• 제목/요약/키워드: C rate

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Ni, Cu 변화에 따른 Ni-Cu-Zn Ferrite의 자기적 특성 (Magnetic Properties of Ni-Cu-Zn Ferrite with varying Ni, Cu)

  • 백승철;정승우;김태원;김성수;최우성
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1999년도 춘계학술대회 논문집
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    • pp.259-262
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    • 1999
  • In this study, we investigated magnetic Properties of N $i_{0.2-x}$C $u_{x}$Z $n_{0.305}$F $e_{0.495}$ (x=0 ~0.2) ferrites. As the increased, the density and shrinkage increased until 5.3g/㎤, 20% respects, but the absorption decreased rate until 0.01%. As a results of the density, absorption rate, and shrinkage rate, the grain growth progressed rapidly in x=0.125 at 105$0^{\circ}C$, x=0.075 at 115$0^{\circ}C$, and x=0.025 at 115$0^{\circ}C$ for 3hours. As the CuO concentration increased, initial permeability increased at sintered 105$0^{\circ}C$ and 115$0^{\circ}C$ for 3 hours, but decreased at 125$0^{\circ}C$ for 3 hoers. The complex permeability as a function of frequency were high values at sintered 105$0^{\circ}C$ for 3 hours in x=0.005, 0.075.5.5.5.

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304 스테인리스강의 300℃에서 저주기 피로수명 증가 (Increase of Low Cycle Fatigue Life at 300℃ for Type 304 Stainless Steel)

  • 김대환;한창희;이봉상
    • 대한금속재료학회지
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    • 제47권7호
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    • pp.391-396
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    • 2009
  • Tensile, low cycle fatigue, and fatigue crack growth rate tests were conducted at RT and $300^{\circ}C$ for type 304 stainless steel. Tensile was tested under displacement control and low cycle fatigue was tested under strain control. Fatigue crack growth rate test was conducted under load control and crack was measured by DCPD method. Yield strength and elongation decreased at $300^{\circ}C$. Dynamic strain aging was not detected at $300^{\circ}C$. Low cycle fatigue life increased but fatigue strength decreased at $300^{\circ}C$. Fatigue crack growth rate increased at $300^{\circ}C$. Dislocation structures were mixed with cell and planar and did not change with temperature. Grain size did not change but plastic strain increased at $300^{\circ}C$. Strain induced martensite after low cycle fatigue test increased at RT but decreased at $300^{\circ}C$. It was concluded that the increase of low cycle fatigue life at $300^{\circ}C$ was due to the decrease of strain induced martensite at which crack was initiated.

새만금호의 수질예측과 그에 따른 대책 3. 환경오염이 담수산 미세조류, Cryptomonas ovata의 증식과 참재첩(Corbicula leana) 섭이율에 미치는 영향 (Prediction of Water Quality and Water Treatment in Saemankeum Lake 3. Effects of Environmental Pollutants on Propagation of Freshwater Microalgae, Cryptomonas ovata and Feeding Rate of Corbicula leana)

  • 최문술;정의영;신윤경
    • 한국패류학회지
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    • 제14권2호
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    • pp.167-172
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    • 1998
  • As a preliminary study, effects of environmetal pollutants on propagation of freshwater microalgae, Cryptomonas ovata and feeding rate of Corbicula leana were investigated at 20${\pm}$1$^{\circ}C$, over 20 days after treatment of pollutants, glucose, complex fertilizer and NH4Cl. Number of C. ovata in control group was increased from 38${\times}$104 cell/ml to 1.910${\times}$104 cell/ml after 20 days cultivation in Sorokin-Krauss medium. Increments of cell number in experimental groups treated with glucose, complex fertilizer and NH4Cl were higher than that of control group. The higher propagation rate of C.ovata was observed when 30 mg/l of glucose treated, 120 mg/l of complex fertilizer treated, and 4 mg/l of NH4Cl treated, compared with other concentrations in each pollutant treated group. The feeding rates of large size group of C. leana which fed with a living organism, C. ovata in each experimental group were higher than small size group, and slightly reduced with the increase of pollutant concentrations. The feeding rates were not significantly different between any concentrations of the pollutant, and among experimental groups treated with glucose, complex fertilizer and NH4Cl.

