• The Journal of Advanced Prosthodontics
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• 제2권4호
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• pp.142-147
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• 2010

PURPOSE. One of the major keys to achieve successful osseointegration of the implant is its surface properties. The aim of this study was to investigate the bone response to dental implants with different surface characteristics using the rabbit tibia model. Tricalcium phosphate (TCP) coated, anodic oxidized and turned (control) surfaces were compared. MATERIALS AND METHODS. Seventy two implants were placed in the tibia of eighteen rabbits. Nine rabbits were sacrificed at 3 weeks of healing and the remaining nine were sacrificed at 6 weeks of healing. The bone-to-implant contact (BIC) and the bone volume density (BVD) were assessed by light microscope after 3 and 6 weeks of healing. RESULTS. Statistical analysis showed that no significant differences in the BIC and BVD were observed between the different implant surfaces and the control group at 3 weeks and 6 weeks of healing. Data also suggested that the BVD of all the surfaces showed significant difference at 3 and 6 weeks. CONCLUSION. The present study has showed that osseointegration occurred in all investigated types of surface-treated implants. In the current study all of the threads of the implants were observed to calculate BIC and BVD values (instead of choosing some of the threads from the bone cortex for example), which didn't make BIC or BVD percentage values better than in the control group, therefore the clinical relevance of these results remains to be shown.

• 수산해양교육연구
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• 제15권2호
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• pp.176-183
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• 2003

Recently, with the tendency of lightening, high-strength and high-speed in the marine industries such as marine structures, ships and propellers, it is rapidly enlarged the use of the aluminium alloy. Therefore, there occurs much interest in the study on corrosion characteristics of aluminium alloy. This paper was studied on the corrosion characteristics of Al-Mg alloy propeller used for a coasting vessel. Under the various pH of marine environment, the corrosion test of Al-Mg alloy was carried out. And thus polarization resistance, corrosion potential, and current density behavior of Al-Mg alloy and galvanic corrosion behavior of Al-brass and Al-Mg alloy coupled Al 5086 and SS 400 for hull were investigated. The main results are as following: 1. The corrosion potential of Al-brass propeller is more nobel than materials for hull, but that of Al-Mg alloy propeller is low or similar to materials for hull. Therefore, the galvanic corrosion of hull due to Al-Mg propeller don't occur. 2. The polarization resistance of Al-Mg alloy in sea water of pH 4 is highest, and corrosion current density of Al-Mg propeller is the most controlled. 3. As pH value decreases, potential showed Evans polarization diagram approaches cathodic potential. The corrosion current density of Al-Mg alloy is controlled to anodic reaction rate, therefore, the corrosion reaction of Al-Mg alloy is anodic control.

• 공업화학
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• 제17권3호
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• pp.327-330
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• 2006

Si nanodot 배열을 형성하기 위하여 $NbO_{x}$ nanopillar를 건식식각 공정의 식각마스크로써 이용하기 위한 가능성이 조사되었다. $NbO_{x}$ nanopillar는 Al과 Nb의 양극산화 공정을 이용하여 준비되었다. $NbO_{x}$ nanopillar의 식각속도와 식각프로파일은 고밀도 플라즈마를 이용한 반응성 이온 식각법에 의해서 식각가스의 농도와 coil rf power, 그리고 dc bias voltage를 각각 변화시키면서 조사 되었다. $Cl_{2}$ 가스의 농도가 증가할수록 $NbO_{x}$ nanopillar의 식각속도는 감소하였고 coil rf power와 dc bias voltage의 증가는 식각속도의 상승을 초래했다. 선택된 식각조건에서 식각시간을 변화하여 $NbO_{x}$ nanopillar의 식각특성 및 식각메커니즘이 조사되었다.

