• 제목/요약/키워드: Aqueous tape casting

검색결과 17건 처리시간 0.024초

PDP 투명 유전체용 Bi계 프릿트 필름의 제조 및 특성분석 (Fabrication and Characterization of Bi-Based Frit Film for PDP Transparent Dielectric Front Panel)

  • 이상진;김주원;황종희
    • 한국세라믹학회지
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    • 제44권10호
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    • pp.548-553
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    • 2007
  • Ceramic green sheets consisting Bi-based glass frit were fabricated for an application to PDP transparent dielectric front panel. The dispersion condition of the slurry for tape casting was pre-examined, and two kinds of hinder and plasticizer were used in the non-aqueous slurry system. In the fabrication process for the frit film, the properties such as dry and firing shrinkage, elongation, and transmittance were examined at the condition of various mixing ratio of plasticizers. In the mixing ratio of polyethylene glycol to dibutyl phthalate of 3:5wt%, a good adhesion, elongation and transmittance were observed at the firing temperature of $580^{\circ}C$. The photograph for the cross section of the interface was also showed a dense microstructure.

PDP 투명유전체 형성용 Green Sheet 제조 (Fabrication of Transparent Dielectric Green Sheet for Plasma Display Panel)

  • Heo, Sung-Cheol;Park, Duck-Kyun;Oh, Young-Jei
    • 한국세라믹학회지
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    • 제41권4호
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    • pp.277-283
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    • 2004
  • Plasma Display Panel(PDP) 상판용 투명유전체의 green sheet를 제조코자 투명유전체 슬러리의 분산특성 및 유기물의 함량과 조성비에 따른 밀도와 기계적 특성을 연구하였다. 비수계 시스템에서 슬러리의 완전분산을 위한 분산제의 종류와 분산제의 양을 결정하기 위해 침강실험, 점도측정을 행하여 최적의 분산조건을 구하였다. 조성물 변수로서 투명유전체조성 분말/(투명유전체조성 분말+유기물)의 비와 결합제/(결합제+가소제)의 비를 각각 변화시켜 green sheet를 제조하였다. 제조된 tape casting 슬러리의 대부분은 의가소성(pseudoplastic) 거동을 보이는데, 의가소성 거동은 shear thinning의 효과를 가지는 것으로 기술 할 수 있다. 각각의 조성을 가지는 슬러리는 모두 전단속도가 증가함에 겉보기 점도가 감소하는 shear thinning 효과를 보여 주었다. Green sheet의 특성을 조사한 결과 유기물의 함량 및 조성이 green sheet의 밀도와 기계적 특성을 결정하는 중요한 인자가 되었다.

비수계 테잎성형공정의 유기공정변수의 변화에 따른 티탄산바륨-붕규산염유리계 현탁액의 분산안정성 (Effect of Organic Processing Parameters in Non-aqueous Tape-casting on Dispersion Stability of Barium Titanate-Borosilicate Glass Based Suspensions)

  • 여정구;최성철
    • 한국재료학회지
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    • 제13권11호
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    • pp.725-731
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    • 2003
  • The effect of organic processing parameters on the dispersion stability of the BaTiO$_3$-based dielectric particles and borosilicate glass particulate suspensions was investigated in a system where organic solvents, dispersant, binder and modifier were used as processing additives in a low temperature cofired ceramic fabrication processes. Two- and three-component organic solvents were used to disperse ceramic particles and it was found the better stability in the particulate suspension prepared in a bi-solvent, which was consists of toluene and ethanol in a non-azeotropic composition. The addition amount of organic additives had a great impact on dispersion in the present investigation. The flow curves of the suspensions prepared with binder and modifier were fitted according to the power-law equation, which indicates that the internal structure of the suspension could be disturbed under the applied shear stress. Finally, the LTCC green tapes were successfully tape-cast based upon the optimum formulation of LTCC suspension and its microstructure was compared with that of the hard-agglomerates.

유기물 조성에 따른 LTCC 테입 특성 연구 (LTCC Tape Characterization as Organic formulation)

  • 임욱;강병환;유찬세;이영신;조현민;이우성;강남기
    • 한국마이크로전자및패키징학회:학술대회논문집
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    • 한국마이크로전자및패키징학회 2000년도 추계 기술심포지움 논문집
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    • pp.89-92
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    • 2000
  • 테입 캐스터를 이용하여 바인더/가소제, 글말함량 비율이 다른 LTCC 테입을 제작한 후 특성평가를 하고자 하였다. 슬러리 조성은 서로 다른 바인더/가소제 그리고 분말함량에 따라 각각 4개 조성으로 구성하였다. 모든 슬러리에서 발포나 핀홀이 없는 미려한 표면을 갖는 테입을 얻을 수 있었다. 가장 우수한 기계적 특성 특성은 B/P=3.0, 분말함량 70vo1%인 두께 52 $\mu\textrm{m}$인 테입에서 인장강도 4.6MPa, 신을 29.5%의 특성을 얻을 수 있었다.