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보일러 배관용 P92 파이프강의 기계적 특성 및 미세조직에 관한 연구 (A Study on the Mechanical Property and Microstructure of SA213 P92 Boiler Pipe Steel)

  • 김범수;손태하;민택기
    • 설비공학논문집
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    • 제24권11호
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    • pp.777-783
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    • 2012
  • The hardness and strength test was performed to make the manufacturing process of SA213 P92 boiler pipe steel. And the microstructure change was studied to find out the cause of room temperature property of P92 steel, ie, low hardness and strength property. The room temperature property of P92 steel depends on the improper normalizing and cooling rate. Especially, Ferrite was formed and the steel had low hardness when the temperature was decreased slowly under the cooling rate $1^{\circ}C$/min after normalizing at the temperature around $A_{c1}$ to $A_{c3}$. The critical heat treatment temperature and cooling rate was over $900^{\circ}C$ and over $10^{\circ}C$/min to satisfy the minimum yield and tensile stress which was laid down by ASME Code.

철의 고온 황화부식에 미치는 탄소의 영향 (The Effect of Carbon on the Hot Corrosion of lron by Sulfur Containing Environment.)

  • 최성필;강성군;백영남
    • 한국표면공학회지
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    • 제21권2호
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    • pp.53-67
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    • 1988
  • The high temperature corrosion of Fe-C alloys were studied at I atm SO gas in the temperature range 500~80$0^{\circ}C$ by means of a thermogravimetric analysis. The Na2SO4 induced high tempwrature corrosion rate was also measured at atm O2 gas under above the temperature renge. The reaction products were identified with the aid of X-ray diffraction technique, and micostruction of the alloy/scale interface was observed with a optical microscope and SEM. The experimental results were disussed by the themodeynamic calcutions. Under above the experimental condition. the reaction rates decrbon with increasing carbon content. The transfer of Fe ion was limited by a residue of carbon precipitated at alloy scale interface due to the oxidation of Fe-C alloys at alloy surface. The effect of cold working on reaction rate was different between the Fe containing low carbon and Fe-C Alloy containing carbon above 0,73 wt%. In a cold worked iron containing low carbon content, the crystallization of metal surface leads to the poor adherence between the alloy and the cavity formed between the alloy and scale. The outward diffusion of ion through the scale is estimated to be hindered by the cavity formed between the scale, consequently decreasing reaction rate. In the case Fe-C containing carbon above 0.73 Wt% alloy, the reaction rate was little affected by cold working, because the effect of content on reaction rats is greater than the effect of cold working.

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등전환 분석(Isoconversional Analysis)를 이용한 자유라디칼 중합의 활성화 에너지 계산 (Estimation of Activation Energy for the Free Radical Polymerization by Using Isoconversional Analysis)

  • 정익수
    • Elastomers and Composites
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    • 제39권4호
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    • pp.281-285
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    • 2004
  • 이 연구는 열분석법을 이용하여 간단하게 자유 라디칼 중합의 활성화 에너지를 결정하는 방법을 부틸 아크릴레이트을 모델로 하여 구했다. 활성화 에너지는 Kissinger, Osawa 및 half-width법인 다수의 주사 속도법 (multiple scanning-rate method)을 이용하여 $1^{\circ}C/min,\;2^{\circ}C/min,\;5^{\circ}C/min$, 그리고 $10^{\circ}C/min$로 측정하였으며 단수 주사 속도법인 Barret 법을 이용하여 구하였다. 열분석법에 의해 구해진 중합반응의 활성화 에너지는 개시반응, 성장반응 및 종결반응의 각각의 활성화 에너지에서 계산된 전체 중합반응에서의 활성화 에너지와 가깝게 접근하였다.

