• Title/Summary/Keyword: CFUBMS

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Structure and Mechanical Characteristics of ZrCrAIN Nanocomposite Thin Films by CFUBMS (CFUBMS을 이용한 ZrCrAIN 나노복합 박막의 구조와 기계적 특성)

  • Kim Youn J.;Lee Ho Y.;Shin Kyung S.;Jung Woo S.;Han Jeon G.
    • Journal of the Korean institute of surface engineering
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    • v.38 no.5
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    • pp.183-187
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    • 2005
  • The quaternary ZrCrAIN nanocomposite thin films are synthesized by Closed-Field Unbalanced Magnetron Sputtering (CFUBMS). Microstructure and mechanical properties of ZrCrAIN nanocomposite thin films are studied. Grain refinement of ZrCrAIN nanocomposite thin film is occurred by controlling $N_{2}$ partial pressure. Maximum hardness value according to the various $N_{2}$ partial pressures is obtained at 45 GPa. It is also conformed that critical value of the grain size (d) needs to achieve the maximum hardness.

Microstructural and Mechanical Characteristics of TiZrAlN Nanocomposite Thin Films by CFUBMS (CFUBMS을 이용한 TiZrAlN 나노복합 박막의 미세 구조와 기계적 특성)

  • Kim, Youn-J.;Lee, Ho-Y.;Kim, Yong-M.;Kim, Kab-S.;Han, Jeon-G.
    • Journal of the Korean institute of surface engineering
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    • v.40 no.1
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    • pp.1-5
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    • 2007
  • Quaternary TiZrAlN nanocomposite thin films were synthesized by Closed-Field Unbalanced Magnetron Sputtering (CFUBMS), and their microstructure and mechanical characteristics were examined. The grain refinement of the TiZrAlN nanocomposite thin films was controlled by adjusting the $N_2$ partial pressure. The hardness of the film varied with the $N_2$ partial pressure and the maximum value was obtained approximately 47 GPa. It was also confirmed that there is a critical value of the grain size($d_c$) to need maximum hardness.

Oxidation of TiZrAlN nanocomposite thin films in air at temperatures between 500 and $700^{\circ}C$ (TiZrAlN의 500-$700^{\circ}C$ 사이에서 공기 중 산화)

  • Kim, Min-Jeong;Bong, Seong-Jun;Lee, Dong-Bok
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2011.05a
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    • pp.167-170
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    • 2011
  • Quaternary TiZrAlN nanocomposite thin films with a composition of 20.7Ti-22.2Zr-2.7Al-54.4N (at.%) were deposited by the closed-field unbalanced magnetron sputtering (CFUBMS) method and oxidized in air at temperatures between 500 and $700^{\circ}C$. The oxides formed were $TiO_2$, $ZrO_2$, and $Al_2O_3$. The films had inferior oxidation resistance because the amounts of $ZrO_2$ and $TiO_2$ were large while the amount of $Al_2O_3$ was small. The oxidation progressed primarily by the inward diffusion of oxygen and the outward diffusion of nitrogen.

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