• 한국가스학회지
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• 제11권2호통권35호
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• pp.31-36
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• 2007

가스 냉온수기용 STS 304 배관 용접부의 부식특성을 연구하기 위하여, 0.5M $H_2SO_4+0.01M$ KSCN 수용액 중에서 전기화학적 분극시험, 금속조직시험 과 경도시험을 실시하여 STS 304배관 용접부의 양극분극거동, 인가전위에 따른 부식거동, 용접부의 금속조직 및 경도거동를 고찰하였다. 다음과 같은 결론을 얻었다. 1) 임계양극전류밀도는 모재보다 용접열영향부에서 많이 배류되고, 기본부동태전위는 모재보다 용접열영향부에서 더 높게 된다. 2) 부동태전류밀도는 모재보다 용접열영향부에서 더 많이 배류되고, 부동태영역은 용접열영향부보다 모재가 더 크게 된다. 3)인가전압에 의한 용접열영향부의 전류밀도는 모재의 전류밀도보다 더 많이 배류된다.

• 한국분말재료학회지
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• 제13권5호
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• pp.327-335
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• 2006

In the development of new hydrogen absorbing materials for a next generation of metal hydride electrodes for rechargeable batteries, metastable Mg-Ni-based compounds find currently special attention. Amor phous-nanocrystalline $Mg_{63}Ni_{30}Y_7$ and $Mg_{50}Ni_{30}Y_{20}$ alloys were produced by mechanical alloying and melt-spinning and characterized by means of XRD, TEM and DSC. On basis of mechanically alloyed Mg-Ni-Y powders, complex hydride electrodes were fabricated and their electrochemical behaviour in 6M KOH (pH=14,8) was investigated. The electrodes made from $Mg_{63}Ni_{30}Y_7$ powders, which were prepared under use of a SPEX shaker mill, with a major fraction of nanocrystalline phase reveal a higher electrochemical activity far hydrogen reduction and a higher maximum discharge capacity (247 mAh/g) than the electrodes from alloy powder with predominantly amorphous microstructure (216 mAh/g) obtained when using a Retsch planetary ball mill at low temperatures. Those discharge capacities are higher that those fur nanocrystalline $Mg_2Ni$ electrodes. However, the cyclic stability of those alloy powder electrodes was low. Therefore, fundamental stability studies were performed on $Mg_{63}Ni_{30}Y_7$ and $Mg_{50}Ni_{30}Y_{20}$ ribbon samples in the as-quenched state and after cathodic hydrogen charging by means of anodic and cathodic polarisation measurements. Gradual oxidation and dissolution of nickel governs the anodic behaviour before a passive state is attained. A stabilizing effect of higher fractions of yttrium in the alloy on the passivation was detected. During the cathodic hydrogen charging process the alloys exhibit a change in the surface state chemistry, i.e. an enrichment of nickel-species, causing preferential oxidation and dissolution during subsequent anodization. The effect of chemical pre-treatments in 1% HF and in $10\;mg/l\;YCl_3/1%\;H_2O_2$ solution on the surface degradation processes was investigated. A HF treatment can improve their anodic passivation behavior by inhibiting a preferential nickel oxidation-dissolution at low polarisation, whereas a $YCl_3/H_2O_2$ treatment has the opposite effect. Both pre-treatment methods lead to an enhancement of cathodically induced surface degradation processes.

• Nuclear Engineering and Technology
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• 제6권1호
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• pp.14-22
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• 1974

