• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 1999년도 춘계학술대회논문집
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• pp.119-124
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• 1999

Quantitative evaluation of the tribological conditions at the tool-workpiece interface in metal forming is usually accomplished by the ring-compressinon. test This paper describes an experimental investigation into shear friction factor under cold and hot forming conditions according to materials and lubricants using the ring compression test. Six different materials and five different lubricants were applied in the experiments. calibration curves with the friction coefficient were obtained using FEM analysis and verified by the verified by the experimental results. The influence of materials and lubricants level on friction are discussed. In the ring compression test the shear friction factor has a different from steels and aluminum water base graphite lubricants on cold working conditions and hot working conditions.

• 한국환경과학회지
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• 제12권1호
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• pp.87-92
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• 2003

Synchronous spectrofluorimetry was carried out for the simultaneous determination of various polycyclic aromatic hydrocarbons(PAHs) in aqueous solution by fluorescence spectrometry have been studied. The optimal wavelength interval(${\triangle}{\lambda}$) for synchronous spectra of acenaphthene, anthracene, benzo[a]anthracene, fluorene and pyrene were investigated in the presence of surfactants. The great enhancement of the fluorescence of these PAHs in Triton X-100 was obtained and optimal wavelength was 50 nm. The calibration curves in synthetic mixture solution of 5 PAHs were linear over the range from $1.0{\times}10^{-8}M$ to $1.0{\tiems}10^{-4}M$. Under the optimal experimental conditions, the detection limits were $4.9{\tiems}10^{-9}M$,\;7.0{\times}10^{-9}M,\;4.7{\tiems}10^{-9}M,\;1.6{\tiems}10^{-9}M$ and $3.2{\tiems}10^{-9}M$ for acenaphthene, anthracene, benzo[a]anthracene, fluorene and pyrene, respectively.

• 대한기계학회논문집B
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• 제25권9호
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• pp.1201-1208
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• 2001

Variable temperature anemometer(VTA) has greater sensitivity than a conventional constant temperature anemometer(CTA). In order to design a reliable VTA system, however, an elaborate photoconductive cell stabilizing circuit which plays a key role in setting wire-overheat ratio should be firstly developed. In this study, a stabilizing circuit which adopts proportional-integral analog controller was proposed and thoroughly tested for its accuracy and reproducibility. In contrast to the available circuit suggested by Takagi, the present circuit has characteristic that the resistance of a photoconductive cell increases with the increase of input voltage, which makes the current circuit very suitable for the design of VTA. Finally, VTA adopting stabilizing circuit was made and the enhanced sensitivity of the VTA was validated experimentally by comparing the calibration curves of VTA and CTA.

• 한국지하수토양환경학회:학술대회논문집
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• 한국지하수토양환경학회 2003년도 총회 및 춘계학술발표회
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• pp.111-114
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• 2003

A new monitoring system has been developed for in-situ and realtime measurement of ozone transport in unsaturated porous media using a fiber optic sensor. The calibration of the fiber optic transflection dip probe (FOTDP) system was successfully carried out at various ozone concentrations using a column with length of 30 cm and diameter of 5 cm packed with glass beads, which don't react with gaseous ozone. The breakthrough curves (BTCs) of ozone was obtained by converting the normalized intensity into ozone concentration. The FOTDP system reflected the ideal transport phenomena of gas phase ozone at various flow rates. The FOTDP system worked well for in-situ monitoring of gas phase ozone at various water saturations and in presence of SOM. However, the FOTDP system did not measure the ozone concentration at more than 70% water saturation.

• 분석과학
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• 제8권4호
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• pp.419-425
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• 1995

A method has been investigated for the determination of selenium and tellurium in Ginseng, Ganoderma and Garlic using hydride generation atomic absorption spectrometry(HG-AAS). The concentration effects of hydrochloric acid and sodium tetrahydroborate on the hydride generation for the determination of selenium and tellurium were investigated. The method of sample decomposition was also investigated using various mineral acids, such as nitric, perchloric and sulfuric acid in the closed system, and foreign ion effects containing in the samples were studied. The calibration curves of selenium and tellurium were obtained in the range of 0~40 ppb. The detection limits(S/N=2) of selenium and tellurium are 0.1 and 0.2 ppb. Analytical data of selenium and tellurium in Garlic, Ganoderma and Ginseng are 289, 296 and 198 ng/g for selenium and 146, 127 and 110 ng/g for tellurium, respectively.