The Equilibrium between Dilatant and Thixotropic Flow Units

  • 방정환;김남정;최상원;김응렬;한상준
    • Bulletin of the Korean Chemical Society
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    • 제17권3호
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    • pp.262-268
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    • 1996
  • Flow properties of all suspensions are controlled by their flow units. The factors effecting on the flow units are the characteristics of the particle itself (surface properties, particle sizes, particle shapes and etc.), the electrostatic interactions among the particles and the influences of the medium in the suspensions. Here, we studied the transition between the flow units with shear rate which can be added to the above factors. For the concentrated starch-water suspensions, by using the Couette type rotational viscometer, we confirmed that at low shear rate, dilatancy is appeared, but it is transformed to thixotropy with increasing shear rate. In order to explain this fact, we derived the following flow equation, representing the transition from dilatancy to thixotropy with shear rate, by assuming the equilibrium between the flow units. f = X1β1s./α1 + 1/(1+Kexp(c0s.2/RT))((1-X1)/α2)sinh-1{(β2)0 s. exp(c2s.2/RT)} + K exp(c0s.2/RT)/(1+K exp(c0s.2/RT))((1-X1)/α3)sinh-1{(β3)0 s. exp(-c3s.2/RT)} By applying this flow equation to the experimental flow curves for the concentrated starch-water suspensions, the flow parameters were obtained. And, by substituting the obtained flow parameters to the flow equation, the theoretical flow curves were reproduced. Also, Ostwald curve was represented by applying the flow equation, and the applicability for stress relaxation was discussed.

Carbide분말상의 무전해 도금 (Electroless Deposition on Carbide Powders)

  • 이창언;최순돈
    • 한국표면공학회지
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    • 제28권1호
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    • pp.3-13
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    • 1995
  • Electroless Ni and Cu platings were conducted on $B_4C$ and SiC. In the electroless Ni plating, the deposition rate on $B_4C$ was higher than on SiC. However, the electroless Cu deposition occured with high deposition rate regardless of the carbide substrates used in this study. Uniformity of the deposits was better in the electroless Cu deposition than in the electroless Ni deposition. In the topographies of the electroless depositions, Ni deposits have grown as colony, whereas Cu deposits have grown as fine individual grains.

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Acanthopanax koreanum Nakai의 약효성분에 관한 연구 (A Study on the Chemical Constituents of Acanthopanax koreanum Nakai and Its Pharmaco-biological Activities)

  • 한덕룡;김창종;김정희
    • 약학회지
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    • 제29권6호
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    • pp.357-361
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    • 1985
  • Two glycosides, assumed to be one of the potential active principles, is isolate from the root bark of Acanthopanax koreanu Nakai, identified to be acanthoside D, $C_{34}H_{46}O_{18}$, mp $242^{\circ}C$, and syringo side, $C_{17}H_{24}O_{9}$ mp $192^{\circ}C$. Acanthoside D has been found to have s-GPT, s-GOT lowering effect, BSP-retention rate and survival rate in the toxic state through the bio-pharmacological experiments.

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보관 방법에 따른 Rotifer Brachionus plicatilis 내구란의 부화 (The Hatching Rate of Resting Eggs of the Rotifer Brachionus plicatilis according to Preservation Method)

  • 윤주연;허성범
    • 한국수산과학회지
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    • 제44권6호
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    • pp.665-670
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    • 2011
  • The rotifer Brachionus plicatilis is one of the most important food organisms in aquaculture. The resting eggs produced by mictic female rotifers are easily stored and hatched, making them useful as the starter for the mass culture of rotifers in marine larval culture. This study examined the optimum preservation method for resting eggs to ensure a high hatching rate. To produce resting eggs, the marine rotifer B. plicatilis was cultured with Nannochloris oculata (KMMCC 16). The resting eggs were harvested and cryopreserved using 5% and 10% methanol (MeOH), dimethylsulfoxide (DMSO), and glycerol as cryoprotectant agents (CPAs). The cryopreservation comprised slow or rapid freezing and the resting eggs were stored for one month in liquid nitrogen ($-196^{\circ}C$). The resting eggs were also dried at different temperatures (30, 40, and $50^{\circ}C$) and for different times (1, 2, and 3 h). In general, the hatching rates of the resting eggs preserved with CPA were higher than those without CPA and the slow freezing method was better than the rapid freezing method. However, the optimum CPA concentration for the hatching rate of the resting eggs varied with the freezing method and kind of CPA, and the CPA also affected the viability of the resting eggs. Dried resting eggs had a high, rapid hatching rate over 80%. The moisture content of the resting eggs cryopreserved in liquid nitrogen affected the hatching rate. Drying at $30^{\circ}C$ for 1 hour resulted in a high hatching rate of the resting eggs. In conclusion, drying at $30^{\circ}C$ for 1 hour and preservation in liquid nitrogen with the slow freezing method, without CPA, is recommended for a high hatching rate (ca. 95%) of rotifer resting eggs.