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Characteristics of Bi-2212 Superconductor Tube Depending on Heat-treatment Conditions (열처리 조건에 따른 Bi-2212 초전도 튜브의 특성)

  • 박용민;장건익
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.14 no.7
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    • pp.606-610
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    • 2001
  • Bi-2212 HTS tube was fabricated by centrifugal forming and partial melting processes. Bi-2212 bulk tube has been optimized to achieve smooth surface and uniform thickness. The slurry was prepared in the mixing ratio of 10:1 between Bi-2212 powder and binder and initially charged into the rotating mold under the speed of 300~450 rpm. Heat-treatment was performed at the temperature ranges of 860~89$0^{\circ}C$ in air for partial melting. the HTS tube fabricated by centrifugal forming process at 89$0^{\circ}C$ under the rotating speed of 450 rpm was highly densified and the plate-like grains with more than 20${\mu}{\textrm}{m}$ were well oriented along the rotating axis. The measured Tc and J$_{c}$ at 10K on specimen heat treated at 89$0^{\circ}C$ was around 85 K and 1,200 A/$\textrm{cm}^2$ respectively.y.

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Microstructure and Phase Transition of ZnO Varistor Ceramics (ZnO 바리스터 세라믹스의 미세구조와 상전이)

  • 김경남;한상목
    • Journal of the Korean Ceramic Society
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    • v.28 no.2
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    • pp.160-166
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    • 1991
  • Microstructure and phase changes during the sintering of ZnO varistors were studied in ZnO-Bi2O3-CoO-Sb2O3 and ZnO-Bi2O3-CoO-Sb2O3-Cr2O3 systems using acanning electron microscopy (SEM) with an energy dispersive X-ray analysis (EDAX), X-ray diffraction (XRD) and differential thermal analysis (DTA). The spinel phase and the Bi2O3 phase were formed by the decomposition of the pyrochlore phase during heating. The spinel particles (2-4$\mu\textrm{m}$), which were formed both along ther grain boundaries and within the ZnO grain, were always found near the pyrochlore phase. Intergranular phases (Bi2O3 and pyrochlore) were precipitated from the liquid phase during cooling. The Bi2O3 phases were located at the triple (or multiple) point of the ZnO grains. Cr2O3 played a role in decreasing the formation temperature of the spinel phase and Bi2O3 phase during sintering, and inhibited the grain growth.

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INTUITIONISTIC FUZZY FILTERS OF ORDERED SEMIGROUPS

  • Shabir, M.;Khan, A.
    • Journal of applied mathematics & informatics
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    • v.26 no.5_6
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    • pp.1071-1084
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    • 2008
  • The notion of intuitionistic fuzzy filters in ordered semigroups is introduced and relation between intuitionistic fuzzy filters and intuitionistic fuzzy prime ideals is investegated. The notion of intuitionistic fuzzy bi-ideal subsets and intuitionistic fuzzy bi-filters are provided and relation between intuitionistic fuzzy bi-filters and intuitionistic fuzzy prime bi-ideal subsets is established. The concept of intuitionistic fuzzy right filters(1eft filters) is given and their relation with intuitionistic fuzzy prime right (left) ideals is discussed.

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Characterizations of fine Bi-2223 precursor powder by spray pyrolysis process (분무 열분해법으로 제조된 미세 Bi-2223 전구분말의 특성)

  • Kim S. H.;Yoo J. M.;Ko J. W.;Kim Y. K.
    • Progress in Superconductivity
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    • v.6 no.2
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    • pp.124-128
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    • 2005
  • Homogeneous and fine powders for Bi-2223 tape were prepared by ultrasonic spray pyrolysis (SP) method from an aqueous solution of metal nitrates. Bi-2223 precursor powders were synthesized with various solutes concentration and pyrolysis temperature. The synthesized precursor powders had a narrow particle size distribution and an average particle size was $\~{\cal}um$. The reactivity of precursor powder by SP method is very high, attributed to the fine and narrow particle size distribution. Bi-2223/Ag tape was prepared using PIT method and followed by various sintering conditions. The precursor powder by SP method promoted a very quick formation of the Bi-2223 phase for short sintering time while the secondary phase such as large AEC phase and $Ca_2PbO_4$ were minimized for SP tapes.

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A Study on Precision Machining Technology for Disk Cams using Bi-arc Method (Bi-arc법을 이용한 평면 캠의 정밀 가공 기술에 관한 연구)

  • Shin J.H.;Kwon S.M.;Cho I.Y.;Kim J.C.;Kang H.S.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.235-236
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    • 2006
  • The disk cam mechanism can produce a positive motion with relatively few components. This paper introduce a shape design of cam using the relative velocity method and a precision machining technology for using Bi-arc method. The paper gives a machining information at each point using the Bi-arc method and the analysis method of the cutting error due to the moving path of the cutter, so that we can lead to the optimum design in a disk cam mechanism.

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The characteristic research of a Bi-2223 wires by the Various Transport Current (수송전류에 따른 Bi-2223 선재의 특성연구)

  • 오정훈;배덕권;강형구;안민철;이상진;고태국
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2003.02a
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    • pp.220-223
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    • 2003
  • High-Tc superconducting(HT S) systems are commercialized by many study on high-Tc superconductor. For the successful commercialization of superconducting systems using Bi-2223 wires, the database on the degradation of critical current is essentially needed. In this paper, critical current variation of Bi-2223 wires according to the transport time was investigated. The degradation rate of critical current was also calculated. Solenoid type specimens have the length of 190cm Bi-2223 wire and double-pancake type specimens have the length of l0m wire were tested. Tested Bi-2223 wires are commercialized products of AMSC (American Superconductor) and Innost. When the transportation current was 95% of critical current, the degradation of critical current was appeared after 5 hours of transport time.

