• Title/Summary/Keyword: Casting Process

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Effect of Chemical Parameters on Aqueous Acrylamide Gelcasting (수용성 Acrylamide 겔캐스팅에 대한 화학적 변수의 영향)

  • Yun, Seog-Eun;Woo, Sang-Kuk;Bae, Kang;Kim, Dong-Pyo
    • Applied Chemistry for Engineering
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    • v.10 no.5
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    • pp.748-753
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    • 1999
  • In gelcasting process of the Si powder slurry mixed with acrylamide monomers, it was characterized the effects of chemical parameters such as monomers and additives(polymerization initiator, catalyst and dispersant), Si powder and humidity at drying on processing parameters such as viscosity and idle time as well as on shrinkage and mechanical strength of green bodies. Generally, idle time decreased as initiator and catalyst amounts were increased, but rather depended on initiator. Idle times of the slurries greatly decreased to less than 1/2 time of the premix solutions in which gelation was delayed at higher MBAM portion as a crosslinking monomer. And fluidity of the slurries became worse at greater than 0.6 wt % dispersant. The green bodies showed only less than 7% of linear shrinkage without crack and distortion when dried for longer than 300 hrs under 98% humidity. Typically, the dried bodies containing 40, 50 vol % of Si powder displayed 64 and 36 Mpa in average, respectively.

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Development of Interactive Prototyping Methods applying Behavioral Prototyping Methods for Interactive Experience Design (인터랙티브 경험 디자인에 있어서 행위모형 기법을 응용한 인터랙티브 묘형 기법 개발)

  • 이태일
    • Archives of design research
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    • v.17 no.2
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    • pp.253-260
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    • 2004
  • As the need for more variety of interactive media grows, alternative interaction methods beyond conventional ones such as mice and keyboards are vigorously explored recently. In particular, these new approaches are getting attentions because they can enhance the user experiences in the interaction. Howerver, since they are case-dependent and specific, it still becomes crucial to consider and evaluate the effects and possibilities of interactions. The study aims to explore the ways to design the interactions by applying Behavioral Prototyping Methods in the initial stage of design development, which it calls 'Interactive Prototyping Method'. With the case project, 'Shadow Theater', which is an interactive installation for children, children can play and participate in interactive story-making by wearing hand puppets, casting shadows of hand puppets, and interacting with virtual objects on screen. To explore and design the interactions of Shadow Theater at the initial design process, the study builds an interactive prototype which borrows puppet theater settings and lets children play with hand puppets and other objects. The session of user try-outs with the prototype help to understand what and how they interact with virtual objects, and to improve the interactions.

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Effect of the Structure of the Smallest Poresize Layer on the Permeability of PES Microfiltration Membranes (최소 기공층 구조가 PES계 정밀여과막 투과 성능에 미치는 영향)

  • Kim, No-Won
    • Membrane Journal
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    • v.19 no.1
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    • pp.25-33
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    • 2009
  • PES (polyethersulfone) membranes with highly enhanced their asymmetry were prepared by phase inversion process. The membranes were prepared by using PES/DMF (N,N-dimethylformamide)/TSA (p-toluenesulfonic acid)/PVP (polyvinylpyrrolidone) casting solution and water coagulant. The pre-coagulation of membrane surface which was induced by an addition of TSA as a demixing agent and PVP as a swelling polymer in the PES solution and humid exposure time, played a crucial role in determining morphological properties and the PWP (pure water permeation) performance. The PES solution was coated on polyester film under condition of 80% humidity for a while ($72{\sim}144$ sec) before immersing in a coagulation bath. The characterization of membranes was carried out by a capillary flow porometer, a FE-SEM and a permeation test apparatus. As the thickness of the smallest pore size layer (SPL) decreased, the asymmetry of membrane increased under conditions of 20 wt% of TSA and 10 wt% of PVP in 11 wt% of PES solution during longer humid contact time. As a result, the membranes showed a remarkable increase of PWP.

A study on the fabrication technology of ceramic interconnect for the SOFC by wet process (습식법을 이용한 고체산화물 연료전지용 세라믹 연결재 제조 특성연구)

