• Journal of Magnetics
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• 제4권3호
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• pp.73-75
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• 1999

By appliying an slternate pulsed magnetic field -generated by using a sequential ignition circuit and a magnet exciting circuit- with peak value of about 10 T to the rod type Nd based magnet Nd2Fe12.7Cr1.3B with length of 5 mm and diameter of 3.6 mm, the basic magnetic properties such as saturation magnetization, residual magnetization, coercivity, maximum energy products, magnetic anisotropy and anisotropic field are investigated with obtaining the major and minor J-H loops of the magnet. The increase in coercivity due to eddy currents in ac measurement of coercivity is calculated considering eddy current loss by analyzing a wave of generating magnetic field. The average coercivity calculated for the magnet is about 12.2 kOe, anisotropy magnetic field and anisotropic constant are measured as 60 kOe 2.43 Mj/$m^3$, respectively.

• 한국진공학회지
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• 제4권S2호
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• pp.24-29
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• 1995

The magnetic amd magneto-optical(MO)properties of Co-based multilayered(ML)films are known to vary sensitively according to the manufacturing methods and the film microstructures. Co/Pd and Co/Pt ML films with ultrathin layers of Co were prepared by alternating deposition in an ultrahigh-vacuum physical-vapor-deposition system. The individual layer thicknesses of the samples were estimated making use of the angular positions of x-ray diffraction peaks. The magnetic and MO properties were investigated, and correlated systematically to the structural parameters of the films. A Kerr spectrometer was self-manufactured to measure the MO properties such as Kerr rotation angle, ellipticity and reflectivity. The rms surface roughness was also measured using atomic force microscopy. Some of the samples showed good properties for MO medium, such as large perpendicular magnetic anisotropy and Kerr rotation, and perfect squareness of the magnetic hysteresis loop.

• 한국자기학회:학술대회 개요집
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• 한국자기학회 2012년도 임시총회 및 하계학술연구발표회
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• pp.121-122
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• 2012

Iron-excess gallium ferrite, $Ga_{0.6}Fe_{1.4}O_3$ (GFO), is known to have room-temperature ferromagnetic phases and potentially exhibit ferroelectricity as well [1]. But, leaky polarization-electric field (PE) hysteresis curves of the GFO thin film are hurdle to prove its spontaneous polarization, in other words, ferroelecticity. One of the reasons that the GFO films have leaky PE hysteresis loop is carrier hopping between $Fe^{2+}$ and $Fe^{3+}$ sites due to oxygen deficiency. We focus on reducing conducting current by substituting divalent cations at $Fe^{2+}$ sites. GFO thin films were grown epitaxially along b-axis normal to $SrRuO_3/SrTiO_3$ (111) substrates by pulsed laser deposition. Current density of the ion-substituted GFO thin films was reduced by $10^3$ or more. Ferroelectric properties of the ion-substituted GFO thin films were measured using macroscopic and microscopic schemes. In particular, local ferroelectric properties of the GFO thin films were exhibited and their remnant polarization and piezoelectric d33 coefficient were obtained.

• 대한화학회지
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• 제61권1호
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• pp.29-33
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• 2017

