• Title/Summary/Keyword: Bonded Materials

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스테인레스강 Overlay 용접부의 Disbonding에 관한 연구 1

  • 이영호;윤의박
    • Journal of Welding and Joining
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    • v.1 no.2
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    • pp.45-52
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    • 1983
  • Many pressure vessels for the hot H$\sub$2//H$\sub$2/S service are made of 2+1/4Cr-1Mo steel with austenitic stainless steel overlay to combat agressive corrosion due to hydrogen sulfide. Hydrogen dissolves in to materials during operation, and sometimes gives rise to unfore-seeable damages. Appropriate precautions must, therefore, be taken to avoid the hydrogen induced damages in the design, fabrication and operation stage of such reactor vessels. Recently, hydrogeninduced cracking (or Disbonding) was found at the interface between base metal and stainless weld overlay of a desulfurizing reactor. Since the stainless steel overlay weld metal is subjected to thermal and internal-pressure loads in reactor operation, it is desirable for the overlay weld metal to have high strength and ductility from the stand point of structural safety. In section III of ASME Boiler and Pressure Vessel Code, Post-Weld Heat Treatment(PWHT) of more than one hour per inch at over 1100.deg. F(593.deg. C) is required for the weld joints of low alloy pressure vessel steels. This heat treatment to relieve stresses in the welded joint during construction of the pressure vessel is considered to cause sensitization of the overlay weld metal. The present study was carried out to make clear the diffusion of carbon migration by PWHT in dissimilar metal welded joint. The main conclusion reached from this study are as follows: 1) The theoretical analysis for diffusion of carbon in stainless steel overlay weld metal does not agree with Fick's 2nd law but the general law of molecular diffusion phenomenon by thermodynamic chemical potential. 2) In the stainless steel overlay welded joint, the PWHT at 720.deg. C for 10 hours causes a diffusion of carbon atoms from ferritic steel into austenitic steel according to the theoretical analysis for carbon migration and its experiment. 3) In case of PWHT at 720.deg. C for 10 hours, the micro-hardness of stainless steel weld metal in bonded zone increase very highly in the carburized layer with remarkable hardening than that of weld metal.

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A STUDY ON THE SHEAR BOND STRENGTH OF COMPOMER ACCORDING TO SURFACE TREATMENT (Compomer의 치면처리방법에 따른 전단 결합 강도에 관한 연구)

  • Kim, Jin-Yong;Hong, Chan-Ui
    • Restorative Dentistry and Endodontics
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    • v.23 no.1
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    • pp.247-256
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    • 1998
  • To evalutate the change in shear bond strength according to dentin surface treatment, 4 materials were divided into control group(A) and experimental group(B). Group A was treated according to the instruction of manufacture. Group B was treated with 32% phosphoric acid. After dentin surface treatment, each material was bonded and stored in 100% humidity during 7 days, and then, the shear bond strength was evaluated. The results were as follows: 1. In the case of treatment according to the instruction of manufacture, the shear bond strength according to material showed Z-100 to be highest with 12.42 MPa, Compoglass had the lowest shear bond strength with 4.23 MPa and there was significant difference between Compoglass and Z-100, Dyract (p<0.01). 2. The group treated with 32% phosphoric acid showed lower shear bond strength than that of the group treated according to the instruction of manufacture but there was no statistical significance. 3. As a result of observation under SEM, the fracture pattern was a mixture of cohesive and adhesive failure in group 1, and there was more adhesive failure in group 2, and in group 3 and 4 there was cohesive failure of material or tooth structure. From the results above Dyract showed shear bond strength levels between resin and resin -modified glass ionomer but Compoglass showed much lower shear bond strength than that of resin-modified glass ionomer thus indicating that even though they are the same type of material they show evident differences in physical properties. And it is thought that the treatment of dentin surface with phosphoric acid did not increase the shear bond strength, unlike enamel.