  • 이길용;김종희;송락현;백동현;정두환;신동열
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2003.03a
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    • pp.200-200
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    • 2003
  • 고체산화물 연료전지(SOFC)에서 사용되는 연결재의 주 기능은 각 단위 셀의 연료극과 다음 셀의 공기극을 전기적으로 연결하여, 공기와 사용연료의 분리역할을 하기 위하여 사용된다. SOFC용 연결재는 다른 구성요소 소재보다, 높은 전자 전도성, 낮은 이온전도성, 우수한 기계 적강도가 요구되며, SOFC는 고온에서 작동되기 때문에, 상온에서 작동온도까지 다른 요소 소재들과 유사한 열팽창계수와 물리, 화학적으로 안정성이 요구된다. 현재 연결재 제조기술은 EVD, CVD, plasma spraying, tape casting 등 다양하게 연구되고 있으며, 본 연구는 세라믹 연결재 증착방법 중 저렴한 비용으로 대량 생산이 용이한 습식법(dip coaling)을 적용하여, 연료극 지지체식 flat-tube형 고체산화물 연료전지의 지지체를 위해 세라믹 연결재를 제조하고, 그 특성을 연구하였다. 세라믹 연결재로써 선정한 합성조성은 LaCr $O_3$에 Ca이 치환 고용된 L $a_{0.6}$C $a_{0.41}$Cr $O_3$으로 pechini법으로 합성하였다. 합성된 조성은 100$0^{\circ}C$에서 5시간 하소후 가속 Ball Milling하여 0.5$\mu\textrm{m}$의 평균입자크기를 얻을 수 있었다. XRD 상분석결과 perovskite상 (L $a_{1-x}$ Ca/x/Cr $O_3$)과 CaCr $O_4$를 얻을 수 있었다. slurry를 제조하여 막의 밀착성을 증진시키기 위해 sand blasting시킨 flat tube지지체에 진공펌프를 이용하여 소재내부와 외부의 압력차로 dip coating한 후, 140$0^{\circ}C$로 소결 하였다. coating 결과 박리현상은 없었으나, 표면과 단면의 SEM분석결과 다소 porous한 박막층이 형성되었으며, Ca이온이 지지체로 permeation되는 현상이 발생하였다. 이와 같은 결과로부터 보다 치밀한 박막생성을 위해, slurry 제조조건을 변화시켰으며, Ca이온의 migration을 막기 위해 barrier layer를 이용하였다 완전 소결된 지지체는 가스투과도와 전기전도도측정을 통하여 특성을 평가하였다.였다.다.

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Microwave Dielectric Properties of Ti-Te system Ceramics for Triplexer Filter

  • Choi, Eui-Sun;Lee, Moon-Woo;Lee, Sang-Hyun;Kang, Gu-Hong;Kang, Gap-Sul;Lee, Young-Hie
    • Journal of Electrical Engineering and Technology
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    • v.6 no.2
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    • pp.263-269
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    • 2011
  • In this study, the compositions for the microwave dielectric materials were investigated to obtain the improved dielectric properties, the high temperature stability, and the sintering temperature of less than $900^{\circ}C$, which was necessary for cofiring with the internal conductor of silver. In addition, the dielectric sheets were prepared by the tape casting technique, after which the sheets were laminated and sintered. In this process, the optimum ratio of powder and binder, laminating pressure, temperature, and possibility for cofiring with the internal conductor were studied. Finally, multilayer chip treplexer filter for the 800-2,000 MHz range were fabricated, and the frequency characteristics of the triplexer filter were investigated. When the $0.6TiTe_3O_8-0.4MgTiO_3+3wt%SnO+7wt%H_3BO_3$ ceramics were sintered at $820^{\circ}C$ for 0.3 hours, the microwave dielectric properties of the dielectric constant of 29.91, quality factor of 33,000 GHz, and temperature coefficient of resonant frequency of -2.76 ppm/$^{\circ}C$ were obtained. Using the Advanced Design System (ADS) and High Frequency Structure Simulator (HFSS), the multilayer chip triplexer filter acting at the range of 800-2,000 MHz were simulated and manufactured. The manufactured triplexer filter had the excellent frequency properties in the CDAM800, GPS and PCS frequency regions, respectively.

A Study on Development of the Flask-Molds for Manufacturing of the Elbow Shape Shell Molds (엘보어 쉘주형 금형 개발에 관한 연구)

  • Choi, Jae-Hoon;Park, Jong-yeon
    • Design & Manufacturing
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    • v.7 no.1
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    • pp.45-49
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    • 2013
  • Since the shell-molds are used to make casting the metal parts for the automobile industry, the quality may well be inconsistent with the lower productivity, increasing the cost of the end products. The primary elbow design shell molded steel castings being produced through extrusion process has $180^{\varnothing}$ O.D., $150^{\varnothing}$ I.D., 14mm thickness and 400mm length, while being processed onto the left side of the tubing. The primary cause for the poor processing is the uneven manual shell molding. If the manual shell molds should be produced to have even quality, they would not be processed for tube linking. The purpose of this study was to develop the flask-molds for manufacturing of the shell molds to ensure mass-production, consistent quality, ommission of processing and comfortable working environment. For this purpose, four flask-molds were produced and thereby, four shell molds were assembled. In particular, the shell molds for processing were formed of the fine coated sand to be blown. As a result, productivity increased about three times, while a consistent quality was ensured. Furthermore, the tubes could be linked with each other without being processed, while pallets could be stacked, stored, transported and managed more easily. In a nut-shell, the molding theory could be applied more effectively. However, it is conceived that this study should be followed up by future studies which will research into reliability and endurability of the end products.

