• 복합신소재구조학회 논문집
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• 제4권3호
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• pp.38-44
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• 2013

Glass fiber reinforced plastic (GRP) pipes buried underground are attractive for use in harsh environments, such as for the collection and transmission of liquids which are abrasive and/or corrosive. In this paper, we present the result of investigation pertaining to the structural behavior of GRP flexible pipes buried underground. In the investigation of structural behavior such as a ring deflection, experimental and analytical studies are conducted. In addition, vertical ring deflection is measured by the field test and finite element analysis (FEA) is also conducted to simulate behavior of GRP pipe buried underground. Based on the results from the finite element analyses considering soil-pipe interaction the vertical ring deflection behavior of buried GRP pipe is predicted. In addition, analytical and experimental results are compared and discussed.

• Elastomers and Composites
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• 제53권4호
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• pp.213-219
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• 2018

The degradation mechanism and physical properties of an FKM O-ring were observed with thermal aging in this experiment. From X-ray photoelectron spectroscopy (XPS) analysis, we could observe carbon (285 eV), fluoro (688 eV), and oxygen (531 eV) peaks. Before thermal aging, the concentration of fluoro atoms was 51.23%, which decreased to 8.29% after thermal aging. The concentration of oxygen atoms increased from 3.16% to 20.39%. Under thermal aging, the FKM O-ring exhibited debonding of the fluoro-bond by oxidation. Analysis of the C1s, O1s, and F1s peaks revealed that the degradation reaction usually occurred at the C-F, C-F2, and C-F3 bonds, and generated a carboxyl group (-COOH) by oxidation. Due to the debonding reaction and decreasing mobility, the glass transition temperature of the FKM O-ring increased from $-15.91^{\circ}C$ to $-13.79^{\circ}C$. From the intermittent CSR test, the initial sealing force was 2,149.6 N, which decreased to 1,156.2 N after thermal aging. Thus, under thermal aging, the sealing force decreased to 46.2%, compared with its initial state. This phenomenon was caused by the debonding reaction and decreasing mobility of the FKM O-ring. The S-S curve exhibited a 50% increase in modulus, with break at a low strain and stress state. This was also attributed to the decreasing mobility due to thermal aging degradation.

• 공업화학
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• 제19권4호
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• pp.382-387
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• 2008

착체중합법을 이용하여 $Ba_{0.5}Sr_{0.5}Co_{0.8}Fe_{0.2}O_{3-{\delta}}$ 조성의 산화물을 합성하였으며, 합성된 분말은 압축 성형 후 $1080^{\circ}C$에서 소결하여 치밀한 페롭스카이트 분리막을 제조하였다. 밀봉 재료로 gold ring, Pyrex ring 및 Pyrex 분말을 사용하여 가스누출 실험을 수행하였다. $Ba_{0.5}Sr_{0.5}Co_{0.8}Fe_{0.2}O_{3-{\delta}}$ 분리막의 산소투과량 분석결과 온도가 증가함에 따라 산소투과량은 증가하였고, $900^{\circ}C$에서 $0.74mL/min{\cdot}cm^2$의 값을 나타내었다. $950^{\circ}C$에서 밀봉 재료에 따른 투과 특성 분석 결과, gold ring을 이용할 경우 높은 산소투과량을 보인 반면, Pyrex를 밀봉재로 사용할 경우 낮은 투과량을 보였다. 이는 Pyrex를 밀봉재로 이용할 경우 분리막 표면으로 유리가 침투하여 유효 산소투과면적을 감소시켰기 때문이며, 광화학 현미경 분석으로 Pyrex 유리의 확산 침투를 확인하였다.

• 분석과학
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• 제24권3호
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• pp.173-182
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• 2011

약물(Prostanozol)을 복용한 여성을 대상으로 한 뇨시료 중에 함유된 Prostanozol 및 그 대사체들을 검출하기 위해 LC/ESI/MS와 GC/TOF-MS를 이용하여 효과적으로 분리 및 검출하였고, LC/ESI/MS의 질량스펙트럼으로부터는 각각의 분자량을 추정하였으며 GC/TOF-MS로는 이들을 확인하였다. M1은 Prostanozol의 17번 탄소가 케톤기로 치환된 17-keto-Prostanozol, M2는 M1에서 pyrazole nucleus 와 Aring에 한 개의 히드록시기가 치환된 hydroxy-17-keto-Prostanozol, M3는 B-ring 또는 C-ring에 한 개의 히드록시기가 치환된 hydroxy-17-keto-Prostanozol, M4는 한 개의 히드록시기가 D-ring에 치환된 hydroxy-17-keto-Prostsnozol로 확인되었으며 M5는 17번 탄소 위치에 히드록시기를 갖고 B-ring 또는 C-ring에서 하나의 히드록시기가 치환된 hydroxy-17-hydroxy-Prostanozol로 추정되며 M6은 17번 탄소 위치에 케톤기를 갖고 pyrazole nucleus 혹은 A-ring에 하나의 히드록시기를 또한 B-ring 또는 C-ring에 또 하나의 히드록시기가 치환된 dihydroxy-17-keto-Prostanozol, M7은 M6와 같이 17번 탄소에 케톤기를 갖으며 pyrazole nucleus 혹은 A-ring에 하나의 히드록시기를, 또한 D-ring에 또 하나의 히드록시기를 가진 dihydroxy-17-keto-Prostanozol로 확인되었다. 마지막으로 M8은 pyrazole nucleus 혹은 A-ring에 하나의 히드록시기를 갖고 그 외의 ring에 또 다른 히드록시기가 치환된 dihydroxy-17-hydroxy-Prostanozol임을 확인할 수 있었다. 이중 M5, M7, 그리고 M8은 지금까지 밝혀지지 않았던 새로운 대사체였다. 체내에서의 포합반응 여부를 확인한 결과 Prostanozol과 8종의 모든 대사체가 글루쿠론산 포합체를 형성하였고, 8종의 대사체 중 일부는 포합체를 형성하지 않고도 배출되며 특히 M6과 M7은 황산 포합체로도 배설되는 것을 확인할 수 있었다.

