• Title/Summary/Keyword: Bond 식

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Change in shear bond strength of orthodontic brackets using self-etching primer according to adhesive types and saliva contamination (Self-etching primer를 사용하여 교정용 브라켓 접착 시 접착제와 타액오염에 따른 전단결합강도 변화)

  • Nam, Eun-Hye;Yoon, Young-Ah;Kim, Il-Kyu
    • The korean journal of orthodontics
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    • v.35 no.6 s.113
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    • pp.433-442
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    • 2005
  • The purpose of this study was to evaluate and compare the shear bond strength of orthodontic brackets depending on the variety of adhesives and whether saliva exists, by using self-etching primer (SEP). Groups were divided according to the type of adhesive into resin adhesive (Trans bond XT) and resin-modified glass ionomer cement (Fuji Ortho LC). One group of resin adhesive used XT primer after etching with 37% phosphoric acid, and the other group used self-etching primer. One group of resin-modified glass ionomer cement only used etching for bonding, and the other group used SEP. Each of the groups were also classified by whether saliva was contaminated or not. and then the shear bond strength was measured. The results showed that when using resin adhesive, the shear bond strength of SEP was lower than the XT primer. In the resin-modified glass ionomer cement groups, the shear bond strength which depends on the priming method, did not have a meaningful difference statistically When saliva was contaminated, the group which used SEP, regardless of the adhesive variety, had a greater shear bond strength than the normal priming group. From these results, SEP showed a shear bond strength that is possible to be used clinically, regardless of the adhesive variety. It can especially be clinically useful to use SEP to bond brackets even on tooth surfaces contaminated with saliva, because it offers the appropriate bonding strength as well as shorter treatment time and easy application.

Confining Effect of Mortar Grouted Splice Sleeve on Reinforcing Bar (모르타르 충전식 철근이음과 구속효과)

  • Ahn, Byung-Ik;Kim, Hyong-Kee;Park, Bok-Man
    • Journal of the Korea Concrete Institute
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    • v.15 no.1
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    • pp.102-109
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    • 2003
  • The grouted splice steeve has been applied widely due to its superior construction efficiency, such as the unnecessity of post concrete and the large allowable limit to the arrangement of reinforcing bars. However, studies on grout-filled splice steeve still have not been sufficiently peformed. The purpose of this study is to investigate the confining effect of mortar grouted splice sleeve on reinforcing bar, known to strengthen the bond capacity between grout mortar and reinforcing bar. To accomplish this objective, totally 6 full-sized specimens were made and tested under monotonic loading. Each specimens were equipped with strain gauges at the 12 location of sleeve and reinforcing bar. The experimental variables adopted in this study are embedment length and size of reinforcing bars. Following conclusions are obtained; 1) Under ultimate strength condition, the confining pressure of grouted splice sleeve calculated from measured tangential and axial strain of the sleeve is over $200{\sim}300kgf/{cm}^2$ at any location of sleeve and improved with reduction in embedment length of reinforcing bar. 2) Untrauer and Henry's equation which describe bond strength of mortar as a function of its compressive strength and confining pressure, predicted the measured bond capacity of this test within the 5% limits.

Splice Length of GFRP Rebars Based on Flexural Tests of Unconfined RC Members (RC 부재 휨 실험에 의한 GFRP 보강근의 이음길이 제안)

  • Choi, Dong-Uk;Chun, Sung-Chul;Ha, Sang-Su
    • Journal of the Korea Concrete Institute
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    • v.21 no.1
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    • pp.65-74
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    • 2009
  • Glass fiber reinforced polymer (GFRP) bars are sometimes used when corrosion of conventional reinforcing steel bar is of concern. In this study, a total of 36 beams and one-way slabs reinforced using GFRP bars were tested in flexure. Four different GFRP bars of 13 mm diameter were used in the test program. In most test specimens, the GFRP bars were lap spliced at center. All beams and slabs were tested under 4-point loads so that the spliced region be subject to constant moment. Test variables were splice lengths, cover thicknesses, and bar spacings. No stirrups were used in the spliced region so that the tests result in conservative bond strengths. Average bond stresses that develop between GFRP bars and concrete were determined through nonlinear analysis of the cross-sections. An average bond stress prediction equation was derived utilizing two-variable linear regression. A splice length equation based on 5% fractile concept was then developed. As a result of this study, a rational equation with which design splice lengths of the GFRP bars can be determined, was proposed.