Formation of Au particles in nonstoichiometric $Cu_{2-x}{^I}Cu{_2}^{II}O_{3-{\delta}}$ ($x{\approx}0.20$; ${\delta}{\approx}0.10$) oxide from aniline + hydrochloric acid mixtures and chloroauric acid in the ratios 30 : 1; 60 : 1; 90 : 1 (S1-S3) by volume and 0.01 mol of copper acetate, $Cu(OCOCH_3)_2.H_2O$, in each case is performed by sol-gel growth. Powder x-ray diffraction (XRD) results show Au particles are dispersed in tetragonal nonstoichiometric dicopper (I) dicopper (II) oxides, $Cu_{2-x}{^I}Cu{_2}^{II}O_{3-{\delta}}$ ($x{\approx}0.20$; ${\delta}{\approx}0.10$). Average crystallite sizes of Au particles determined using Scherrer equation are found to be in the approximate ranges ${\sim}85-140{\AA}$, ${\sim}85-150{\AA}$ and ${\sim}80-150{\AA}$ in S1-S3, respectively which indicate the formation of Au nano-micro size particles in $Cu_{2-x}{^I}Cu{_2}^{II}O_{3-{\delta}}$ ($x{\approx}0.20$; ${\delta}{\approx}0.10$) oxides. Hysteresis behaviour at 300 K having low loop areas and magnetic susceptibility values ${\sim}5.835{\times}10^{-6}-9.889{\times}10^{-6}emu/gG$ in S1-S3 show weakly ferromagnetic nature of the samples. Broad and isotropic electron paramagnetic resonance (EPR) lineshapes of S1-S4 at 300, 77 and 8 K having $g_{iso}$-values ${\sim}2.053{\pm}0.008-2.304{\pm}0.008$ show rapid spin-lattice relaxation process in magnetic $Cu^{2+}$ ($3d^9$) sites as well as delocalized electrons in Au ($6s^1$) nano-micro size particles in the $Cu_{2-x}{^I}Cu{_2}^{II}O_{3-{\delta}}$ ($x{\approx}0.20$; ${\delta}{\approx}0.10$) oxides. Broad and weak UV-Vis diffuse reflectance optical absorption band ~725 nm is assigned to $^2B_{1g}{\rightarrow}^2A_{1g}$ transitions, and the weak band ~470 nm is due to $^2B_{1g}{\rightarrow}^2E_g$ transitions from the ground state $^2B_{1g}$(${\mid}d_{x^2-y^2}$>) of $Cu^{2+}$ ($3d^9$) ions in octahedral coordination having tetragonal distortion.

• 한국자기학회지
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• 제15권2호
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• pp.72-75
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• 2005

변압기 철심으로 널리 사용되고 있는 $3.2{\%}$ Si-Fe 방향성전기강판에서 인장응력을 인가하면서 자기이력과정 동안 교류 섭동 자기장의 2차 고조파 파형을 관측하였다. 관측된 파형을 인가 자기장에 의한 자구 재배열과정에서 일어나는 비선형, 비대칭 자기유도에 의해 분석하였다. 인장응력 하에서 구한 2차 고조파 파형은 자구 생성 및 소멸 자기장에서 피크를 갖는데, 인장응력의 크기에 따라 피크간격은 선형적으로 감소하며, 그 기울기를 이용하여 포화자기변형을 측정할 수 있는 방법을 제시한다.

• Journal of Magnetics
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• 제16권4호
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• pp.435-439
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• 2011

In this work, we prepared Fe-Ni alloy nanopowders by wire electrical explosion in deionized water and ethanol. Particles size and morphology of the as-synthesized nanoparticles prepared in water and ethanol were observed by transmission electron microscopy. In both cases, the as-synthesized nanoparticles were in nearly spherical shape and their size distribution was broad. The particles prepared in the water were in core-shell structure due to the oxidation of Fe element. X-ray diffraction was used to analyze the phase of the nanopowders. It showed that the nanopowders prepared in water had ${\gamma}$-Fe-Ni solid solution and FeO phase. The samples obtained in ethanol were in two phases of Fe-Ni solid solution, ${\gamma}$-Fe-Ni and ${\alpha}$-Fe-Ni. Bulk samples were made from the as-synthesized nanopowders by spark plasma sintering at $1000^{\circ}C$ for 10 min. Structure of the bulk sample was observed by scanning electron microscope. Magnetic properties of the as-synthesized nanopowders and the bulk samples were investigated by vibrating sample magnetometer. The hysteresis loop of the assynthesized nanopowders and the sintered bulk samples revealed a ferromagnetic characteristic.

