• Title/Summary/Keyword: Boiling method

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Bending of Korea red pine (Pinus densiflora) by Microwave Irradiation (마이크로파 가열에 의한 소나무재의 곡가공)

  • Jung, Sung-Soo;Lee, Weon-Hee
    • Journal of the Korean Wood Science and Technology
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    • v.27 no.3
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    • pp.17-22
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    • 1999
  • The effect of microwave irradiation on wood bending was investigated in this study. The specimens irradiated with microwave were bent around a form by using pedestal-steel and clamps. The specimens, korea red pine (Pinus densiflora), for this test were water-soaked for 78 hours. Saturated specimens were boiled in water for an hour. The size of specimens was 350mm(L) by 20mm(R) by 10mm(T). These specimens were heated by microwave of 2,450MHz. The most suitable time for microwave irradiation seems to range from 60 to 90 seconds. Wood moisture content decreased remarkably with the increase of irradiation time. When a softened wood piece is bent, its convex side was stretched while the concave side was compressed. It can be compressed considerably, but stretched very little. Therefore the failure will be governed by the tensile breaking strain and occur mainly on the convex face. So we obtained results from three different bending process methods as follows : 1) When bending with a pedestal-steel, convex face had not tensile breakings, but concave face had compression fails. 2) When bending with a clamp, bending time increased more than pedestal-steel and occurred tensile breaking. 3) Bending with a pedestal-steel and a clamp was found to be the most excellent operation method in this study.

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Isolation of Alliin in Garlic and Its Quantitative Determination by High Performance Liquid Chromatography and Studies on the Antimicrobial Efforts of Alliin and Ethanol Extracts from Korean Garlic(Alliium sativum L.) (마늘 중 고속 액체 크로마토그래피에 의한 알린의 분리 및 정량과 Alliin과 에탄올 추출물의 항균효과에 관한 연구)

  • 위성언
    • The Korean Journal of Food And Nutrition
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    • v.16 no.4
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    • pp.296-302
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    • 2003
  • First. the purification and analysis of alliin in garlic from different origins by alliin-HPLC determination method were studied. Allinase in garlic was inactivated by heating in boiling water followed by extraction of alliin in garlic with 80% methanol. To remove free amino acids and alliin homologs in garlic, garlic extract was separated by cation exchange column which was packed with amberlite CG-120 resin using 40L d-water as eluent. Alliin in garlic extract was crystallized in a mixture of acetone (50$^{\circ}C$):H$_2$O:acetic acid=70:29:1 and then recrystallized in a mixture of acetone (50$^{\circ}C$):H$_2$O:acetic acid=75:24:1. Obtained alliin was identified by melting point. TLC, microscope observation and mass spectrometry. High performance liquid chromatography (HPLC) following pre-column derivatization of cystein derivatives with o-phthaldialdehyde/2-mercaptoethanol has succeessfully been applied to the analysis of various garlics. Each alliic of standard solution and garlic extract was derivatized to isoindole derivative by o-phthaldialdehyde /2-mercaptoethanol and then analyzed by HPLC. Six point calibration was done by using alliin peak area. Lineality was observed at 0 ∼ 1.0mg/ml of alliin concentration. Weighted regression line function was Y=6254X - 256077. By this function, alliin contents in various garlics were 0.34 ∼ 0.73% fresh weight. Second study was designed to evaluate the effects of garlic extracts of various concentrations on the growth of various pathogenes (Eubacterium limonsum, Bacteroides fragilis, Salmonella typhimurium, Salmonella typhi, Shigella sonnei, Kiebsiella pneumoniae, Enterobacter cloacae, Pserdomonas aeruginosa, Escherichia coli). For antimicrobial effects against microorganism, totally minimal inhibition concentrations (MIC) of alliin were from 5,000 to 20,000ppm. MIC of ethanol extract were 1,250 to 10,000ppm.

