• Title/Summary/Keyword: Average grain size

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Thermal Process Effects on Grain Size and Orientation in $(Bi,La)_4Ti_3O_{12}$ Thin Film Deposited by Spin-on Method (스핀 코팅법으로 증착한 $(Bi,La)_4Ti_3O_{12}$ 박막의 후속 열공정에 따른 입자 크기 및 결정 방향성 변화)

  • Kim, Young-Min;Kim, Nam-Kyeong;Yeom, Seung-Jin;Jang, Gun-Eik;Ryu, Sung-Lim;Kweon, Soon-Yong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.11a
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    • pp.192-193
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    • 2006
  • A 16Mb ITIC FeRAM device was fabricated with BLT capacitors. The average value of the switchable 2 polarization obtained m the 32k-array (unit capacitor size: 068 ${mu}m^2$) capacitors was about 16 ${\mu}C/cm^2$ at 3V and the uniformity within an 8-inch wafer was about 2.8%. But a lot of cells were failed randomly during the measuring the bit-line signal of each cell. It was revealed that the Grain size and orientation of the BLT thin film were severely non-uniform. Therefore, the uniformity of the grain size and orientation was improved by changing the process conditions of post heat treatment. The temperature of nucleation step was the very effective on varying the microstructure of the BLT thin film. The optimized temperature of the nucleation step was $560^{\circ}C$.

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Erosion Control Line (ECL) Establishment Using Coastal Erosion Width Prediction Model by High Wave Height (고파랑 해안 침식폭 예측모델을 이용한 침식한계선(ECL) 설정)

  • Park, Seung-Min;Park, Seol-Hwa;Lee, Jung-Lyul;Kim, Tae-Kon
    • Journal of Ocean Engineering and Technology
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    • v.33 no.6
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    • pp.526-534
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    • 2019
  • The average coastline and the erosion control line introduced as the management coastline, and the average shoreline (MSL) was established from the observed coastline. Also, the median grain size and the wave height of 30-years return period were applied. The erosion control line (ECL) was established through the model, HaeSaBeeN. These two lines set the coastline for evaluation. Based on the observed monitoring data along the coastline, the 1-day variation according to the normal distribution was used to estimate the regional variation, and the width of the erosion was calculated by applying the median grain size (D50) and the wave height of 30-years return period through the high-wave coastal erosion width model, i.e., HaeSaBeeN.

Modeling of Suspended Sediment Transport Using Deep Neural Networks (심층 신경망 기법을 통한 부유사 이동 모델링)

  • Bong, Tae-Ho;Son, Young-Hwan;Kim, Kyu-Sun;Kim, Dong-Geun
    • Journal of The Korean Society of Agricultural Engineers
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    • v.60 no.4
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    • pp.83-91
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    • 2018
  • Land reclamation, coastal construction, coastline extension and port construction, all of which involve dredging, are increasingly required to meet the growing economic and societal demands in the coastal zone. During the land reclamation, a portion of landfills are lost from the desired location due to a variety of causes, and therefore prediction of sediment transport is very important for economical and efficient land reclamation management. In this study, laboratory disposal tests were performed using an open channel, and suspended sediment transport was analyzed according to flow velocity and grain size. The relationships between the average and standard deviation of the deposition distance and the flow velocity were almost linear, and the relationships between the average and standard deviation of deposition distance and the grain size were found to have high non-linearity in the form of power law. The deposition distribution of sediments was demonstrated to have log-normal distributions regardless of the flow velocity. Based on the experimental results, modeling of suspended sediment transport was performed using deep neural network, one of deep learning techniques, and the deposition distribution was reproduced through log-normal distribution.