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Freezing-Thawing Resistance of Fiber Reinforced Polymers in Strengthening RC Members (구조보강용 FRP 복합체의 동결용해 저항성 평가 연구)

  • You, Young-Chan;Choi, Ki-Sun;Kim, Keung-Hwan
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.14 no.1
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    • pp.182-189
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    • 2010
  • The strengthening performance of FRPs(Fiber Reinforced Polymers) is directly affected by the environmental conditions such as freezing-thawing and moisture because FRPs are usually bonded on the concrete surface. It is, therefore, strongly required to evaluate a durability of bond between FRPs and concrete as well as FRP materials itself. The freezing-thawing resistance of FRPs is evaluated in this study with the variables of freezing-thawing conditions, types of FRP and freezing-thawing cycles. From the test results, it is found that tensile strength and pull-off strength of CFRP are not affected by the freezing-thawing. On the other hands, those of GFRP show a little degradation because of continuous water immersion during thawing process. But, cautions are needed on the bond durability between FRPs and concrete in case of continuous water supplying from adjacent to the concrete.

Effect of non-thermal plasma on the shear bond strength of resin cements to Polyetherketoneketone (PEKK)

  • Labriaga, Wilmart;Song, So-Yeon;Park, Jin-Hong;Ryu, Jae-Jun;Lee, Jeong-Yol;Shin, Sang-Wan
    • The Journal of Advanced Prosthodontics
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    • v.10 no.6
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    • pp.408-414
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    • 2018
  • PURPOSE. This study aimed to assess the effect of non-thermal plasma on the shear bond strength of resin cements to polyetherketoneketone (PEKK) in comparison to other surface treatment methods. MATERIALS AND METHODS. Eighty PEKK discs were subjected to different surface treatments: (1) Untreated (UT); (2) Non-thermal plasma (NTP); (3) Sandblasting with $50{\mu}m$ $Al_2O_3$ particles (SB); and (4) Sandblasting + Non-thermal plasma (SB+NTP). After each surface treatment, the contact angle was measured. Surface conditioning with Visio.Link was applied in all groups after pre-treatment. RelyX Unicem resin cement was bonded onto the PEKK specimens. After fabrication of the specimens, half of each group (n=10) was initially tested, while the other half was subjected to thermocycling ($5^{\circ}C$ to $55^{\circ}C$ at 10,000 cycles). Shear bond strength (SBS) testing was performed using a universal testing machine, and failure modes were assessed using stereomicroscopy. The SBS results were analyzed statistically using one-way ANOVA followed by Tukey's post hoc test. Independent t-test was used to examine the effect of thermocycling (P<.05). RESULTS. The highest SBS values with or without thermocycling were observed with PEKK specimens that were treated with SB+NTP followed by the SB group. The lowest SBS results were observed in the UT groups. CONCLUSION. The shear bond strength between PEKK and resin cements was improved using non-thermal plasma treatment in combination with sandblasting.

Strain Transmission Ratio of a Distributed Optical Fiber Sensor with a Coating Layer (코팅된 분포형 광섬유 센서의 변형률 전달률)

  • Yoon, S.Y.;Kown, I.B.;Yu, H.S.;Kim, E.
    • Composites Research
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    • v.31 no.6
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    • pp.429-434
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    • 2018
  • We investigate strain transmissions of a surface bonded distributed optical fiber sensor considering strain variation according to positions. We first derive a strain transmission ratio depending on a wavelength of a strain distribution of the host structure from an analysis model. The strain transmission ratio is compared with numerical results obtained from the finite element method using ABAQUS. We find that the analytical results agree well with the numerical results. The strain transmission ratio is a function of a wavelength, i.e. the strain transmission ratio decreases (increases) as the wavelength of the host strain decreases (increases). Therefore, if an arbitrary strain distribution containing various wavelengths is given to a host structure, a distorted strain distribution will be observed in the distributed optical fiber sensor compare to that of the host structure, because each wavelength shows different strain transmission ratio. The strain transmission ratio derived in this study will be useful for accurately identifying the host strain distribution based on the signal of a distributed optical fiber sensor.

