• Title/Summary/Keyword: Average grain

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Growth Behavior of (Ti,W)(C,N) and WC grains in a Co Matrix (Co 액상 내에 공존하는 (Ti,W)(C,N)과 WC입자의 성장 거동)

  • 이보아;윤병권;강석중
    • Journal of Powder Materials
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    • v.11 no.2
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    • pp.165-170
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    • 2004
  • Growth behavior of two different types of grains, faceted and rounded, in a liquid matrix has been studied in the (75WC-25TiCN)-30Co system. Powder samples were sintered above the eutectic temperature for various times under a carbon saturated condition. (Ti,W)(C,N) grains with a rounded shape and WC grains with a faceted shape coexisted in the same Co based liquid. With increasing sintering time, the average size of (Ti.W)(C,N) grains increased continuously and very large WC grains appeared. The growth of rounded (Ti,W)(C,N) grains followed a cubic law, r^3-r^3_0$=kt, where r is the average size of the grains, $r_0$ the initial average size, k the proportionality constant and t the sintering time. indicating a diffusion-controlled growth. On the other hand, the growth of the faceted WC grains resulted in a bimodal grain size distribution, showing an abnormal grain growth. These observations show that the growth behavior of different types of grains is governed by their shape, faceted or rounded, even in the same liquid matrix.

Effect of Grain Size and Heat-treating Atmosphere on the Phase Stability of Y-TZP (입자크기와 열처리 분위기 변화에 따른 Y-TZP에서의 상안정성 변화)

  • Chung, Tai-Joo;Ahn, Seung-Su;Song, Eun-Wha;Oh, Kyung-Sik;Lee, Jong-Sook;Kim, Young-Sik
    • Journal of Powder Materials
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    • v.13 no.5 s.58
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    • pp.360-365
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    • 2006
  • The phase stability of tetragonal phase in Y-TZP was investigated in terms of the distribution of grain sizes and heat-treating atmosphere. Y-TZP with various grain sizes were prepared using duration time at $1600^{\circ}C$ as experimental parameter. Accumulated grain size distributions were built from the SEM micrographs and the amount of tetragonal phase were measured using XRD. Both results were compared to determine the critical grain size before and after heat-treatment in vacuum. The critical grain size drastically decreased compared with the small increase of average grain size due to the autocatalytic effect which critically affects the tetragonal to monoclinic phase transformation. After heat-treatment in reductive atmosphere critical grain size relatively increased due to the stabilization of tetragonal phase. The formation of oxygen vacancies during heat-treatment was ascribed to the increase of stability.

Inference Models for Tidal Flat Elevation and Sediment Grain Size: A Preliminary Approach on Tidal Flat Macrobenthic Community

  • Yoo, Jae-Won;Hwang, In-Seo;Hong, Jae-Sang
    • Ocean Science Journal
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    • v.42 no.2
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    • pp.69-79
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    • 2007
  • A vertical transect with 4 km length was established for the macrofaunal survey on the Chokchon macrotidal flat in Kyeonggi Bay, Incheon, Korea, 1994. Tidal elevation (m) and sediment mean grain size $(\phi)$ were inversely predicted by the transfer functions from the faunal assemblages. Three methods: weighted average using optimum value (WA), tolerance weighted version of the weighted average (WAT) and maximum likelihood calibration (MLC) were employed. Estimates of tidal elevation and mean grain size obtained by using the three different methods showed positively corresponding trends with the observations. The estimates of MLC were found to have the minimum value of sum of squares due to errors (SSE). When applied to the previous data $(1990\sim1992)$, each of three inference models exhibited high predictive power. This result implied there are visible relationships between species composition and faunas' critical environmental factors. Although a potential significance of the two major abiotic factors was re-affirmed, a weak tendency of biological interaction was detected from faunal distribution patterns across the flat. In comparison to the spatial and temporal patterns of the estimates, it was suggested that sediment characteristics were the primary factors regulating the distribution of macrofaunal assemblages, rather than tidal elevation, and the species composition may be sensitively determined by minute changes in substratum properties on a tidal flat.