A Study on Fourth Group of Basic Food Groups(Source of Calcium) (기초식품군중(基礎食品群中).제사군(第四群)(칼슘급원(給源)) 연구(硏究))

  • Park, Kui-Sun
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.8 no.1
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    • pp.31-36
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    • 1979
  • As a preliminary study to estimate the amount of daily calcium intake of Korean people, the present study was conducted investigating the kinds and amount of food among ordinary Korean food considered to be sources of calcium. The author sampled arbitrarily a total of 165 apartment households in Pusan City which were distributed in seven administration sections. Duration of this study was eight months, from June, 1975 to February, 1976. During summer vacation in this period twenty trained students visited these households where they measured the calcium source food at dinner, and three times this amount was regarded as the total daily intake. Also questionairs itemizing the various kinds of food which were considered to be sources of calcium were given to housewives and collected about two months later. The results are summarized as follows: The major sources of calcium food were milk and anchovy, and the total calcium content taken daily was an average 195.06 mg which was far smaller than the recommended standard. Cooking methods varied according to the kinds of food; for anchovy, the boiled water extract or the part remaining after removing bone and head was used, and for chopped cattle bone, the broth from boiling foe 5 to 6 hours was used. For boiled water extract, during extraction the amount of calcium was increased in the water but smaller than foe fresh anchovy. It is, therefore, desirable to cook and eat edible fish bone instead of discarding it after extraction. The amount of calcium of shrimp and whitebait consumed was considerably less than that of milk or anchovy. Most housewives, about 71%, discarded fish bones which contained a lot of calium before or after cooking them. So, it was considered necessary to find a good method of preparing fish so that it can be eaten palatably together with the bones.

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A Study on the Probability of BLEVE of Above-ground LP Gas Storage Tanks Exposed to External Fire (지상식 LPG 저장탱크의 외부화재에 의한 BLEVE 가능성 해석)

  • Lee Seung-Lim;Lee Young-Soon
    • Journal of the Korean Institute of Gas
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    • v.7 no.1 s.18
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    • pp.19-23
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    • 2003
  • The purpose of this thesis is to investigate the BLEVE probability of LP gas storage tanks which are relatively more dangerous, by the deductive calculating method using the results of Birk's pilot tank test and the required heat capacity of BLEVE. The result that BLEVEs can occur in only above 43.68 percent of liquid filling level under $600^{\circ}C$ of tank pate temperature and $53^{\circ}C$ of inner liquid temperature, was obtained and will be useful for preventing the BLEVE of LP gas storage tanks in fire sites. In addition, this research showed conditions of external leak and fire causing BLEVE, based on 15ton capacity of LP gas tank which has the same specifications as those in Puchon LP gas filling station accident. The result of the calculation is that the minimum pool fire conditions of BLEVE are above 7.2mm equivalent diameter under a liquid release condition and above 17.6mm equivalent diameter under a two-phase release condition. In the end, the result of calculating the pool size corresponding the above conditions using EFFECTS version 2.1, concludes that a minimum of 3.3 meters of diameter and 10.4 meters of height should be needed for BLEVE outbreak.

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Study on the Risk of Flammability & Combustion of Liquid Mixtures such as Alcohols (알코올류 등의 액체 혼합물에 대한 인화 및 연소 위험성에 관한 연구)

  • Koh, Jae-Sun
    • Journal of the Society of Disaster Information
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    • v.15 no.4
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    • pp.634-647
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    • 2019
  • Purpose: Currently, many chemicals are used in industrial and real life, and many substances are used in the form of a single substance, but most of them are used in the form of a mixture, and there is a need for a criterion for judging the danger of these substances. Method: Therefore, this study aims to confirm the risk criteria of the mixture through experimental studies on flammable mixtures in order to secure the effectiveness of the details of the existing Dangerous Goods Safety Management Act angerous Goods Judgment Criteria and to ensure the reliability and reproducibility of the dangerous goods judgment. Result: Experimental results show that alcohol flash point is mixed with water, which is a non-flammable liquid. Similar flash point trends occurred around 60% on an alcohol basis. In addition, in the case of flammable-combustible mixtures, there was little change in flash point if the flash point difference of the two materials was not large, and if the flash point difference of the two materials was low, the flash point tended to increase with the increase of the high flash point material. Conclusion: In the future, the test results may provide reference data on the experimental criteria for the flammable liquids that are cracked at the fire site.

