• Title/Summary/Keyword: Ceramic body

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A Study on the P.T.C.R-N.T.C.R. Ceramic Resister (P.T.C.R.-N.T.C.R. 자기를 이용한 저항체에 관한 연구)

  • 안영필;이병하;김일기
    • Journal of the Korean Ceramic Society
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    • v.18 no.2
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    • pp.119-125
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    • 1981
  • The thermostable resistor was made by using P.T.C.R-N.T.C.R. ceramics. In this study $BaTiO_3$ type P.T.C.R. ceramics and $SnO_2-Sb_2O_3$ type N.T.C.R. ceramics were cocrystallized in one body and electrical resistance was stable under the temperature variation between $25^{\circ}C$-40$0^{\circ}C$. The ceramics showed the most stable electrical resistance for the mal variation when the composition was 0.6P.T.C.R. $BaTiO_3$,$ 0.4SnO_2$ and 0.01 $Sb_2O_3$.

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The Influence of Calcining and Sintering Conditions on the Properties of $YBa_2Cu_3O_{7-x}$ Superconducting Ceramics Prepared by the Polymeric Precursor Process (Polymeric Precursor법으로 제조한 $YBa_2Cu_3O_{7-x}$초전도세라믹스의 특성에 대한 하소 및 소결조건의 영향)

  • 석상일;오재희
    • Journal of the Korean Ceramic Society
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    • v.28 no.1
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    • pp.37-45
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    • 1991
  • The critical current density, electrical conductivity, critical magnetic field, Meissner effect, apparent density, and microstructure of YBa2Cu3O7-x ceramic superconductor prepared by polymeric precursor, while varing calcining and sintering conditions, were investigated. The best superconducting properties could be obtained from the body sintered at 93$0^{\circ}C$ for 10h after calcining at 90$0^{\circ}C$ for 10h, which gave 383A/$\textrm{cm}^2$ of critical current density(Jc), 96K of onset temperature(Tonset), 94. 8K of zero temperature (Tzero) 225 Oe of critical magnetic field (Hc1), 72.8% of superconducting volume fraction measured by Meissner effect and 6.28g/㎤ of apparent density.

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EFfect of Molding Temperature and Debinding Conditions on Fabrication of Alumina Component by Injection Molding (금형온도와 탈지조건이 사출성형에 의한 알루미나 부품 제조에 미치는 영향)

  • 임형택;임대순
    • Journal of the Korean Ceramic Society
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    • v.32 no.5
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    • pp.559-566
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    • 1995
  • Alumina powder was coated with stearic acid and then mixed with isotactic polypropylene, atactic polypropylene as binders at 15$0^{\circ}C$ for 2 hours. The mixture was then injection molded at various mold temperatures using injection molding machine to investigate the effect of the molding temperature and debinding parameters on the formation of the defects. The molded specimens were debinded in both air and nitrogen atmospheres. Wicking and solvent methods were also used to enhance debinding efficiency. The specimens were prefired at 120$0^{\circ}C$ and then sintered at 150$0^{\circ}C$ for 3 hours. Various defects were formed at mold temoperature of 3$0^{\circ}C$, 6$0^{\circ}C$ and 10$0^{\circ}C$ and any noticeable defect was not formed at 85$^{\circ}C$. The density of green body increased with mold temperature. Debinding in air atmosphere was more effective than in nitrogen atmosphere. Results also proved that wicking and solvent treatments helped minimize the number of defects.

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Solid State Sintering of Calcium Phosphate Ceramic Composites and Their Cellular Response

  • Cho, Yeong-Cheol;Kong, Young-Min;Riu, Doh-Hyung
    • Korean Journal of Metals and Materials
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    • v.50 no.9
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    • pp.691-695
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    • 2012
  • Calcium phosphate ceramic composites, consisting of hydroxyapatite(HA) and tricalcium phosphate (TCP), were fabricated by solid state sintering in order to investigate the effect of their initial compositions on microstructural evolutions and biocompatibility. All the sintered calcium phosphate ceramics exhibited almost full densification, while the grain growth of the composites increased with an increasing TCP content in the green body. The TCP phase transformed into a Ca-deficient HA phase during sintering via the diffusion of calcium ions from the HA phase into the TCP phase. The phases formed in the composites significantly affected the biocompatibility of the composites. The HA-matrix ceramic composites with TCP had a better cellular response than the pure HA ceramics, presumably due to the newly formed Ca-deficient HA.

Fabrication and Thermal Properties of Fumed Silica/Ceramic Wool Inorganic Composites (Fumed Silica/Ceramic Wool 무기복합재의 제조 및 열적 성질)

  • Ahn, WonSool
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.6
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    • pp.4007-4012
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    • 2014
  • This study examined the fabrication and thermal properties of fumed silica/ceramic wool inorganic composites. A predetermined quantity of fumed silica and ceramic wool was mixed uniformly into a slurry state and stabilized in the mold at room temperature, and converted to a massive foamed body through a complete drying process at $150^{\circ}C$. Although the samples without polyvinyl alcohol (PVA) as an interfacial adhesive showed a bulk density of 0.6-0.8 $g/cm^3$ in the range, 10-70wt% fumed silica, those samples with 3wt% PVA exhibited remarkably lower bulk densities with enhanced mechanical and thermal insulation properties, without thermal cracking even above $800^{\circ}C$. The K-factor of the samples was lower in proportion to the fumed silica contents, showing good thermal insulation properties of ca. 0.08 $W/m^{\circ}K$ at $500^{\circ}C$ for the sample with 30wt% fumed silica.