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Bi(Pb)SrCaCuO superconductor fabricated by interdiffusion of SrCaCuO and BiPbCuO double layers (SrCaCuO와 BiPbCuO 이중층의 상호확산에 의해 제조된 Bi(Pb)SrCaCuO 초전도체)

  • 최효상;이중근;정동철;한병성
    • Electrical & Electronic Materials
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    • v.9 no.7
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    • pp.680-689
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    • 1996
  • SrCaCuO와 BiPbCuO 화합물로 이루어진 이중층시료가 만들어 졌으며, 소결과정에서 나타나는 확산과 입자간의 상호작용으로 108K의 임계온도를 나타내었다. 이 시료는 820.deg. C에서 0-210 시간동안 소결되었다. 초전도체의 생성, 성장메카니즘과 임계온도의 관계가 연구되었으며, 최적조건은 820.deg. C에서 210시간 소결하고 SrCaCuO와 BiPbCuO의 도포비가 1:0.6인 시편에서 나타났다. 또한 이중층시료에서 가장 좋은 조성비는 S $r_{2}$C $a_{2}$C $u_{2}$ $O_{x}$와 B $i_{1.9}$P $b_{0.5}$C $u_{3}$ $O_{y}$ 이었다.다.

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Uniform deformation and Critical Current properties of 500 m class Bi-2223/Ag HTS tapes (500 m급 Bi-2223/Ag 고온초전도 선재의 균일 가공 및 임계전류 특성)

  • 이동훈;양주생;최정규;윤진국;황선역;김상철;하홍수;하동우;오상수
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2003.02a
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    • pp.85-87
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    • 2003
  • Intermediate annealing was carried out during wire drawing for uniform deformation of 500 m class Bi-2223/Ag HTS tapes. Wire drawing force was measured to evaluate the uniformity of wire deformation along the length. To prevent sausage and filament breakage of wire, drawing stress was controlled below 200 MPa by using intermediate annealing process. Thickness and width of the rolled tapes was measured 0.23 mm and 4.1 mm with low deviation $\pm$ 0.08 mm and $\pm$ 0.09 mm, respectively. The critical current of the 500 m tapes was measured 33.7 A $\pm$ 3.7 A by continuous critical current measurement system.

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Simulation of Magneto-optic characteristic of One Dimensional Magneto-Photonic Crystal with an Active Layer of a Highly Bi-Substituted Iron Garnet (Bi가 다량 치환된 가네트 박막을 이용한 1차원 자성 포토닉 결정의 자기광학 특성의 시뮬레이션)

  • 류선열;박재혁;이종백;조재경
    • Proceedings of the Optical Society of Korea Conference
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    • 2000.08a
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    • pp.184-185
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    • 2000
  • 1 차원 자성 포토닉 결정은 원하는 파장에서 큰 페러데이 회전각과 투과율을 얻을 수 있기에 아주 흥미롭다. 두 종류의 유전체 층(S: $SiO_2$, T:T $a_2$ $O_{5}$)을 주기적으로 적층한 구조에, Bi를 다량 치환한 가네트 박막(M:B $i_{1.07}$ $Y_{1.93}$F $e_{5}$ $O_{12}$)을 결함층으로 삽입한 (A/B)$_{k}$ M/(B/A)$_{k}$ 의 구조를 갖는 1차원 자성 포토닉 결정의 자기 광학 특성을 수치해석하였다. 가시광과 적외선 영역에서 1차원 자성 포토닉 결정의 자성체 층의 두께( $d_{M}$ )와 유전체 층의 적층수(k)를 변화시키며, 투과율(T)과 페러데이 회전각($ heta$$_{F}$ ) 및 성능지수(Q)를 조사하였다. (중략). (중략)(중략)

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Determination of Bi Impurity in Lead Stock Standard Solutions by Hydride-generation Inductively Coupled Plasma Mass Spectrometry

  • Park, Chang J.
    • Bulletin of the Korean Chemical Society
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    • v.25 no.2
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    • pp.233-236
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    • 2004
  • Total impurity analysis of a primary standard solution is one of the essential procedures to determine an accurate concentration of the standard solution by the gravimetry. Bi impurity is determined in Pb standard solutions by inductively coupled plasma mass spectrometry (ICP-MS). The direct nebulization of the Pb standard solution produces a significant amount of the Pb matrix-induced molecular ions which give rise to a serious spectral interference to the Bi determination. In order to avoid the spectral interference from the interferent $^{208}PbH^+$, the hydride generation method is employed for the matrix separation. The Bi hydride vapor is generated by reaction of the sample solution with 1% sodium borohydride solution. The vapor is then directed by argon carrier gas into the ICP after separation from the mixture solution in a liquid-gas separator made of a polytetrafluoroethylene membrane tube. The presence of 1000 ${\mu}$g/mL Pb matrix caused reduction of the bismuthine generation efficiency by about 40%. The standard addition method is used to overcome the chemical interference from the Pb matrix. Optimum conditions are investigated for the hydride-generation ICPMS. The detection limit of this method is 0.5 pg/mL for the sample solutions containing 1000 ${\mu}$g/mL Pb matrix.