Influence of application methods of one-step self-etching adhesives on microtensile bond strength (한 단계 자가 산부식 접착제의 적용 방식이 미세인장 결합강도에 미치는 효과)

  • Choi, Chul-Kyu;Son, Sung-Ae;Ha, Jin-Hee;Hur, Bock;Kim, Hyeon-Cheol;Kwon, Yong-Hun;Park, Jeong-Kil
    • Restorative Dentistry and Endodontics
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    • v.36 no.3
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    • pp.203-210
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    • 2011
  • Objectives: The purpose of this study was to evaluate the effect of various application methods of one-step self-etch adhesives to microtensile resin-dentin bond strength. Materials and Methods: Thirty-six extracted human molars were used. The teeth were assigned randomly to twelve groups (n = 15), according to the three different adhesive systems (Clearfil Tri-S Bond, Adper Prompt L-Pop, G-Bond) and application methods. The adhesive systems were applied on the dentin as follows: 1) The single coating, 2) The double coating, 3) Manual agitation, 4) Ultrasonic agitation. Following the adhesive application, light-cure composite resin was constructed. The restored teeth were stored in distilled water at room temperature for 24 hours, and prepared 15 specimens per groups. Then microtensile bond strength was measured and the failure mode was examined. Results: Manual agitation and ultrasonic agitation of adhesive significantly increased the microtensile bond strength than single coating and double coating did. Double coating of adhesive significantly increased the microtensile bond strength than single coating did and there was no significant difference between the manual agitation and ultrasonic agitation group. There was significant difference in microtensile bonding strength among all adhesives and Clearfil Tri-S Bond showed the highest bond strength. Conclusions: In one-step self-etching adhesives, there was significant difference according to application methods and type of adhesives. No matter of the material, the manual or ultrasonic agitation of the adhesive showed significantly higher microtensile bond strength.

The study of shear bond strength of a self-adhesive resin luting cement to dentin (상아질에 대한 자가 접착 레진 시멘트의 전단결합강도에 관한 연구)

  • In, Hee-Sun;Park, Jong-Il;Choi, Jong-In;Cho, Hye-Won;Dong, Jin-Keun
    • The Journal of Korean Academy of Prosthodontics
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    • v.46 no.5
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    • pp.535-543
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    • 2008
  • Purpose: The objective of this study was to compare the bonding characteristics of a new self-adhesive resin cement to dentin, which does not require bonding and conditioning procedure of the tooth surface, and conventional resin cement. The effect of phosphoric acid etching prior to application of self-adhesive resin cement on the shear bond strength was also evaluated. Material and methods: Fortyfive non-carious human adult molars extracted within 6 months were embedded in chemically cured acrylic resin. The teeth were ground with a series of SiC-papers ending with 800 grit until the flat dentin surfaces of the teeth were exposed. The teeth were randomly divided into 3 experimental groups. In group 1, self-adhesive resin cement, RelyX Unicem (3M ESPE, Seefeld, Germany) was bonded without any conditioning of teeth. In group 2, RelyX Unicem was bonded to teeth after phosphoric acid etching. For group 3, Syntac Primer (Ivoclar Vivadent AG, Schaan, Liechtenstein) was applied to the teeth before Syntac adhesive (Ivoclar Vivadent AG, Schaan, Liechtenstein) and Helibond (Ivoclar Vivadent AG, Schaan, Liechtenstein) followed by conventional resin cement, Variolink II (Ivoclar Vivadent AG, Schaan, Liechtenstein). To make a shear bond strength test model, a plastic tuble (3 mm diameter, 3 mm height) was applied to the dentin surfaces at a right angle and filled it with respective resin cement, and light-polymerized for 40 seconds. All the specimens were stored in distilled water at $37^{\circ}C$ for 24 hours before test. Universal Testing Machine (Z020, Zwick, Ulm, Germany) at a cross head speed of 1 mm/min was used to evaluate the shear bond strength. The failure sites were inspected under a magnifier and Scanning Electron Microscope. The data was analyzed with One way ANOVA and Scheffe test at ${\alpha}$= 0.05. Results: (1) The shear bond strengths to dentin of RelyX Unicem was not significantly different from those of Variolink II/Syntac. (2) Phosphoric acid etching lowered the shear bond strength of RelyX Unicem significantly. (3) Most of RelyX Unicem and Variolink II showed mixed fractures, while all the specimens of RelyX Unicem with phosphoric acid etching demonstrated adhesive failure between dentin and resin cement. Conclusion: Shear bond strength to dentin of self-adhesive resin cement is not significantly different from conventional resin cement, and phosphoric acid etching decrease the shear bond strength to dentin of self-adhesive resin cement.

THE EFFCT OF TIME DELAY AFTER SILICOATING ON THE BOND STRENGTH BETWEEN THE METAL AND RESIN CEMENT (Silicoating후 시간지연이 금속과 레진 시멘트 간의 접착강도에 미치는 영향)