Microstructure and Dielectric Properties of (Sr·Ca)TiO3-based Ceramics Exhibiting Nonlinear Characteristics (비선형 특성을 갖는 (Sr·Ca)TiO3계 세라믹의 미세구조 및 유전 특성)

  • 최운식;강재훈;박철하;김진사;조춘남;송민종
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.1
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    • pp.24-29
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    • 2002
  • In this paper, the microstructure and the dielectric properties of Sr$\_$1-x/CaxTiO$_3$(0$\leq$x$\leq$0.2)-based grain boundary layer ceramics were investigated. The sintering temperature and time were 1420∼152 0$\^{C}$ and 4 hours in N$_2$ gas, respectively. The average grain size and the lattice constant were decreased with increasing content of Ca, but the average grain size was increased with increase of sintering temperature. The second phase foamed by the thermal diffusion of CuO from the surface leads to verb high apparent dielectric constant, $\xi$$\_$r/>50000 and low dielectric loss, tan$\delta$<0.05. X-ray diffraction patterns of Sr$\_$1-x/CaxTiO$_3$ exhibited cubic structure, and the peaks shifted upward and the peak intensity were decreased with x. This is due to the lattice contraction as Sr is replaced by Ca with a smaller ionic radius. The specimens treated thermal diffusion for 2hrs in 1150$\^{C}$ exhibited nonlinear current-voltage characteristic, and its nonlinear coefficient(a) was overt 7.

Experimental Study of Bending and Bearing Strength of Parallel Strand Lumber (PSL) from Japanese Larch Veneer Strand

  • OH, Seichang
    • Journal of the Korean Wood Science and Technology
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    • v.50 no.4
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    • pp.237-245
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    • 2022
  • This study examined the structural performance of experimental parallel strand lumber (PSL) from a Larch veneer strand. The prototype of PSL from a Larch veneer strand was manufactured in the experimental laboratory and tested. The bending and dowel bearing strength were determined from the modulus of elasticity (MOE), modulus of rupture (MOR), and dowel bearing strength based on a 5% offset yield load. The test results indicated that the average MOR of PSL was higher than that of 2 × 4 dimension lumber, and the average MOE of PSL was lower than that of 2 × 4 dimension lumber. A linear relationship was observed between the MOR and MOE. The allowable bending stress of PSL was derived as specified in ASTM D2915 and compared with other research. The dowel bearing strength of PSL in parallel to the grain was approximately double that perpendicular to the grain of PSL. A comparison of several theoretical calculations based on each national code for the dowel bearing strength was conducted, and some theoretical equations produced results closer to the experimental results when it was parallel to the grain, but the difference was higher in the case perpendicular to the grain. The test results showed that PSL made with Japanese larch veneer strands appeared to be suitable for a raw material of structural composite lumber (SCL) appeared to be used as a raw material for SCL.

Improvement of System for Grain Drying, Storing , and Processing in Rural Area (농촌의 주곡 건조.저장.가공 작업체계 개선확립)

  • 서상용;이승규;김용환
    • Journal of Biosystems Engineering
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    • v.3 no.1
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    • pp.33-46
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    • 1978
  • To get the goal of self-supply of food grain, improvement of post-harvest grain operations in rural area is under consideration as an important task of agriculture in Korea. This is study is focused on elimination of losses and deteriorations of grain and reduction of labour requirements and funds for post-harvest grain operations. The purpose of this study are presentation of basic data referring to conventional post-harvest grain operations in rural area and suggestion of improving methods for the operations, and also finding out reasonable operating processes of the operations. The result of this study are follows; 1. Grain drying in-the-filed which is performed before threshing has major factors of grain loss during drying, and so should be restrained as possible. Combine harvesting system is recommended among other king of mechanized harvesting systems for restraining in-the-field drying and securing available labors for drying. 2. It is predicted that mechanical grain drying could be prevalent when combine harvesting is taken place. Recommended grain drier for pre-combine harvesting system and for combine harvesting system is batch-type drier and circulating -type drier, respectively. 3. As existing farm storages for grain have insufficient spaces and offer poor conditions for grain storing , it is greatly needed to build up new storage which store only grains. And it is concluded that storing grain in community common storages in desirable. 4. Power supplying system for milling machinery in local milling plants, that a large capacity prime mover supplies power to 4 to 6 kinds of milling machinery simultaeously, should be converted to a system of several small capacity prime movers supplying power to each machiner y for the purpose of reducing extra consumption of energy. 5. Governmental grain, of which Korean farms produced, should be milled and stored in the local milling plant successively for the purpose of reducing transportation fee and stroing facilities. 6. Furture post-havest grain operations-drying, storing and milling should be periormed successively in he community common plant. And average optimum processing capacity of the plant is estimated about 300 metric ton of grain every year.