Smartphone Digital Image Processing Method for Sand Particle Size Analysis (모래 입도분석을 위한 스마트폰 디지털 이미지 처리 방법)

  • Ju-Yeong Hur;Se-Hyeon Cheon
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.35 no.6
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    • pp.164-172
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    • 2023
  • The grain size distribution of sand provides crucial information for understanding coastal erosion and sediment deposition. The commonly used sieve analysis for grain size distribution analysis has limitations such as time-consuming processes and the inability to obtain information about individual particle shapes and colors. In this study, we propose a grain size distribution analysis method using smartphone digital images, which is simpler and more efficient than the sieve analysis method. During the image analysis process, we effectively detect particles from relatively low-resolution smartphone digital images by extracting particle boundaries through image gradient calculation. Using samples collected from four beaches in Gyeongsangbuk-do, we compare and validate the proposed boundary extraction image analysis method with the analysis method that does not extract boundaries, against sieve analysis results. The proposed method shows an average error rate of 8.21% at D50, exhibiting a 65% lower error compared to the method without boundary extraction. Therefore, grain size distribution analysis using smartphone digital images is convenient, efficient, and demonstrated accuracy comparable to sieve analysis.

Microstructure and Dielectric Properties of (Sr·Ca)TiO3-based Ceramics Exhibiting Nonlinear Characteristics (비선형 특성을 갖는 (Sr·Ca)TiO3계 세라믹의 미세구조 및 유전 특성)

  • 최운식;강재훈;박철하;김진사;조춘남;송민종
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.1
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    • pp.24-29
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    • 2002
  • In this paper, the microstructure and the dielectric properties of Sr$\_$1-x/CaxTiO$_3$(0$\leq$x$\leq$0.2)-based grain boundary layer ceramics were investigated. The sintering temperature and time were 1420∼152 0$\^{C}$ and 4 hours in N$_2$ gas, respectively. The average grain size and the lattice constant were decreased with increasing content of Ca, but the average grain size was increased with increase of sintering temperature. The second phase foamed by the thermal diffusion of CuO from the surface leads to verb high apparent dielectric constant, $\xi$$\_$r/>50000 and low dielectric loss, tan$\delta$<0.05. X-ray diffraction patterns of Sr$\_$1-x/CaxTiO$_3$ exhibited cubic structure, and the peaks shifted upward and the peak intensity were decreased with x. This is due to the lattice contraction as Sr is replaced by Ca with a smaller ionic radius. The specimens treated thermal diffusion for 2hrs in 1150$\^{C}$ exhibited nonlinear current-voltage characteristic, and its nonlinear coefficient(a) was overt 7.

Microstructure and Electrical Properties of $SiO_2$-Doped Zinc Oxide Varistors ($SiO_2$가 첨가된 산화아연 바리스터의 미세구조 및 전기적 특성)

  • 남춘우;정순철
    • Electrical & Electronic Materials
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    • v.10 no.7
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    • pp.659-667
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    • 1997
  • The influence of SiO$_2$on the microstructure and electrical properties of zinc oxide varistor was investigated. Zn$_2$SiO$_4$third phase in the sintered body was found at grain boundaries, multiple grain junctions, and occasionally within ZnO grains. This phase acted as a grain growth inhibitor, which retard the grain growth of the ZnO matrix by impeding migration on the grain boundaries. As SiO$_2$ addition increases, average grain size decreased from 40.6${\mu}{\textrm}{m}$ to 26.9${\mu}{\textrm}{m}$ due to the pinning effect by Zn$_2$SiO$_4$ and drag effect by Si segregation at grain boundaries, the breakdown voltage consequently increased. When SiO$_2$ addition is increased, interface state density decreased, however, the barrier height increased by decrease of donor concentration, as a result, the nonlinear exponent increased and leakage current decreased. While, as SiO$_2$ addition increase, it was found that the apparent dielectric loss factor shows a tendency of decrease. Wholly, electrical properties of zinc oxide varistor can be said to be improved by SiO$_2$addition.

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Effect of the Ni Content and W Grain Size on the High Temperature Com-pressive Properties of W-Ni Activated Sintered Parts (Ni 함량과 W 결정립 크기에 따른 W-Ni 활성소결체의 고온압축 특성)

  • 박영삼;오승탁;양주환;김영도;문인형
    • Journal of Powder Materials
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    • v.11 no.2
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    • pp.149-157
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    • 2004
  • High temperature deformation behavior of activated sintered W powder compacts was investigated. The compression tests were carried out in the temperature range between 900 and 110$0^{\circ}C$ at the strain rate of $10^{-3}s^{-1}$. The sintered specimens of Ni-doped submicron W powder compacts showed decrease in W grain size with increasing the Ni content. As the result, the flow stress was significantly increased with increasing the Ni content. We obtained Ni-activated sintered W compacts with the relative density of 94 $\pm$ l%and the average grain size of less than 5${\mu}{\textrm}{m}$. A moderate true strain up to 0.60 was obtained without fracture even at 110$0^{\circ}C$ with the strain rate of $10^{-3}s^{-1}$ for the activated W compact despite adding the 1.0 wt%Ni to submicron W powder.

