different TiC contents and sintering temperatures are investigated. YSZ - x vol.% TiC (x=10, 20, 30) system is selected as compositions of interest. The mixed powders are sintered using hot pressing (HP) at different temperatures of 1300, 1400, and 1500℃. The densification behavior and mechanical properties of sintered ceramics, such as hardness and fracture toughness, are examined.

• 한국세라믹학회지
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• 제49권4호
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• pp.385-396
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• 2012

Thermal shock test methods and thermal shock parameters for ceramics were reviewed from the following viewpoints: (1) The test methods should be based on the precise estimation of both temperature and thermal stress distributions in a specimen taking into account the temperature-dependent thermo-mechanical properties; (2) The thermal shock parameters must be defined as a physical property of the materials and described as a function of temperature at the fracture point of the specimen; (3) The relation between the strength and fracture toughness of brittle ceramics under a thermal shock load must be the same as the relation under a mechanical load. In addition, appropriate thermal shock parameters should be defined by the thermal shock strength and thermal shock fracture toughness based on stress and energy criteria, respectively. A constant heat flux method is introduced as a testing technique suitable for estimating these thermal shock parameters directly from the electric power charged.

• 한국추진공학회:학술대회논문집
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• 한국추진공학회 2005년도 제24회 춘계학술대회논문집
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• pp.112-115
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• 2005

본 연구는 램제트 엔진의 돔포트 커버의 소재로 사용 될 첨단 그라스 세라믹(MACOR) 소재에 대한 동적 파괴인성 시험을 목적으로 한다. 다양한 노치반경의 시험편에 대하여 스트레인게이지법을 사용한 정적과 동적 파괴인성 시험을 수행하였다.

• 한국세라믹학회지
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• 제29권4호
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• pp.312-318
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• 1992

Two kinds of alumina specimens with different grain size (1 and 51 $\mu\textrm{m}$) but same density were prepared by hot-pressing. Fracture strength and fracture toughness of these specimens at low strain rate, sonic velocity, and elastic property were evaluated. Ballistic performance against Cal. 50 AP projectile was characterized by thick-backing method by using A16061-T6 reference block. Mechanical properties measured at low strain rate showed that the specimen with samll grain (SG) were better than specimen with large grain (LG). Fracture strength and fracture toughness of LG specimen were 131 MPa and 3.01 MPa{{{{ SQRT { m} }}, but those of SG specimen were 349 and 4.23, respectively. Sonic velocity and elastic properties of these specimen were similar, but bulk velocity and bulk modulus were different at amount of 4 and 9%. The tendency of ballistic performance was not consistent with the mechnaical properties at low strain rate. The ballistic performance based on quantitative efficiency revealed that the LG specimen (5.13) was ballistically better than the SG specimen (4.00) in spite of their lower mechanical properties.

• 한국세라믹학회지
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• 제28권10호
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• pp.785-792
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• 1991

An investigation of the crack propagation behavior of Al2O3-33Vol.% SiCw at 140$0^{\circ}C$ was conducted with various loading frequencies. Higher crack propagation was observed in lower frequency and higher load ratios. Interface sliding fracture due to glassy phase from the oxidation of SiCw and cavitation along grain boundary of diffusional creep appeared to be the main mechanism of fatigue fracture in slower crack propagation while interface sliding and whisker pull out aided by glassy phase formation played main role of fatigue fracture for higher crack growth condition. The frequency effect on deformation behavior was discussed with a Maxwell model.

• 한국세라믹학회지
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• 제31권7호
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• pp.772-776
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• 1994

Using two kinds of ZrO2 powder stabilized by 8 mol% and 3 mol% of Y2O3 several microstructures were designed; two single composition specimens of 8 mol% Y2O3-ZrO3 and 3 mol% Y2O3-ZrO2 and five mixture specimens with multi-layered structure and particulate mixture structure at a mixing ratio of 1:1 by weight. Electrical conductivities were measured from 250 to 75$0^{\circ}C$ in air using an impedance analyser, and fracture toughness at room temperature using the indentation method. Making the mixture structures was more effective in enhancing fracture toughness than electrical conductivity. At low temperatures 3 mol% Y2O3-ZrO2 showed the highest values in both electrical conductivity and fracture toughness, while at high temperature the specimens of alternately stacked planar and coarse granulated structure were most favorable.

• 한국세라믹학회지
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• 제44권4호
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• pp.189-193
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• 2007

Effect of additive composition on fracture toughness of in situ-toughened $SiC-Si_3N_4$ composites was investigated for five different additive compositions. The highest toughness $(6.4MPa{\cdot}m^{1/2})\;in\;SiC-Si_3N_4$ composites investigated herein was obtained when an Y-Mg-Si-Al-O-N oxynitride glass was used as a sintering additive. The improvement in fracture toughness was produced by enhanced bridging and deflection by $Si_3N_4$ grains.