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Varietal Variation of Grain-Filling Period under the Different Environmental Conditions in Barley (대맥의 재배환경에 따른 등숙일수의 품종간 변이)

  • Hong-Suk Lee
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.28 no.2
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    • pp.202-210
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    • 1983
  • These experiments were conducted to study the relationship among agronomic traits, varietal variation of grain-filling periods and the effect of environmental conditions on the grain-filling in the ten selected barley cultivars. The varietal variation of grain-filling periods was of significance: Tokak had the similar increment in both greenhouse and field plot, Suweon two row was believed to be an cultivar with short grainfilling period. Cultivars with higher grain-filling rates tended to. have significantly lower ash content. Ash content of a cultivar tended to be lower when grown under favorable condition. At maturity, the time of development of yellow or dark pigment at the crease base could be a possible criterion for physiological maturity determination. However, this requires further study. Average grain-filling period in the different conditions was constant, but varietal differences were 9 days in the greenhouse and 5 days in the field. The grain moisture content was not constant in accordance to both cultivars and growing conditions. Average accelerated days for heading and ripening periods were very constant in comparision with field and vinyl mulching suggests that the selected materials will be useful for genetic study on grain-filling periods. The cultivars and grown conditions with higher accumulated temperature per $100^{\circ}C$ from early grain-filling had larger grain-filling rates and heavier 1000 grain weight. This study showed that if the variation among and within cultivars is to be minimized, the greenhouse and vinyl mulching plots could be useful for genetic study on grain-filling periods in $BC_1$ and $F_2$ segregation.

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Effect of Nano Grain Growth on Coefficient of Thermal Expansion in Electroplated Fe-Ni Invar Alloy (Fe-Ni Invar 합금에서 나노 결정립 성장이 열팽창계수에 미치는 영향)

  • Yim, Tai Hong;Choe, Byung Hak;Jeong, Hyo Tae
    • Korean Journal of Materials Research
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    • v.24 no.10
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    • pp.515-519
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    • 2014
  • The aim of this paper is to consider the effect of annealing on the coefficient of thermal expansion (CTE) of electroplated Invar Fe-Ni alloy. The CTE of the as-electroplated alloy is lower than those of alloys annealed at $400^{\circ}C$ and $800^{\circ}C$. XRD peaks become sharper as the as-electroplated alloy is annealed, which means the grain growth. The average grain sizes of as-electroplated and as-annealed alloys at $400^{\circ}C$ and $800^{\circ}C$ are 10 nm, 70 nm, and $2{\mu}m$, respectively, as determined by TEM and EBSD analyses. The CTE variation for the various grain sizes after annealing may come from the magnetostriction effect, which generates strain due to changes in the magnetization state of the alloys. The thermal expansion coefficient is considered to be affected by nano grain size in electroplated Fe-Ni Invar alloys. As grain size decreases, ferromagnetic forces might change to paramagnetic forces. The effect of lattice vibration damping of nano grain boundaries could lead to the decrease of CTE.

Determination of Material Parameters for Microstructure Prediction Model of Alloy 718 Based on Recystallization and Grain Growth Theories (재결정 및 결정립 성장이론에 기초한 Alloy 718의 조직예측 모델에 대한 재료상수 결정방법)

  • Yeom, J.T.;Hong, J.K.;Kim, J.H.;Park, N.K.
    • Transactions of Materials Processing
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    • v.20 no.7
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    • pp.491-497
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    • 2011
  • This work describes a method for determining material parameters included in recrystallization and grain growth models of metallic materials. The focus is on the recrystallization and grain growth models of Ni-Fe based superalloy, Alloy 718. High temperature compression test data at different strain, strain rate and temperature conditions were chosen to determine the material parameters of the model. The critical strain and dynamically recrystallized grain size and fraction at various process conditions were generated from the microstructural analysis and strain-stress relationships of the compression tests. Also, isothermal heat treatments were utilized to fit the material constants included in the grain growth model. Verification of the determined material parameters is carried out by comparing the average grain size data obtained from other compression tests of the Alloy 718 specimens with the initial grain size of $59.5{\mu}m$.

Microstructure and Electrical Properties of $SiO_2$-Doped Zinc Oxide Varistors ($SiO_2$가 첨가된 산화아연 바리스터의 미세구조 및 전기적 특성)

  • 남춘우;정순철
    • Electrical & Electronic Materials
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    • v.10 no.7
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    • pp.659-667
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    • 1997
  • The influence of SiO$_2$on the microstructure and electrical properties of zinc oxide varistor was investigated. Zn$_2$SiO$_4$third phase in the sintered body was found at grain boundaries, multiple grain junctions, and occasionally within ZnO grains. This phase acted as a grain growth inhibitor, which retard the grain growth of the ZnO matrix by impeding migration on the grain boundaries. As SiO$_2$ addition increases, average grain size decreased from 40.6${\mu}{\textrm}{m}$ to 26.9${\mu}{\textrm}{m}$ due to the pinning effect by Zn$_2$SiO$_4$ and drag effect by Si segregation at grain boundaries, the breakdown voltage consequently increased. When SiO$_2$ addition is increased, interface state density decreased, however, the barrier height increased by decrease of donor concentration, as a result, the nonlinear exponent increased and leakage current decreased. While, as SiO$_2$ addition increase, it was found that the apparent dielectric loss factor shows a tendency of decrease. Wholly, electrical properties of zinc oxide varistor can be said to be improved by SiO$_2$addition.

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