Effect of Mullite Generation on the Strength Improvement of Porcelain (Mullite 생성이 도자기 강도개선에 미치는 영향)

  • Choi, Hyo-Sung;Pee, Jae-Hwan;Kim, Yoo-Jin;Cho, Woo-Seok;Kim, Kyeong-Ja
    • Journal of the Korean Ceramic Society
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    • v.48 no.2
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    • pp.168-172
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    • 2011
  • Alumina powder was added in a general porcelain (Backja) with clay, feldspar and quartz contents to promote the mullite ($3Al_2O_3{\cdot}2SiO_2$) generation in the porcelain. Low melting materials ($B_2O_3(450^{\circ}C)$, $MnO_3(940^{\circ}C)$, CuO($1080^{\circ}C$)) were doped at ~3 wt% to modify the sinterability of porcelain with a high alumina contents and promote the mullite generation. Green body was made by slip casting method with blended slurry and then, they were fired at $1280^{\circ}C$ for 1hr by a $2^{\circ}C/min$. Densifications of samples with high alumina contents (20~30 wt%) were impeded. As the doping contents of low melting materilas increased, the sinterability of samples was improved. The shrinkage rate and bulk density of samples were improved by doping with low melting materials. Mullite phase increased with increasing the low melting contents in the phase analyses. This means lots of alumina and quartz were transformed into mullite phase by low melting contents doping. In the results, high bending strength of samples with high alumina contents was accomplished by improving the densification and mullite generation in the porcelain.

Mechanical Strength Values of Reaction-Bonded-Silicon-Carbide Tubes with Different Sample Size (튜브형상 반응소결 탄화규소 부품의 시편크기에 따른 강도평가 유용성 고찰)

  • Kim, Seongwon;Lee, Soyul;Oh, Yoon-Suk;Lee, Sung-Min;Han, Yoonsoo;Shin, Hyun-Ick;Kim, Youngseok
    • Journal of Powder Materials
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    • v.24 no.6
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    • pp.450-456
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    • 2017
  • Reaction-bonded silicon carbide (RBSC) is a SiC-based composite ceramic fabricated by the infiltration of molten silicon into a skeleton of SiC particles and carbon, in order to manufacture a ceramic body with full density. RBSC has been widely used and studied for many years in the SiC field, because of its relatively low processing temperature for fabrication, easy use in forming components with a near-net shape, and high density, compared with other sintering methods for SiC. A radiant tube is one of the most commonly employed ceramics components when using RBSC materials in industrial fields. In this study, the mechanical strengths of commercial RBSC tubes with different sizes are evaluated using 3-point flexural and C-ring tests. The size scaling law is applied to the obtained mechanical strength values for specimens with different sizes. The discrepancy between the flexural and C-ring strengths is also discussed.

Study on the Fabrication of Ceramic Core using a Gel-casting Process in Aqueous medium(I) : Gelation Behavior of Polydispered Ceramic Slip (수용액 매체에서 젤-케스팅 공정을 이용한 세라믹 코어 제조에 관한 연구(I) : 다성분계 분산 세라믹 슬립의 젤화 거동)

  • Kim, Jae-Won;Kim, Du-Hyeon;Kim, In-Su;Yu, Yeong-Su;Kim, Jae-Cheol;Jo, Chang-Yong
    • Korean Journal of Materials Research
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    • v.11 no.2
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    • pp.137-145
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    • 2001
  • A new process, gelcasting in aqueous medium, to fabricate complex-shaped ceramic core has investigated. The ceramic slurry, mixture of fused silica powder and additives such as zircon and cordierite, was electrosterically stabilizes. The slip was prepared by ball milling of polydispered ceramic suspension with monomer, dimer and dispersant. The rheological behavior of slip was evaluated by viscosity measurement. It was found that the high solid loading of polydispersed ceramic slip, which has low viscosity of 50vol%, is possible to obtained. The viscosity of the slip was significantly dependent upon the amount of polymer dispersant and the formulation of monomer and dimer. The green bodies were fabricated through casting and gelation at room temperature followed by drying at $25^{\circ}C$ for 48hrs under relative humidity of 80~85%. Crack-free green body was successfully fabricated through the above process.

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Crystal chemistry and growth of$La_3Ga_5SiO_{14}$ for the applications of filter and resonator (필터와 레죠네이터 응용을 위한 $La_3Ga_5SiO_{14}$ 의 결정화학 및 성장)

  • Jung, Il-Hyoung;Joo, Kyung;Shim, Kwang-Bo;Auh, Keun-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.1
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    • pp.74-79
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    • 1999
  • Langasite($La_3Ga_5SiO_14$) is a new piezoelectric material which is similar to quartz, LN($LiNbO_3$) and LT($LiTaO_3$) in its acoustic behavior. In this study, pure Langasite and Lagnasite family groups were synthesized by the solid state reactions in air. The diffusion species for synthesis were investigated and the sintered body was studied on dielectric property to comparison of characteristics. Also, Langasite single crystals were grown by self-designed Czochralski system and characterized.

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Fabrication of Double-layered Porous Materials (이중 기공구조를 갖는 다공질체의 제조)

  • Yun, Jung-Yeul;Kim, Hai-Doo;Park, Chun-Hong
    • Journal of the Korean Ceramic Society
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    • v.39 no.10
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    • pp.919-927
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    • 2002
  • In order to fabricate double-layered porous materials powders of different particle sizes were pressed stepwise. Ford's equation which predicts the fired density with the change in pressed density was employed in order to adjust the difference in sintering shrinkage of the green body with double-layered porous structure. Double-layered porous materials were characterized by investigating microstructures and permeability. SEM micrographs showed the distinct difference in pore sizes of double-layered porous material. Permeability of single-layered porous material increased by increasing the starting particle sizes and porosity as well. Permeability of the double-layered porous material depends largely on the layer of small pore diameter.