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Measurement of the intrinsic speed of sound in a hot melt ceramic slurry for 3D rapid prototyping with inkjet technology (3차원 잉크젯 쾌속 조형법을 위한 세라믹 상변화 잉크의 음속측정)

  • Shin, Dong-Youn
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.9 no.4
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    • pp.892-898
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    • 2008
  • 3D rapid prototyping is the manufacturing technology to fabricate a prototype with the data stored in a computer, which differs from conventional casting technology in terms of an additive process. Various 3D rapid prototyping techniques such as stereolithograpy. fused deposition modeling. selective laser sintering, laminated object manufacturing have been developed but among them, 3D inkjet printing has a unique feature that materials could be jetted to directly form the body of a prototype, which could be a finished product functionally and structurally. However, this needs ink with a high solid content, which tends to increase the dynamic viscosity of ink. The increase of ink viscositytends to restrict the jettable range of ink and hence the jetting conditions should be optimized. The intrinsic speed of sound in a hot melt ink with ceramic nanoparticles dispersed is one of key components to determine the jettable range of ink. In this paper, the way to measure the intrinsic speed of sound in a hot melt ceramic ink is proposed and its influence on the jetting condition is discussed.

Characteristics and Hair Growth Efficacy of Water Dissolving Micro-needles Containing Minoxidil Regarding Length of Micro-needles (미녹시딜을 내포한 용융형 고분자 마이크로 니들의 길이에 따른 특성 및 발모 효능 관찰)

  • Han, Mee-Ree;Kim, Eun-Young;Jung, Yong-Hyun;Kim, Myoung-Seok;Park, Jung-Hwan
    • Polymer(Korea)
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    • v.37 no.3
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    • pp.393-398
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    • 2013
  • Two types of polymeric micro-needles with 250 and $750{\mu}m$ lengths were prepared by a micromolding process. The geometry of dissolving micro-needles with minoxidil was investigated and the mechanical property of polymer micro-needles was also evaluated. Water dissolving micro-needles containing minoxidil were successfully inserted into skin and delivered minoxidil to the skin layer after 30 min of insertion. The observed hair growth was less when the minoxidil treatment was not applied or used without the micro-needles than that the minoxidil was applied by micro-needles. Histologically, these hair follicles became bigger, and the hair papillae were totally encircled by the hair bulbs. In this feasibility test, we show the successful delivery of minoxidil, and effective treatment of hair loss can be possible by using dissolving micro-needles with minoxidil.

Performance Study of Membrane Capacitive Deionization Process Applied by Perfluoropolymer and Aminated Poly(ether imide) Ion Exchange Membranes (불소화고분자와 아민화된 폴리이서이미드 이온교환막을 적용한 축전식 탈염공정의 성능 연구)

  • Kim, Ji Seon;Jeong, Joo Hwan;Rhim, Ji Won
    • Membrane Journal
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    • v.25 no.1
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    • pp.60-66
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    • 2015
  • To investigate the performance of the composite carbon electrodes which the ion exchange polymers were directly casted onto porous carbon electrode surfaces, the adsorption/desorption experiments were carried out by varying the feed concentration, feed flow rate, and desorption voltages for the NaCl solution. When the feed concentration was 100 mg/L, the increase of the adsorption time led to the increase of the salt removal due to the increase of the residence time inside the cell while the increase of the feed flow rate from 15 mL/min to 23 mL/min gave the decrease of the salt removal efficiency, 12% because of the short residence time. When the feed concentration was 200 mg/L, the salt removal was shown 10~15% low because of the incomplete desorption within the desorption intervals.

Fabrication of ACtA/$SiC_w$ composite by squeeze casting (I) (용탕 단조법에 의한 AC4A/Si$C_w$복합재료 제조에 관한 연구 (I))

  • Moon, Kyung-Cheol;Lee, Jun-Hee
    • Korean Journal of Materials Research
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    • v.2 no.6
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    • pp.461-467
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    • 1992
  • A fabrication process for SiC whisker preform reinforced AC4A Al composites is being developed. The Al alloy used as the matrix in this study is AC4A. SiC whisker preform made by Tokai Carbon Co. Ltd. Shizuoka, Japan were used. These consisted of $\beta$-type single crystals 0.1 ~ 10${\mu}$m in diameter and 20~10${\mu}$m in length. The most adequate fabrication condition was that whisker preform was preheated up to 750~80$0^{\circ}C$, set into a mould preheated to ~40$0^{\circ}C$, molten Al alloy heated to ~80$0^{\circ}C$ and applied pressure 75MPa. And Si$C_w$reinforced AC4A composite was advanced above twice than AC4AI/M. Also it was not large effect by pressure at Si$C_w$ 20v/o.

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