• 대한의용생체공학회:학술대회논문집
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• 대한의용생체공학회 1995년도 춘계학술대회
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• pp.173-178
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• 1995

This paper relates the occidental constitutional theory to the oriental one, concluding their origins to be similar, and demonstrates a new method of constitutional diagnosis by O-Ring Measurement System Of Muscular Meridians and Laser Constitutional Diagnosis. It establishes Laser Constitutional Diagnosis(L.C.D) using laser beams according to the principles of acupuncture and Sa-Sang constitutional physiology under the effect of spatial morphological energy of geometric isomers. Finally, hypothetical theory of L.C.D. was experimented by the O-Ring Measurement Systems of Muscular Meridians(O-R MSMM). O-R MSMM has been specially devised to improve the manual O-Ring Test prevailing to distinguish energetic response by muscle tonicity. Statistically, it has been proved that the constitutional diagnosis with O-R MSMM was highly effective and objective in the clinical experiences.

• 대한안전경영과학회지
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• 제2권4호
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• pp.197-208
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• 2000

ABS sensor ring has been manufactured by powder metallurgy (P/M) method using 400 series ferrite stainless steel. The results are following. It is supposedly sufficient to use for control computer due to good experimental results of magnetic characteristics. Compared with sensor ring made by iron, 400 series ferrite stainless steel has shown a good corrosion resistance without an addition surface treatment. Thus the decreasing production process has been obtained. As a result mechanical characteristics of hardness and tensile test, 400 series ferrite stainless steel shown a good endurance when it is combined to constant velocity joint(C/V), and has a good hardness properties endurable to sand and pebble impact. The products before sintering are much more corrodible in the condition of spray test of salt water and ammonia than humidity and nitrogen condition.

• Journal of Welding and Joining
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• 제32권5호
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• pp.1-6
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• 2014

This study aims at manufacturing SA welded API-X70 line-pipe with sour gas resistance. A pipe was manufactured by JCO bending process and SA welding using the API-X70 plate guaranteed HIC resistance. SA welded pipe was expanded in order to reduce the residual stress. The evaluation of a pipe for resistance to HIC and SSCC were performed by the RS D 0004 and RS D 0005 standards. For verification that a pipe has acceptable resistance to HIC, fullscale test was carried out. Results showed no cracking for the HIC and SSCC.

• 대한안전경영과학회지
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• 제5권1호
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• pp.129-141
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• 2003

In this thesis, using the 400 series ferrite stainless steel such as 434LD$_2$ which are furter excellent then the existing ferric products in mechanical characteristics, and experiment has been conducted on corrosion resistance of sensor ring. The results are following. 1. The products before sintering are much more corrodible in the condition of spray test of salt water and ammonia than humidity and nitrogen condition. 2. 434LD$_2$ ferrite stainless steel has shown a good corrosion resistance without an addition surface treatment. thus the decreasing production process has been obtained. 3. As hardness value of $H_{RB}$ 80 and tensile test, 434LD$_2$ ferrite stainless steel with show a good endurance when it is combined to constant velocity joint (c/v joint), and has a good hardness properties endurable to sand and pebble impact.

• 한국건설순환자원학회논문집
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• 제4권4호
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• pp.483-488
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• 2016

본 연구에서는 시멘트풀 및 모르타르의 초기재령 변형률 거동을 측정할 수 있는 경제적인 매입형 링센서를 고안하였고, 이를 활용하여 시멘트 풀 및 모르타르의 응결시간을 편리하게 측정할 수 있는 방법을 제안하고자 하였다. W/C가 0.30, 0.35, 0.40, 0.45인 배합들에 대하여 실험 연구를 수행하였다. 기존의 비카침과 관입저항침에 의해 측정된 응결시간과 제안된 방법에 의한 응결시간을 비교하였다. 실험결과에 따르면 개발된 링센서는 초기의 팽창거동이 수축거동으로 변화하는 수축의 시작시점을 정확하게 측정할 수 있었다. 또한, 수축 시작 시점을 응결에 대한 합리적인 기준으로 간주할 수 있었으며, 이는 기존 방법의 초결시간과 유사한 것으로 평가되었다.

• 소성∙가공
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• 제21권1호
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• pp.13-18
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• 2012

During warm forging, materials are formed in the temperature range of $300^{\circ}C\sim900^{\circ}C$. In this temperature range, the friction between the forging die and the material is very high and has a negative effect on the forming process causing severe die wear and possible defects in the component because of stick-slip. Thus, lubrication characteristics are a very important factor for productivity during warm forging. In this paper, ring compression experiments were conducted to estimate the friction factor between the die and the materials as the main factor in characterizing the lubricant. Also, ring tests using normal graphite power as a lubricant coating system were compared with tests using nano graphite powder. The results confirm that the nano graphite is superior to the normal graphite in view of its lubricating effect. In addition, the friction factor (m) was estimated with respect to the amount of the nano graphite content in the lubricant. With 10 % nano graphite the friction factor had the lowest value as compared to other amounts. It can be concluded that the amount of the nano graphite in the coating system can be optimized to obtain the best lubrication condition between the die and the material using ring test experiments.