  • Yang, Jin-Kyoung;Bae, Jeong-Sik
    • The Journal of Korean Academy of Prosthodontics
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    • v.33 no.1
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    • pp.1-12
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    • 1995
  • For the purpose of this study, the silicoating on Ni-Cr-Be alloy surface was carried out by using the Silicoater MD. The effect of time delay after silicoating on the bond strength between the metal and resin cement was examined. The groups were divided into 4 : group 1 : Sandblasted with $250{\mu}m$ aluminium oxide, immediatly cemented group 2 : Sandblasted with $250{\mu}m$ aluminium oxide, silicoated and immediatly cemented group 3 : Sandblasted with $250{\mu}m$ aluminium oxide, silicoated and cemented after 7 days group 4 : Sandblasted with $250{\mu}m$ aluminium oxide, silicoated and coated with unfilled resin and cemented after 7 days Specimens were luted with Comspan, Superbond C&B or Panavia EX. The tensile bond strength between the metal and resin cement was measured by using the universal testing machine. The results were as follows : 1. The bond strength in groups 2, 3 and 4 was higher than that of group 1 (p<0.05). There was no statistically significant difference among the bond strength in groups 2, 3 and 4 (p>0.05). 2. In Comspan-cemented groups, there was no significant difference among the bond strength in groups 2, 3 and 4 (p<0.05). 3. In Panavia EX-cemented groups, the bond strength of group 3 was higher than that of group 2 (p<0.05) and there was no significant difference between groups 3 and 4. 4. In Superbond C&B-cemented groups, there was significant difference between groups 2 and 3 (p<0.05) and the bond strength of group 4 was higher than that of group 3 (p<0.05). 5. The highest tensile bond strength was obtained by using the Superbond C&B and no difference in the Panavia EX and Comspan. 6. The modes of bond failure were mainly cohesive failure. The method of storage and transport indicated in this study seems recommendable for laboratory and clinical use at least up to 7 days.

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COMPARATIVE TENSILE BOND STRENGTH OF HEAT-CURED, COLD-CURED, AND LIGHT CURED DENTURE BASE RESINS BONDED TO CONTINUOUS-PRESSURE INJECTION TYPE DENTURE BASE RESIN (지속적 가압 주사식 열중합 의치상 레진에 대한 열중합, 자가중합 및 광중합 레진의 결합력에 관한 비교분석)

  • Whang Seung-Woo;Chung Moon-Kyu
    • The Journal of Korean Academy of Prosthodontics
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    • v.31 no.3
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    • pp.385-393
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    • 1993
  • Injection processing of denture base resin was introduced by Pryer in 1942, in an attempt to reduce processing shrinkage. More recently a continuous-pressure injection type technique has been developed (SR-Ivocap, Ivoclar AG, Schaan, Liechtenstein.), and it reduced processing error and increased resin density. The purpose of this study was to compare tensile bond strength of heat-cured, cold-cured, and light-cured denture base resin bonded to continuous-pressure injection type resin. To know it, 60 cylindrical resin specimens were fabricated, and tensile bond strength were measured. The results were as follows : 1. The mean tensile bond strength bonded to continuous-pressure injection type resin was lower than bonded to conventional heat cured resin. But tensile bond strength of conventional heat cured resin bonding with light cured resin was lower than continuous-pressure injection type resin. 2. Of the tensile bond strength bonded to continuous-pressure injection type resin, tensile bond strength bonding with continuous-pressure injection type resin was the greatest(but not significantly different from bonding with conventional heat cured resin), followed by cold-cured, light-cured resin. 3. Of the tensile bond strength bonded to conventional heat cured resin, tensile bond strength bonding with conventional heat cured resin was the greatest and followed by continuous-pressure injection type resin, cold-cured resin, light-cured resin. According to these results, bonding of continuous-pressure injection type resin with conventional heat cured resin or continuous-pressure injection type resin is acceptable, but bonding with light-cured resin is questionable.

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An Experimental Study on Flexural Tensile Strength and Bond Strength Between Concrete-to-Concrete (콘크리트의 휨인장강도 및 신·구콘크리트 사이의 부착강도에 관한 실험 연구)

  • Yang, In-Hwan;Yoo, Sung-Won;Seo, Jung-In
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.13 no.3 s.55
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    • pp.155-163
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    • 2009
  • The purpose of this paper is to investigate the bond strength between old and new concrete as well as flexural tensile strength of concrete. To achieve this purpose, a comprehensive experimental program has been set up and strength tests using a series of specimens have been carried out. The present study represents that the flexural bond strength between old and new concrete is much smaller than that of flexural tensile strength. The ratio of bond strength to flexural tensile strength ranged through 15~27%. It is seen that concrete-to-concrete bond strength has been affected by curing condition. Also, test results of tensile strength show that recommendation by ACI 363 committee is estimated to be more realistic than another recommendations for predicting tensile strength of concrete.

Bond Splitting Strength and Behavior of GFRP Reinforcement with Roughened Surface (거친표면 GFRP 보강근의 쪼갬부착파괴강도 및 거동 고찰)

  • Moon, Do-Young
    • Journal of the Korean Society of Hazard Mitigation
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    • v.11 no.2
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    • pp.23-29
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    • 2011
  • In this experimental study, bond splitting strength and behavior were evaluated through pull-out tests. The tests were conducted on a GFRP rebar with roughened surface which was produced by Canadian manufacturer. The used variables in this study were rebar diameter, cover depth and compressive strength of concrete. For each variable, five specimens were made and tested to obtain good results. The bond splitting behavior was investigated from the relationship of pull-out force and slip. The experimental bond splitting strength was compared with the predicted strength obtained from the equations presented by some researchers. The results of the comparison demonstrated that the strength could be predicted well by using the Harajli et al's equation.