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Bimodal 입도분포를 보이는 AlN 분말의 테이프캐스팅 성형을 위한 분산효과 (Effect of Dispersion on Tape Casted Green Sheet Prepared from Bimodal-Type AlN Powders)

  • 최홍수;이상진
    • 한국세라믹학회지
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    • 제47권6호
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    • pp.566-571
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    • 2010
  • Dispersion behavior of the slurries consisted of bimodal-type AlN powders was examined in non-aqueous solvent system. Azotropic solvent system and copolymer acidic dispersant were applied to the slurries. Measurements of the sedimentation height and the viscosity of the each slurry, and the test of particle size distribution of the each powder sample were conducted as examinations for the dispersion behavior at the various dispersant contents. The bimodal-type particle size distribution was continued after addition of the dispersant and small particle portions were increased as the dispersant content increases. The density of the green sheet was also increased as the dispersant content increases and a green density of $2.114\;g/cm^3$ was obtained at the sample prepared from 2.4 wt% dispersant content. The increase of large particle portions resulted in the surface defects of the green sheets.

다양한 분산제에 의한 AlN-Y2O3 혼합분말의 비수계 용매 중 분산특성 (Dispersion Characteristics of AlN-Y2O3 Powder Mixture by Various Dispersants in Non-aqueous Solvents)

  • 김신;방상우;황인준;윤상옥;신현호
    • 한국세라믹학회지
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    • 제51권4호
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    • pp.324-331
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    • 2014
  • The dispersion characteristics of AlN-4.5 wt% $Y_2O_3$ powder mixture by various dispersants were investigated in ethanol and methyethly-ketone (MEK) solvents. In general, the cationic polymer dispersants demonstrated superior dispersion of the powder as compared to the non-ionic ester-type dispersants or anionic phosphate-ester-based ones. The dispersion performance of the cationic polymer dispersants was sensitive to the type of solvent. An anhydric maleic-acid-based graft copolymer dispersant, AFB-1521, demonstrated a very good dispersion capability in ethanol but exhibited a much inferior dispersion in MEK. On the other hand, the dispersion of the powder mixture was very good with a phosphate-ester-based block polymer dispersant, BYK-111, in MEK solvent, while dispersionwas much degraded in ethanol.

The Protective Effects of Zanthoxylum bungeanum Maxim Pharmacopuncture on Disuse Muscle Atrophy in Rat Gastrocnemius Muscle

  • Chung, Yeon Joong;Lee, Yun Kyu;Lee, Bong Hyo;Kim, Jae Soo;Lee, Hyun-Jong
    • Journal of Acupuncture Research
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    • 제36권4호
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    • pp.238-244
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    • 2019
  • Background: This study aimed to investigate the protective effects of Zanthoxylum bungeanum Maxim pharmacopuncture on disuse muscle atrophy in the gastrocnemius muscle of rats. Methods: Thirty male 250 g Sprague-Dawley rats were distributed randomly into 3 groups. The left hindlimb immobilization was performed with casting tape for 2 weeks, and no treatment was given to the right hindlimb. Rats received pharmacopuncture and were injected daily on the BL57 with either 2 mL of Zanthoxylum bungeanum Maxim aqueous extract (ZM-W group), 1 mL pharmacopuncture of Zanthoxylum bungeanum Maxim ethanol extract (ZM-E group), or 2 mL normal saline (control group). After 2 weeks of immobilization, the weight of the whole gastrocnemius muscle was measured, and the morphology of both the left and the right gastrocnemius muscles were assessed by Hematoxylin and Eosin staining. To investigate the immobilization-induced muscular apoptosis, the immunohistochemical analysis of BAX and Bcl-2 was carried out. Results: ZM-W and ZM-E significantly inhibited the reduction in weight of the left gastrocnemius muscle, the reduction in the left myofibrils, and the cross-sectional area of gastrocnemius, as compared with the control. Moreover, the ZM-W and ZM-E groups showed significantly reduced immunoreactivity for BAX, and increased immunoreactivity of Bcl-2 in left gastrocnemius muscle compared with the control group. Conclusion: These results suggest that Zanthoxylum bungeanum Maxim pharmacopuncture has protective effects against immobilization-induced muscle atrophy by regulating the activity of apoptosis-associated BAX / Bcl-2 proteins in the gastrocnemius muscle.