• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.123-126
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• 2007

Deformation behavior of $Zr_{55}Cu_{30}Al_{10}Ni_5$ (at. %) bulk metallic glass (BMG) fabricated by suction casting method has been investigated at elevated temperatures in this study. The BMG was first verified to have an amorphous structure thru X-ray diffraction (XRD) and differential scanning calorimetry (DSC). A series of compression tests has consequently been performed in supercooled liquid temperature region to investigate the high temperature deformation behavior. A transition from Newtonian to non-Newtonian flow appeared to take place depending upon both the strain rate and test temperature. A processing map based on a dynamic materials model has been constructed to estimate a feasible forming condition for this BMG alloy.

• KIEE International Transactions on Electrophysics and Applications
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• v.4C no.2
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• pp.51-54
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• 2004

In this paper, the thermal and mechanical properties of elastic epoxy for the application of high voltage products were investigated. Glass transition temperature (Tg) of elastic epoxies cannot be found from room temperature to 20$0^{\circ}C$ by DSC (Differential Scanning Calorimetry). Weight reduction occurred at 285$^{\circ}C$ and 451$^{\circ}C$ according to a thermogravimeter. The first temperature was affected by addictives and the second by epoxies characteristic. Maximum tensile strain showed 28.3kgf/$\textrm{cm}^2$/$\textrm{cm}^2$ at 20% of mechanical stress in addictives 35 (phr). The SEM (Scanning electron microscope) micrograph of the fracture surface observed void and tearing of elastic epoxy at addictives 35 (phr). On the other side, the SEM micrograph of the rigid epoxy showed a broken trace.

• Proceedings of the KIEE Conference
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• 1999.07d
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• pp.1575-1577
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• 1999

XLPE is widely used as a main insulation in EHV power cables, deeply connected with thermal stress. In this study, the thermal history of XLPE insulation was examined using DSC(Differential Scanning Calorimetry). The principle is on the basis of the phenomenon that crystal in polyethylene is rearranged as it is annealed near/below the melting temperature. From the result, it was possible to define accurate temperature which was really applied on the XLPE insulation and this method was assured as a useful tool in characterization of thermal history in XLPE cable insulation.

• Proceedings of the KIEE Conference
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• 2004.07c
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• pp.1667-1669
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• 2004

In this paper, the elastic epoxy added elastomer having viscoelasticity to existing epoxy was measured thermal, structural properties by DSC (Differential Scanning Calorimetry) and FESEM (Field Emission Scanning Electron Microscope). Specimens were made of dumbbell forms by the ratio of 5, 10, 15, and 20[phr] by regulation with elastomer contents. The measurement temperature dimensions of DSC were -20[$^{\circ}C$] to 150[$^{\circ}C$] and rising temperature was 4[$^{\circ}C$/min]. Also we observed structure through FESEM at the magnification of 1000 times with the voltage of 15[kV] after breaking by quenching specimens. As experimental results, we could know that thermal and structural properties were improved quantity according to decrease of elastomer contents. Namely, it increased glass transition temperature, high temperature, and matrix structure. In general, thermal, structural properties of 15[phr] was excellent among the specimens.

• Proceedings of the Korea Institute of Fire Science and Engineering Conference
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• 1996.11a
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• pp.43-48
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• 1996

It is considered that automobile inner space is dangerous due to its combustion characteristics. (Automobile interior is largely made by plastic materials.) At last it is necessary to study on combustion characteristics of automobile interior. we could obtain its rapid combustion velocity and high smoke density by using ASTM D 2863 apparatus, DSC (Differential Scanning Calorimetry), Smoke density apparatus and so on. The study is summerized by following conditions and results. 1. Sample size was 150mm(length)$\times$60mmwidth). 2. Combustion velocity appeared peak point in the 2cm point. 3. PVC and foam layers are important factors in the face of smoke density. 4. Using DSC, we obtained the point that automobile interior was melted. 5. Automobile interior should be improved because of its low L.O.I value and rapid flame propagation velocity.

• Journal of Pharmaceutical Investigation
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• v.39 no.3
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• pp.173-176
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• 2009

A new crystal form of valsartan dipotassium was isolated by recrystallization using the one-pot method. The new crystal form was identified as a monohydrate form ($C_{24}H_{27}N_5O_3K_2.H_2O$) and characterized by diffential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and X-ray powder diffractometry (PXRD). The new crystal data demonstrated to be clearly different from those known for the tetrahydrate form ($C_{24}H_{27}N_5O_3K_2.4H_2O$). It was observed that the monohydrate of vasartan dipotassium salt was completely dissolved in water within 1 hour and its dissolution rate was much faster than anhydrous free form of valsartan.

• Korean Journal of Materials Research
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• v.1 no.3
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• pp.145-150
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• 1991

Crystallization and embrittlement of $Fe_{78}B_{13}Si_{9}$ amorphous alloy was investigated by differential scanning calorimetry, X-ray diffraction and transmission electron microscopy. The crystallization comprizes two exothermic processes. In the first crystallization stage, $\alpha$-(Fe, Si) dendrites are formed from the amorphous state, and in the second crystallization, $Fe_2B$ compounds are formed. An abrupt decrease of the fracture strain of the ribbon started from amorphous started annealed at about $340^{\circ}C$

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.10a
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• pp.323-327
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• 2009

Silicone is recently used for LED chip encapsulment due to its good thermal stability and optical transmittance. In order to predict residual stress which causes optical briefringence and mechanical warpage of silicone, finite element analysis was conducted for both curing and cooling process during silicone molding. For analysis of curing process, a cure kinetics model was derived based on the differential scanning calorimetry(DSC) test and applied to the material properties for finite element analysis. Finite element simulation result showed that the curing as well as the cooling process should be designed carefully so as to reduce the residual stress although the cooling process plays the bigger role than curing process in determining the final residual stress state.

• Proceedings of the Korean Society of Dyers and Finishers Conference
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• 2008.04a
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• pp.114-116
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• 2008

Poly(${\varepsilon}$-caprolactone) nanocapsules(nanoPCL) containing phytoncide oil were synthesized by emulsion diffusion method using ethyl acetate as organic solvent. The influence of the degree of hydrolyzation of poly(vinyl acohol) used as an emulsion stabilizer, and the different weight ratio of core material to wall material on the particle size, morphology, and emulsion stability was investigated to design nanocapsules. The encapsulated nanoPCL were characterized by FT-IR spetrometry, Scanning electron microscope, Differential scanning calorimetry, and Thermogravimetry analysis, respectively.

• The Korean Journal of Food And Nutrition
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• v.24 no.4
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• pp.602-606
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• 2011

찹쌀전분의 고압처리시 pH 3~10 조건에서 고유점도는 1.328~1.426 ml/g 범위로 원료전분(1.15 ml/g)보다 낮았다. 특히, 고유점도는 산성 및 알칼리성 조건에서 감소하였다. 전분의 호화과정 중 열에너지량을 나타내는 호화엔탈피는 pH 3, 4 및 5 조건에서 고압처리한 찹쌀전분이 각각 13.86, 13.47 및 13.42 J/g으로 원료전분(16.3 J/g)보다 낮은 값을 보였다. 찹쌀전분의 호화온도 및 엔탈피 감소는 고유점도가 낮아지는 현상과 일치하였다.