Comparison of Temperatures of the Resin Cement in Polycrystalline Ceramic Brackets Irradiated Using a Diode Laser

  • Son, Young-Tak;Son, KeunBaDa;Kim, Kyung-Min;Lee, Jae-Mok;Kim, Jin-Wook;Yu, Wonjae;Lee, Kyu-Bok
    • Journal of Korean Dental Science
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    • v.14 no.2
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    • pp.69-78
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    • 2021
  • Purpose: The primary objective of this study was to evaluate the change in the temperature of the adhesive resin in polycrystalline ceramic brackets irradiated using a diode laser at different irradiation energy levels and times. Materials and Methods: For the measurement of the temperature of the adhesive resin, it was applied at the base of the ceramic bracket, a thermocouple was placed at the center of the base surface, the bracket was placed on prepared resin specimens for light curing, and a laser was irradiated to the center of the bracket slot at 5, 7, and 10 W. For the measurement of the temperatures of the enamel under the bracket and pulp cavity, extracted premolar was fixed to a prepared mold and the ceramic bracket was bonded to the buccal surface of the premolar. The Kruskal-Wallis H test and Friedman test were used for statistical analysis. Result: At 5 W, the temperature of the adhesive resin did not reach the resin softening temperature of 200℃ within 30 seconds. At 7 W, it reached 200℃ when the ceramic bracket was irradiated continuously for 28 seconds. At 10 W, it reached 200℃ when the ceramic bracket was irradiated continuously for 15 seconds. During laser irradiation, the temperature of the enamel under the bracket increased by over 5℃ within 15 seconds. Conclusion: The use of diode laser irradiation for bracket debonding should be carefully considered because the pulp cavity temperature increases by over 5℃ within the irradiation time for resin thermal softening.

Growth and thermal annealing of polycrystalline Ga2O3/diamond thin films on Si substrates (다결정 산화갈륨/다이아몬드 이종 박막 성장 및 열처리 효과 연구)

  • Seo, Ji-Yeon;Kim, Tae-Gyu;Shin, Yun-Ji;Jeong, Seong-Min;Bae, Si-Young
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.31 no.6
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    • pp.233-239
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    • 2021
  • In this study, Ga2O3/diamond layers were grown on Si substrates to improve the thermal characteristics of Ga2O3 materials. Firstly, diamond thin film was grown on Si substrates by hot-filament chemical vapor deposition. Afterward, Ga2O3 layer was grown in the growth temperature range of from 450~600℃ by mist chemical vapor deposition. We found that layer separation happens at the Ga2O3/diamond interface at the growth temperature of 500℃. This is attributed to the different thermal expansion coefficient of the mixture of amorphous and crystalline structures during cooling process. Therefore, this study might contribute to the heat-sink-layer bonded power semiconductor applications by stabilizing the thermal properties at Ga2O3/diamond interface.

Manufacture of Wood Veneer-Bamboo Zephyr Composite Board - I. Properties of Bamboo Zephyr and Composite Board Made from Moso, Giant Timber and Hachiku Bamboo -

