• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 추계학술대회논문집A
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• pp.171-176
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• 2000

As huge energy transfer systems like a nuclear power plant, steam power plant and petrochemical plant are operated for a long time, mechanical properties are changed by degradation. The life time of the systems can be affected by the mechanical properties. BI(Ball Indentation) test has a potential to replace conventional fracture tests like a uniaxial tensile test, fracture toughness test, hardness test and so on. In this paper, we would like to present the aging evaluation technique by the BI method. The four classes of the thermally aged 1Cr-1Mo-0.25V specimens were prepared using an artificially accelerated aging method. Tensile tests, fracture toughness tests, hardness tests and BI tests were performed. The results of the BI tests were in good agreement with fracture characteristics by a standard fracture test method. The IDE(Indentation Deformation Energy) of a BI technique as a new parameter for evaluating a degradation was suggested and the new IDE parameter clearly depicts the degradation degree.

• 보존과학회지
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• 제28권3호
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• pp.247-256
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• 2012

호박은 삼국시대 이전부터 보석이나 공예품 등에 사용되어 왔으며, 매장문화재 형태로 발굴되고 있다. 하지만, 호박의 산지에 관한 정보가 없어 호박유물의 국내 유입 및 유통경로에 대한 논의가 어려운 실정이다. 본 연구에서는 호박유물의 산지 구분에 활용하기 위해 5개 산지 호박의 IR스펙트럼을 확보하였고, 산지별 특징적인 peak를 바탕으로 호박의 산지분류 스킴을 작성하였다. 또한, 열, 빛, 산소 조건에서 60일 동안 인공열화 실험을 실시하여 IR스펙트럼과 산지별 특징적인 peak들의 변화를 관찰하였다. 열화 후 대체적으로 C=O band와 O-H band가 증가하였고, C=C 결합과 관련된 band는 감소하였다. 열화와 함께 산지별 특성 peak이 일부 사라져 분류스킴의 수정이 필요하였으나, Baltic 호박, 중남미산 호박, 아시아산 호박 간의 구분은 열화 후에도 여전히 가능하였다. 따라서 이 결과를 토대로 풍화가 많이 진행된 실제 호박유물에 적용하여 신뢰성을 평가한다면, 향후 출토 호박유물의 산지 추정에 활용할 수 있을 것으로 기대된다.

• 대한기계학회논문집A
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• 제24권9호
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• pp.2183-2190
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• 2000

A thermal aging is observed in a primary reactor cooling system(RCS) made of a casting stainless steel when the RCS is exposed for long period at the reactor operating temperature, 290~3300C An investigation of effects of thermal aging on a low cycle fatigue characteristics included a stress variations caused by a reactor operation and trip, is required. The purpose of the present investigation is to find an effect of a thermal aging of the CF8M on a low cycle fatigue life. The specimen of CF8M are prepared by an artificially accelerated aging technique holding 300 and 1800hr at 4300C respectively. The low cycle fatigue tests for the virgin and two aged specimens are performed at the room temperature for various strain amplitudes($\varepsilon$ta), 0.3, 0.5, 0.8, 1.0, 1.2 and 1.5% strain. Through the experiment, it is found that the fatigue life is rapidly reduced with an creasing of the aging time. The experimental fatigue life estimation formulas between the virgin and two aged specimen are obtained and are proposed to a analysis purpose.

• Journal of Mechanical Science and Technology
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• 제16권7호
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• pp.902-910
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• 2002

Cast stainless steel may experience embrittlement when it is exposed approximately to 300$\^{C}$ for a long period. In the present investigation, the three classes of the thermally-aged CF8M specimen were prepared using an artificially-accelerated aging method. After the specimens were held for 300, 1800 and 3600hrs. at 430$\^{C}$, respectively, the specimens were quenched in water which is at room temperature. Load versus load line displacement curves and J-R curves were obtained using the unloading compliance method. talc values were obtained using the ASTM E813-87 and ASTM E 813-81 methods. In addition to these methods, talc values were obtained using the SZW (stretch zone width) method described in JSME S 001-1981. The results of the unloading compliance method are J$\_$Q/=543.9kJ/㎡ for virgin materials. The values of J$\_$IC/ for the degraded materials at 300, 1800 and 3600hrs. are obtained 369.25kJ/㎡, 311.02kJ/㎡, 276.7kJ/㎡, respectively. The results obtained by the SZW method are compared with those obtained by the unloading compliance method. Both results are quite similar. Through the elastic-plastic fracture toughness test, it is found that the value of loc is decreased with an increase of the aging time.

• 한국도로학회논문집
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• 제18권6호
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• pp.41-50
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• 2016

OBJECTIVES : In this study, microstructural components of crumb rubber modified asphalt (CRMA) binder were investigated using environmental scanning electron microscope (ESEM). To clearly understand the elemental composition of the CRMA binder, energy dispersive X-ray spectroscopy (EDX) was employed on the ESEM samples. METHODS : CRMA binders were produced using open blade mixers at $177^{\circ}C$ for 30 min. The binders were artificially aged through a series of accelerated aging processes. Sample preparation was done by making a mold shape on the glass slide. Thereafter, the morphology of the CRMA binder was observed using the ESEM coupled with the EDX. RESULTS : The images captured from the ESEM indicate that the unaged CRMA binder appears to have a single-phase continuous nonuniform structure after the addition of crumb rubber particles, whereas the artificially aged CRMA binder was observed to have two different phases. ESEM coupled with EDX shows detailed internal structure of the modified binders compared to other technologies (i.e., optical microscopy, atomic force microscopy, and conventional scanning electron microscope). CONCLUSIONS : The captured images resemble the internal structures such as the viscous properties of the unaged CRMA binder and the interaction between the rubber particles and the base binder at aged condition. ESEM is a powerful instrument and with the introduction of EDX, it provided more details of the network microstructure of the asphalt binder. ESEM coupled with EDX is recommended for use in future investigation of microstructure of asphalt binders.