Decontamination Characteristics of 304 Stainless Steel Surfaces by a Q-switched Nd:YAG Laser at 532 nm (532 nm 파장의 큐스위치 Nd:YAG 레이저를 이용한 스테인리스 스틸 표면 제염특성)

  • Moon, Jei-Kwon;Baigalmaa, Byambatseren;Won, Hui-Jun;Lee, Kune-Woo
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.8 no.3
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    • pp.181-188
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    • 2010
  • Metal surface decontamination characteristics were investigated by using a laser ablation method. A second harmonic generation of a Q-switched Nd:YAG laser with a wave length of 532 nm, a pulse energy of 150 mJ and a pulse width of 5 ns was employed to assess the decontamination performance for metal surfaces contaminated with $CsNO_3$, $Co(NH_4)_2(SO_4)_2$, $Eu_2O_3$ and $CeO_2$. The ablation behavior was investigated for the decontamination variables such as a number of laser shots, laser fluence and an irradiation angle. Their optimum values were found to be 8, 13.3 J/$cm^2$ and $30^{\circ}$, respectively. The decontamination efficiency was different depending on the kinds of the contaminated ions, due to their different melting and boiling points and was in the order: $CsNO_3>Co(NH_4)_2(SO_4)_2>Eu_2O_3>CeO_2$. We also evaluated a correlation between the metal ablation thickness and the number of laser shots for the different laser fluences.

Design of Naphtha Cracker Gas Splitter Process in Petlyuk Column (납사열분해 가스분리공정에서의 Petlyuk Column 설계)

  • Lee, Ju Yeong
    • Journal of the Korean Institute of Gas
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    • v.24 no.1
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    • pp.17-22
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    • 2020
  • Light Naphtha is distillated from crude oil unit and separated into the methane, ethylene and propylene by boiling point difference in sequence. This separation is conducted using a series of binary-like columns. This separation method is known that the energy consumed in the reboiler is used to separate the heaviest components and most of this energy is discarded as vapor condensation in the overhead cooler. In this study, the first two columns of the separation process are replaced with the Petlyuk column. A structural design was exercised by the stage computation with ideal tray efficiency in equilibrium condition. Compared with the performance of a conventional system of 3-column model, The design outcome shows that the procedure is simple and efficient because the composition of the liquid component in the column tray was designed to be similar to the equilibrium distillation curve. The performance of the new process indicates that an energy saving of 12.1% is obtained and the cost savings of 44 million won per day based on gross domestic product is reduced under same total number of trays and the initial investment cost is saved.

Development of an Optimization Technique of CETOP-D Inlet Flow Factor for Reactor Core Thermal Margin Improvement (원자로심의 열적여유도 증대를 위한CETOP-D의 입구유량인자 최적화 기법 개발)

  • Hong, Sung-Deok;Lim, Jong-Seon;Yoo, Yeon-Jong;Kwon, Jung-Tack;Park, Jong-Ryul
    • Nuclear Engineering and Technology
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    • v.27 no.4
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    • pp.562-570
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    • 1995
  • The recent ABB/CE(Asea Brown Boveri Combustion Engineering) type pressurized oater reactor-s have the on-line monitoring system, i.e., the COLSS(core operating limit supervisory system), to prevent the specified acceptable fuel design limits from being violated during normal operation and anticipated operational occurrences. One of the main functions of COLSS is the on-line monitoring of the DNB(departure from nucleate boiling) overpower margin by calculating the MDNBR(mini-mum DNB ratio) for the measured operating condition at every second. The CETOP-D model, used in the MDNBR calculation of COLSS, is benchmarked conservatively against the TORC mod-el using an inlet flow factor of hot assembly in CETOP-D as an adjustment factor for TORC. In this study, a technique to optimize the CETOP-D inlet flow factor has been developed by elim-inating the excessive conservatism in the ABB/CE's. A correlation is introduced to account for the actual variation of the CETOP-D inlet flow factor within the core operating limits. This technique was applied to the core operating range of the YongGwang Units 3&4 Cycle 1, which results in the increase of 2% in the DNB overpower margin at the normal operating condition, compared with that from the ABB/CE method.