아노다이징 전압이 탄탈양극산화피막의 주파수 특성에 미치는 영향을 다음 임피단스 식을 이용하여 분석하였다. (equation omitted) 여기서 $R_{f}$, $C_{f}$는 각각 양극산화피막의 등가직렬저항, 등가직련용량, 유전 손실이다. 파라데타 P, $\tau$$_{ο}$, $\tau$$_{\omega}$, Co는 다음과 같이 정의된다. P=(d-w)/w, $\tau$$_{ο}$=$textsc{k}$$\rho$$_{ο}$, $\tau$$_{\omega}$=$textsc{k}$$\rho$$_{\omega}$, $C_{ο}$=$textsc{k}$A/d 여기서 d는 양극산화피막의 두께, $\omega$는 화산층의 두께, $\rho$$_{ο}$는 금속과산화물의 계면에서의 산화물의 비저항, $\rho$$_{omega}$는 앙극산화피막의 진성영역에서의 비저항, A는 양극산화 피막의 면적이며, $textsc{k}$=0.0885$\times$$10^{-12}$ $\times$유전상수(in farad/cm). 등가직렬용량의 주파수에 따른 변화와 유전손실은 아노다이징전압이 증가함에 따라 감소하였다. 이 현상은 산화피막의 화산충의 두께가 아노다이징전압이 증가함에 따라 약간 증하는반면 선화피막 전체두께는 아노다이징전압에 비례하여 증가한다는 사실 때문이다. 실험측정치가 tan$\delta$$_{f}$=0.682$\Delta$ $C_{f}$ 관계식으로부터 부로 이탈하는것을 위의 임피단스식에 바탕을 두고 검토하였다. 여기서 $\Delta$ $C_{f}$는 0.1과 1KHZ 사이에서의 용량변화이다.이다.다.

• 한국지하수토양환경학회:학술대회논문집
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• 한국지하수토양환경학회 2001년도 추계학술발표회
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• pp.61-64
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• 2001

In the remediation of contaminated soil by electrokinetic process, transport characteristics of contaminants are major factors. Pb is highly fixed to entire soil and not moved readily. High concentration of Cd was analyzed in the cathodic section but anodic section's concentration was lower than initial concentration. Although the Cd had high treatment effect, 50% of total mass was concentrated in cathodic section and was not flowed out readily. Most of transported Cd may be adsorbed in the cathodic side soil due to increased pH at adjacent to catholyte.

• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2008년도 International Meeting on Information Display
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• pp.408-411
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• 2008

In an attempt to enhance luminance efficiency and to reduce discharge delays of test panels with aluminum fence-electrodes, various designs of the electrodes were prepared by chemically etching the aluminum foils bonded to soda-lime glass substrate via anodic bonding process. The effects of fence design on luminance and discharge characteristics were investigated and compared with conventional ac-PDPs. These results showed a possibility of using fence-type aluminum electrode at front plates of ac-PDDs without sacrificing its performance.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2014년도 추계학술대회 논문집
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• pp.185-185
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• 2014

In this study, we investigated surface characteristics of hydroxyapatite coated surface on nano/micro pore structured Ti-35Ta-xNb alloys. This paper was focus on morphology and corrosion resistance of Anodic oxidation. To prepare the samples, Ti-35Ta-xNb (x= 0, 10 wt. %) alloys were manufactured by arc melting and heat-treated for 12 h at $1050^{\circ}C$ in Ar atmosphere at $0^{\circ}C$ water quenching. Micro-pore structured surface was performed using anodization with a DC power supply at 280 V for 3 min, nanotube formed on Ti-35Ta-xNb alloys was performed using DC power supply at 30 V in 60 min at room temperature. Surface morphology and structure were examined by field-emission scanning electron microscopy, energy-dispersive X-ray spectroscopy and X-ray diffraction.

• Corrosion Science and Technology
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• 제19권5호
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• pp.259-264
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• 2020

Many studies have been conducted to improve the corrosion resistance and durability of various aluminum alloys through the anodizing technique. It is already used as a unique technique for enhancing the properties of aluminum alloys in various industries. This paper investigated the electrochemical corrosion and stress corrosion cracking characteristics of anodized aluminum 5083-H321 alloy in natural seawater. The corrosion characteristics were assessed by the electrochemical technique and potentiodynamic polarization test. The stress corrosion cracking characteristic was evaluated with a slow strain rate tensile test under 0.005 mm/min rate, which showed that the hard anodizing film had a thickness of about 16.8 ㎛. Although no significant characteristics of stress corrosion cracking were observed in the slow strain rate test, the anodized specimen presented excellent corrosion resistance. The corrosion current density was measured to be approximately 4.2 times lower than that of the base material, and no surface damage was observed in the anodic polarization test.