• Journal of Magnetics
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• 제21권2호
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• pp.209-214
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• 2016

This paper analyzes the magnetic property according to the machined shape of steel material with non-oriented silicon steel (50PN470/50A470), that is most commonly used in the design of electrical equipment. Toward this end, specimens were produced and divided into Bar-Specimen (Epstein Frame Tester) and Ring-Specimen (Toroidal Ring Tester). The characteristics of the electrical Silicon steel were measured using the instruments solely dedicated to measuring each specimen. The core loss of the Bar-Specimen, which is commonly used, was found to be less than that of the Ring-Specimen. This is a very important design factor in achieving the objectives of improving the product efficiency and predicting the performance of electrical equipment. It serves as a critical point of view in order to reduce the error between design value and product value. A comparative analysis was conducted regarding various characteristics (Hysteresis, B-H characteristic, Iron loss, Minor loop, Coercive force, Residual magnetic flux density, etc.) of the electrical silicon steel considered in the design of the electrical equipment according to the specimen.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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• pp.242-242
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• 2007

무방향성 규소강판을 lamination core 형태로 제작하여 자기적 특성을 조사 하였다. 그 결과 1차, 2차 권선수가 400turns 시료에서 보자력(Hc)과 포화자속밀도(Bs)는 최대값을 나타내었고, 보자력은 0.05Oe, 포화자속밀도는 1.8T 이었다. 현재 국내에서 생산되고 있는 무방향성 규소강판의 자속밀도값 보다 더 우수한 강을 나타내었으며, 열화특성이 자기적 특성에 미치는 영향을 통해 고효율 무방항성 규소강판 개발의 가능성을 확인하였다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
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• pp.245-246
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• 2006

방향성 규소강판을 tape-wound core 형태로 제작하여 $N_2$ gas 분위기에서 $760^{\circ}C$ 4 시간동안 열처리후 자기적 특성을 조사 하였다. 그 결과 1차, 2차 권선수가 85 turns 시료에서 보자력(Hc)과 포화자속밀도(Bs)는 최대값을 나타내었고, 보자력은 0.019Oe, 포화자속밀도는 1.92T 이었다. 현재 국내에서 생산되고 있는 방향성 규소강판의 자속밀도값 보다 더 우수한 값을 나타내었으며, 열화특성이 자기적 특성에 미치는 영향을 통해 고효율 방향성 규소강판 개발의 가능성을 확인하였다.

• 한국자기학회지
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• 제18권1호
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• pp.24-27
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• 2008

Polyol법을 이용하여 $MnFe_2O_4$ 나노입자를 제조하고, X-선 회절기(XRD)와 진동시료형 자화율 측정기(VSM)를 이용하여 결정학적 및 거시적인 자기적 특성을 분석하였고, 뫼스바우어($M\"{o}ssbauer$) 분광실험을 통하여 $MnFe_2O_4$ 물질의 초미세 상호작용에 대한 연구를 수행하였다. 고분해능 투과형 전자 현미경(High Resolution Transmission Electron Microscope; HRTEM)을 이용하여 입자의 크기를 분석한 결과, 대부분의 입자크기가 $6{\sim}8$ nm 정도의 분포를 가지는 매우 균일한 입자로 형성되었음을 확인할 수 있었다. X-선 회절실험의 분석 결과, $a_0=8.418{\pm}0.001{\AA}$의 격자상수를 가지는 입방정형의 스피넬 구조로써 그 공간군이 Fd3m 임을 확인하였다. 상온에서의 VSM 측정결과 강한 초상자성 거동을 보였고, 뫼스바우어 분석결과로 상온에서 초상자성 영향에 따른 요동현상이 나타남을 관측할 수 있었다. 4.2K에서는 6개의 공명흡수선이 2 set으로 존재하고 초미세 자기장 값($H_{hf}$)이 A-site의 경우 498 kOe, B-site의 경우 521 kOe 로 분석되었다.