Grain size, crystalline phase and fracture toughness of the monolithic zirconia

  • Bocam, Kodchakorn;Anunmana, Chuchai;Eiampongpaiboon, Trinuch
    • The Journal of Advanced Prosthodontics
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    • v.14 no.5
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    • pp.285-293
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    • 2022
  • PURPOSE. This study evaluated the relationship among translucency, crystalline phase, grain size, and fracture toughness of zirconia. MATERIALS AND METHODS. Four commercial zirconia - Prettau®Anterior® (PA), Prettau® (P), InCorisZI (ZI), and InCorisTZI (TZI)- were selected for this study. The bar specimens were prepared to determine fracture toughness by using chevron notched beam method with four-point bending test. The grain size was evaluated by a mean linear intercept method using a scanning electron microscope. X-ray diffraction and Rietveld refinement were performed to evaluate the amount of tetragonal and cubic phases of zirconia. Contrast ratio (CR) was measured to investigate the level of translucency. RESULTS. PA had the lowest fracture toughness among other groups (P < .05). In addition, the mean fracture toughness of P was significantly less than that of ZI, but there was no difference compared with TZI. Regarding grain size measurement, PA had the largest average grain size among the groups. P obtained larger grain size than ZI and TZI (P < .05). However, there was no significant difference between ZI and TZI. Moreover, PA had the lowest CR value compared with the other groups (P < .05). This means PA was the most translucent material in this study. Rietveld refinement found that PA presented the greatest percentage of cubic phase, followed by TZI, ZI, and P, respectively. CONCLUSION. The different approaches are used by manufacturers to fabricate various types of translucent zirconia with different levels of translucency and mechanical properties, which should be concerned for material selection for successful clinical outcome.

Study for Prediction of Strain Distribution in Heavy Plate Rolling (후판압연에 있어서의 변형률 분포예측에 관한 연구)

  • Moon, C.H.;Lee, D.M.;Park, H.D.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.10a
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    • pp.96-99
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    • 2007
  • The microstructure with fine and uniform AGS(austenite grain size) along thickness direction over no recrystallization temperature is strongly required for production of the high strength steels. The previous AGS prediction only based on the average strain improves to find the rolling conditions for accomplishment of the fine grain, but cannot find those for uniform grain. In this paper, an integrated mathematical model for prediction of the strain distribution along thickness direction is developed by carrying out finite element simulation for a series of rolling conditions. Also, the AGS distribution after rough rolling is predicted by applying the proposed model with AGS prediction model.

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Effect of Hot Forging Ratio on the Mechanical Properties in Incoloy 825 Alloy (Incoloy 825 합금의 기계적 성질에 미치는 열간단조비의 영향)

  • Park, Y.T.;Jeong, Y.H.;Kang, C.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.29 no.6
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    • pp.259-263
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    • 2016
  • This study was carried out to investigate the effect of hot forging ratio on the microstructure and mechanical properties of incoloy 825 alloy. Hot forging was carried out at the forging ratio of 0%, 60% and 90% respectively in a range of $900^{\circ}C{\sim}1,140^{\circ}C$ and followed solution treatment was conducted at $1,000^{\circ}C$ for 1 hr. In all the specimens of hot forged of 0%, 60% and 90%, precipitates were not observed. The average grain size of 0% specimen is $82{\mu}m$ and that of 60% and 90% is $56{\mu}m$ and $31{\mu}m$, respectively. The range of grain size in the 0% specimen is uneven in $182{\mu}m$ to $31{\mu}m$, but the grain size of 90% specimen is uniform. With increasing hot forging ratio, the mechanical properties such as tensile strength, elongation, hardness increased and impact toughness increased by grain refinement.