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Separation of $SF_6$ from $SF_6/N_2$ Mixtures Using Polymeric Membranes (고분자 분리막을 이용하여 $SF_6/N_2$ 혼합 기체에서 $SF_6$ 분리)

  • Ko, Young-deok;Lee, Hyung-Keun;Hong, Seong-Uk
    • Membrane Journal
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    • v.22 no.1
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    • pp.72-76
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    • 2012
  • $SF_6$ has an extremely high global worming potential (GWP). Therefore, there has been an effort to reduce the use of $SF_6$ and its emission into atmosphere. One possible solution for minimizing the use of $SF_6$ in electrical equipments is utilization of gas mixtures such as $SF_6/N_2$. The $SF_6$ concentration in the gas mixture varies from 10 to 60%. However, when the apparatus is repaired or dismantled, we have to recover $SF_6$ from the gas mixture. Since the boiling point of $SF_6$is low (${\sim}-60^{\circ}C$), the liquefaction method is difficult to apply. One possible alternative is the membrane separation technology. In this study, we investigated the $SF_6$ and $N_2$ permeation properties of 5 polymeric membranes. For example, permeability of $N_2$ in BOPP membrane at $25^{\circ}C$was 0.19 barrer, whereas that of $SF_6$ was only 0.0012 barrer, resulting in the selectivity of 158. An upper bound for $SF_6/N_2$ gas pair was suggested for the first time with n = -1.33 and k = 160 (barrer).

Changes of Antioxidative Activity and Related Compounds on the Chungkukjang Preparation by Adding Drained Boiling Water (콩 삶은 물을 첨가한 청국장 제조시 항산화활성 및 관련 성분들의 변화)

  • Lee Kyung-Hee;Ryu Seung-Hee;Lee Young-Soon;Kim Young-Man;Moon Gap-Soon
    • Korean journal of food and cookery science
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    • v.21 no.2 s.86
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    • pp.163-170
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    • 2005
  • Soybean is an important plant as the source of protein and oil, as well as phytochemicals such as genistien, daidzein, phenolic acids, phytic acid, tocopherol, and saponin. Chungkukjang, a fermented soybean paste, is common in Korean meals and bacillus is usually used in the fermentation of steamed soybean. For its processing, whole soybeans are boiled in water until the beans are soft, and then the drained beans are wrapped with rice straw or starter and set in a warm place at $65^{\circ}C\;for\;3\;\~\;4\;days$. Normally, the remaining cooked water which was drained from the steamed beans is discarded. We supposed that this water possesses hish amounts of useful components, and we therefore developed a modified method using the cooked water. After fermentation, we added the remaining cooked water which had been drained from the beans to the fermented soy beans and boiled them together. To investigate the bio-functionality of the modified Chungkukjang, the total antioxidative activity, isoflavones contents, phenolic acids, and 3-deoxyglucosone (3-DG) were measured at each stage of the preparation of chungkukjang. The original and modified chungkukjang possessed a high antioxidative activity compared with the other samples, as did the drained water after steaming of the soybean. The contents of genistein, daidzein, and phenolic acids, which contained antioxidative activity, were also increased in the original chungkukjang and their contents were similar in the modified chungkukjang. The content of 3-DG was increased in the modified chungkukjang compare with the original. It is suggested that the active soybean components delivered to the drained water during the steaming process were useful for increasing the bio-functionality of the modified chungkukjang.