  • Roh, Jeang Kwan;Kim, Jae Kyung;Kim, Sa Ick;Ra, Jong Bum;Kim, Yu Jung;Park, Sang Jin
    • Journal of the Korean Wood Science and Technology
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    • v.32 no.3
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    • pp.42-51
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    • 2004
  • Wood veneer-bamboo zephyr composite board (WBCB) was manufactured to evaluate the properties of bamboo as alternative raw materials for the manufacture of composite panels. Bamboo zephyr was prepared using Moso bamboo (Phyllostachys pubesens Mazel. et Z), Giant timber bamboo (Phyllostachys bambusoides Sieb. et Zucc), and Hachiku bamboo (Phyllostachys nigra var. henosos Stapf). The effect of age and species of bamboo on zephyr production was investigated in terms of the pass number of bamboo split through the rollers, and the width increasing rate of bamboo split. Five-ply WBCBs were produced with Keruing veneers as face and back layers, leading to three layers of bamboo zephyr sheets as core layer. Each layer was placed so that its grain direction was at right angles to that of the adjacent layer and the layers were bonded together with phenol-formaldehyde (PF) resin.The pass number of bamboo split was increased with an increase of the thickness of culm wall. At the same thickness, Moso bamboo showed no effect of the age of bamboo on the pass number. The pass number of split of Giant timber bamboo was lower than that of Moso bamboo. No significant effect of bamboo species and age on the width of zephyr produced was observed. The width of zephyr obtained could be expressed as a function of diameter multiplied by thickness of culm wall. The physical and mechanical properties of WBCB manufactured in all given conditions did not show any significant differences, and they were above the requirement of Korean Standard (KS).

Prediction for Fatigue Life of Composite Ply-overlap Joint Structures (복합재 플라이 오버랩 조인트 구조의 피로 수명 예측)

  • Yeju Lee;Hiyeop Kim;Jungsun Park
    • Journal of Aerospace System Engineering
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    • v.17 no.2
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    • pp.62-70
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    • 2023
  • We proposed a technique for predicting Stress-Life (S-N) curve or fatigue life using geometric features of a ply-overlap joint structure in which plies of two composite materials are partially or wholly laminated and bonded. Geometric features that could affect fatigue properties of a structure were selected as variables. By analyzing relationships between geometric variables and material constants of the Epaarachchi-Clausen model, a fatigue model for composites, relational expressions of these two factors were proposed. To verify the prediction accuracy of the proposed method, fatigue life of a CFRP/GFRP ply-overlap joint was predicted. Predicted life and life obtained by test data-based model were compared to actual life. High prediction accuracy was confirmed by calculating the coefficient of determination of the predicted S-N curve.

Effect of different storage media on elemental analysis and microhardness of cervical cavity margins restored with a bioactive material

  • Hoda Saleh Ismail;Brian Ray Morrow;Ashraf Ibrahim Ali;Rabab Elsayed Elaraby Mehesen;Salah Hasab Mahmoud;Franklin Garcia-Godoy
    • Restorative Dentistry and Endodontics
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    • v.49 no.1
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    • pp.6.1-6.16
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    • 2024
  • Objectives: This study aimed to investigate the elemental analysis and microhardness of a bioactive material (Activa) and marginal tooth structure after storage in different media. Materials and Methods: Fifteen teeth received cervical restorations with occlusal enamel and gingival dentin margins using the tested material bonded with a universal adhesive, 5 of them on the 4 axial surfaces and the other 10 on only the 2 proximal surfaces. The first 5 teeth were sectioned into 4 restorations each, then stored in 4 different media; deionized water, Dulbecco's phosphate buffered saline (DPBS), Tris buffer, and saliva. The storage period for deionized water was 24 hours while it was 3 months for the other media. Each part was analyzed by scanning electron microscopy-energy dispersive spectroscopy (SEM-EDS) analysis for different substrates/distances and the wt% of calcium, phosphorus, silica, and fluoride were calculated. The other 10 teeth were sectioned across the restoration, stored in either Tris buffer or saliva for 24 hours or 3 months, and were evaluated for microhardness of different substrates/areas. Data were analyzed using analysis of variance and Tukey's post hoc test. Results: Enamel and dentin interfaces in the DPBS group exhibited a significant increase in calcium and phosphorus wt%. Both silica and fluoride significantly increased in tooth structure up to a distance of 75 ㎛ in the 3-month-media groups than the immediate group. Storage media did not affect the microhardness values. Conclusions: SEM-EDS analysis suggests an ion movement between Activa and tooth structure through a universal adhesive while stored in DPBS.