• 대한기계학회논문집A
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• 제25권8호
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• pp.1287-1293
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• 2001

Fretting is a potential degradation mechanism of structural components and equipments exposed to various environments and loading conditions. The fretting degradation, for example, for example, can be observed in equipments of nuclear, fossil as well as petroleum chemical plants exposed to special environments and loading conditions. It is well known that a cast stainless steel(CF8M) used in a primary reactor coolant(RCS) degrades seriously when that material is exposed to temperature range from 290$\^{C}$∼390$\^{C}$ for long period. This degradation can be resulted into a catastrophical failure of components. In the present paper, the characteristics of the fretting fatigue are investigated using the artificially aged CF8M specimen. The specimen of CF8M are prepared by an artificially accelerated aging technique holding 180hr at 430$\^{C}$ respectively. Through the investigations, the simple fatigue endurance limit of the virgin specimen is not altered from that obtained from the fatigue tests imposed the fretting fatigue. The similar tests are performed using the degraded specimen. The results are not changed from those of the virgin specimen. The significant effects of fretting fatigue imposed on both virgin and degraded specimen on the fatigue strength are not found.

• 대한기계학회논문집A
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• 제25권12호
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• pp.2116-2124
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• 2001

It's required mechanical properties of in-service facilities to maintain safety operation in power plants as well as chemical plants. In this studdy the four classes of the thermally aged 1Cr-lMo-0.25V specimens were prepared using an artificially accelerated aging method at 630$\^{C}$. Ultrasonic tests, tensile tests, K$\_$IC/ tests and hardness tests were performed in order to evaluate the degree of degradation of the material. The mechanical properties were decreased as degraded, but the attenuation coefficient and the harmonic generation level of a ultrasonic signal were increased. Expecially the nonlinear parameter derived from the harmonic generation level is sensitive and will be a good parameter to evaluate the material degradation.

• 한국정밀공학회지
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• 제18권4호
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• pp.151-159
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• 2001

As huge energy transfer systems like a nuclear power plant, steam power plant and petrochemical plant are operated for a long time, mechanical properties are changed by degradation. The life time of the systems can be affected by the mechanical properties. BI(Ball Indentation) test has a potential to replace conventional fracture tests like a uniaxial tensile test, fracture toughness test, hardness test and so on. In this paper, we would like to present the ageing evaluation technique by the BI method. The four classes of the thermally aged 1Cr-!mo-0.25V specimens were prepared using an artificially accelerated aging method. Tensile tests, fracture toughness tests, hardness tests and BI tests were performed. The results of the BI tests were in good agreement with fracture characteristics by a standard fracture test method within 5%. The IDE(Indentation Deformation Energy) of a BI technique as a new parameter for evaluating a degradation was suggested and the new IDE parameter clearly depicts the degradation degree.

• 한국도로학회논문집
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• 제18권2호
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• pp.1-9
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• 2016

PURPOSES : The performance properties (indirect tensile strength, rutting resistance, and resilient modulus) of recycled aged CRM mixtures and their correlation with Superpave binder properties (viscosity, high failure temperature, $G^*sin{\delta}$, and stiffness) were investigated. METHODS: A series of Superpave binder tests was performed by using a rotational viscometer, DSR, and BBR to evaluate the performance properties. In addition, the CRM mixes were artificially aged through accelerated aging processes, and their properties were evaluated. The correlation between the properties of recycled aged CRM binders and the engineering properties of recycled aged CRM mixtures was experimentally determined. RESULTS : The rut depth values decreased and the ITS values increased with increasing high failure temperature. In general, the resilient modulus properties seemed to be poorly correlated with the high-temperature values, regardless of the aggregate source. CONCLUSIONS: The recycled aged CRM binders and mixtures can lead to satisfactory performance, and the properties of these binders are strongly correlated with the engineering properties of the mixtures.

• 대한기계학회논문집A
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• 제24권10호
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• pp.2405-2412
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• 2000

A cast stainless steel may experience an embrittlement when it is exposed to approximately 30$0^{\circ}C$ for long period. In the present investigation, The three classes of the thermally aged CF8M specimie n are prepared using an artificially accelerated aging method. Namely, after the specimen are held for 300, 1800 and 3600hrs. at 43$0^{\circ}C$ respectively, the specimens are quenched in water to room temperature. Load versus load line displacement curves and J-R curves are obtained using the unloading compliance method. $J_{IC}$ values are obtained following ASTM E 813-87 and ASTM E 813-81 methods. In addition to these methods, JIC values are obtained using SZW(stretch zone width) method described in JSME S 001-1981. The results of the unloading compliance method are $J_Q$=485.7 kJ/m$^2$ for virgin material, $J_{IC}$ of the degraded materials associated with 300, 1800 and 3600hrs are obtained 369.25 kJ/m$^2$, 311.02 kJ/m$^2$, 276.7 kJ/m$^2$, respectively. The results of SZW method are similar to those of the unloading compliance method. Through the elastic-plastic fracture toughness test, it is found that the value of $J_{IC}$ is decreased with increasing of the aging time. The results obtained through the investigation can provide reference data for a leak before break(LBB) of reactor coolant system of nuclear power plants.