• 대한한의학방제학회지
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• 제18권2호
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• pp.251-257
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• 2010

Objectives : To develop and validate High-performance liquid chromatography-photodiode array methods for simultaneous determination of two constituents in Oryeong-san(ORS). Methods : Reverse-phase chromatography using a Gemini C18 column operating at $40^{\circ}C$, and photodiode array(PDA) detection at 280 nm, were used for quantification of the two marker components of ORS. The mobile phase using a gradient flow consisted of two solvent systems. Solvent A was $H_2O$ and solvent B was acetonitrile. Results : Calibration curves were acquired with correlation coefficient ($r^2$)>0.9999, and the relative standard deviation(RSD) values(%) for intra- and inter-day precision were not exceed 1.0%. The recovery rate of each compound was in the range of 93.01-104.16%, with an RSD less than 2.0%. The contents of two compounds in ORS were 1.10-3.72 mg/g. Conclusions : The established HPLC method will be helpful to improve quality control of ORS.

• 한국전자파학회논문지
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• 제8권5호
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• pp.525-533
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• 1997

건축연구에서의 수분측정 방법을 개선하기 위하여 비파괴적인 수분측정기술을 응용하였다. 본 실험은 연속적이고 비파괴적인 측정에서의 핵심요소로서 자유공간에서의 혼 안테나를 사용하여 실험하였으며 사용한 기술은 마이크로파 브릿지 장치로서 9.5GHz의 주파수에서 함수율이 1~12% 범위의 모래수분을 측정하였다. 이로부터 대표적인 교정곡선을 구하였다. 이를 바탕으로 마이크로파를 이용한 석탄, 제지, 식품 미치 건축재료 등과 같은 비금속내의 수분측정이 가능함을 보였다.

• 한국식품영양과학회지
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• 제28권4호
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• pp.882-885
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• 1999

Along with the increasing demands for food irradiation technology, proper detection methods for controlling irradiated foods are required. Dried vegetable(chunggyungchae), which is permitted to be irradiated in Korea, was subjected to a detection study by ESR spectroscopy. Pre established threshold value was successfully applicable to the detection of 50 coded unknown samples of dried clean vege tables, both nonirradiated and electron beam irradiated. Three calibration curves obtained from the samples irradiated at 2.5~15 kGy were not practically adopted to estimate actual absorbed doses ranging from 4 to 7 kGy.

• 약학회지
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• 제46권4호
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• pp.231-236
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• 2002

A high-performance liquid chromatographic method for the simultaneous quantitative analysis of methylparaben (MP), ethylparaben (EP), propylparaben (PP), butylparaben (BP) and imidazolidinyl urea(IU) or diazolidinyl urea(DU) in cosmetics was studied by using a cyano-propyl column and 0.05M hexanesulfonic acid at 228 nm. Calibration curves were found to be linear in the 60-1000 $\mu\textrm{g}$/mL range (parabens), 100-1,250 $\mu\textrm{g}$/mL range (IU) and the 120-2000 $\mu\textrm{g}$/mL range (DU). Linear regression analysis of the data demonstrates the efficacy of the method in terms of precision and accuracy. An extraction method is developed and validated in order to apply this chromatographic method to a commercial cosmetic cream. The precision of this method, calculated as the relative standard deviation (RSD) of the recoveries (0.46-2.71％) was excellent for all compounds.

• 약학회지
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• 제47권4호
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• pp.195-199
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• 2003

An analysis method for the determination of methylendedioxymethamphetamine (MDMA) and its metabolite methylendedioxymethamphetamine (MDA) in hair by gas chromatography/mass spectrometry was proposed. For MDMA and MDA analysis, hair samples were incubated in MeOH (1％ HCl), derivatized with trifluoroacetic anhydride and assayed by GC/MS. Hair of 18 subjects for drug abuse was analyzed for MDMA and MDA. Calibration curves for the determination of MDMA and MDA in hair showed a good linearity at a concentration range from 0.5 ng to 250 ng ($r^2$=0.999) The extraction recovery was determined from hair blanks at 50, 100 ng. The percentage of recovery were found to be 96.08∼103.48 with CV value of 1.62∼3.89. The concentrations of MDMA and MDA ranged 1.14∼38.06 ng/mg and 0.07∼3.91 ng/mg, respectively in 18 hair samples from MDMA abusers. The ratio of MDMA to MDA ranged from 9.65∼28.46 in all specimen. Hair analysis for MDMA is a useful method for identification of long-term drug abuser.