• Title/Summary/Keyword: Alumina mold

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Effect of Sintering condition on Mechanical Properties of Zircon Shell Molds (소결조건이 지르콘 쉘 몰드의 기계적 특성에 미치는 영향)

  • Kim, Jae-Won;Kim, Du-Hyeon;Seo, Seong-Mun;Jo, Chang-Yong;Choe, Seung-Ju
    • Korean Journal of Materials Research
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    • v.9 no.9
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    • pp.865-871
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    • 1999
  • Effect of sintering condition in mechanical properties of ZrSiO\ulcorner shell molds was investigated. Number of microcrack in primary layer of the mold was maximized after preheating at $1000^{\circ}C$ for 1.5 hours. Yield strength and specific surface area of the mold were inversely proportion to sintering temperature and time. After hot deformation test at $1500^{\circ}C$ for 4 hours, molds were deformed opposite to the loading direction and backup layers were cracked along the interface between stucco and zircon slurry. Reverse deformation of the molds during hot deformation test was considered to be resulted from the difference of thermal expansion coefficient between alumina stucco and zircon slurry in primary coat, and size difference between zircon stucco and zircon slurry in backup coat.

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Fabrication of a nanowire diluter using electrical fields (전기장을 이용한 나노와이어 희석기 제작)

  • Yang, Jin-Ho;Yoon, Hyeun-Joong;Yang, Eui-Hyeok;Yang, Sang-Sik
    • Proceedings of the KIEE Conference
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    • 2008.07a
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    • pp.1484-1485
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    • 2008
  • The control of the number and dimension of nanowires is essential for dielectrophoretic(DEP) nanoscale assembly process. However, it is difficult to control the number of nanowires assembled between the electrodes. We have developed a nanowire diluter device, which consists of a glass substrate with gold electrodes and a PDMS layer with microchannel. The diluter device is fabricated by the conventional and soft lithographies using a SU-8 mold. Nickel nanowires (30${\mu}m$-long) are fabricated by a template-directed electrodeposition process using nanoporous alumina templates. A solution containing nanowires is injected into an inlet whereby pulsed voltages are applied to 16 pairs of electrodes in this experiment. The nanowires are trapped or released depending on the pulsed electric field from inlet to outlet (the channel). Therefore, the number of nanowires can be decreased correspondingly if the fixed frequency at each electrode is decreased from electrode to electrode.

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Fabrication of High Strength Mg-Li-Al Alloys by Squeeze Casting Process (용탕단조법에 의한 고강도 Mg-Li-Al합금 제조)

  • Han, Chang-Hwa;Hwang, Yong-Ha;Kim, Yong-Woo;Kim, Do-Hyang;Hong, Chun-Pyo
    • Journal of Korea Foundry Society
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    • v.17 no.3
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    • pp.267-275
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    • 1997
  • Fabrication of high strength Mg-Li-Al alloys by squeeze casting was established by the stabilization of melt and mold temperatures, applied pressure and the refining method. The entrapment of inclusions during pouring was prevented using 30 ppi alumina foam filter. The as-cast microstructure consists of a mixture of ${\alpha}$ and ${\beta}$ phases including AILi and $MgLi_2$, Al particles, which are distributed in the ${\beta}$ matrix. The grain sizes of gravity and squeeze casting alloys were 288 ${\mu}m$ and 207 ${\mu}m$ respectively. The addition of Al in Mg-Li alloys promoted the formation of second phase particles, which were adjusted to optimize the properties of Mg-Li-Al alloys. The Mg-10wt%Li-5wt%Al alloy after heat treatment at $350^{\circ}C$ for 1 hour showed the maximum hardness value. This is due to the facts that the amounts of ${\alpha}$ and ${\beta}$ phases and their distributions are dependent upon the solution treatment temperature, and that the amounts of AILi and $MgLi_2Al$ particles are dependent upon the Al content.

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In-vivo Evaluation of Pneumatic Ventricular Assist Device and Durability Improvement (공압식 심실보조장치의 in-vivo 평가 및 내구성 개선)

  • 이상훈;이광호;박성식;서필원;김삼현;강봉진
    • Journal of Biomedical Engineering Research
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    • v.25 no.1
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    • pp.65-70
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    • 2004
  • In this paper, we described 23 cases of animal experiment with our pneumatic ventricular assist device and new durability-improvement method. The blood pump consists of blood housing, and back plate made by the injection molding of isoplast, and the diaphragm fabricated by dipping of polyurethane solution onto the aluminum mold. Its volume was 75 $m\ell$ and in-vitro test showed that maximum output was 4.5 $\ell$/min at the 100 mmHg. The adult female sheep with weight of 50 + 10 kg were employed for tile in-vivo experiments and the mean blood flow was sustained at 3.0 1/min. 4 animals survived more than 15 days and the longest survival time was 28 days. In the prior 10 cases, the major causes of death were the tearing of diaphragm at the diaphragm to blood housing junction. By the new mesh and alumina ball milling methods, the durability was enhanced, and its qualitative and quantitative improvement was proved via the in-vivo and in-vitro methods. Animal experiments demonstrated that all the physiologic parameters a ere maintained within the permissible ranges and no thrombus formation was observed through the visual and blood test. The in-vivo experiments demonstrated our pneumatic ventricular assist device to he one month's bridge to transplantation device.

The Development of an Automatic Molten Metal Supplier for an Aluminum Thermal Furnace (알루미늄 보온로 용탕 자동공급 시스템 개발)

  • Lee, Jun-Ho
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.18 no.5
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    • pp.483-490
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    • 2009
  • The objective of this development project is to localize an automatic molten metal supplier that has been distributed by WESTOMAT, Germany, throughout the world. To achieve this purpose, an energy-saving pressurized dosing furnace and molten metal differential pressure control system that Is able to automatically supply a determined quantity of aluminum molten metal were developed. The localized equipment was installed in a site. Also, the results of the test operation of this equipment can be summarized as follows: It was able to improve the productivity because there were small decreases in supplying speeds and small losses in wastes compared to the existing mechanical molten metal supplier. Also, it was able to minimize the cost in maintenances due to the direct application of high temperature molten metals to molds. In addition, there were small energy losses due to the use of high thermal insulators compared to the existing reverberating furnace and able to prolong the life-time of furnaces and produce good quality nonferrous metals because it represented small carbon refractories and alumina in applied molten metals. Furthermore, it demonstrated no particular differences by objectively comparing it with the product by WESTOMAT.

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Synthesis of Microcellular Cordierite Ceramics Derived from a Preceramic Polymer (Preceramic Polymer를 이용한 마이크로셀룰라 코디어라이트 세라믹스의 합성)

  • Song, In-Hyuck;Kim, Young-Mi;Kim, Hai-Doo;Kim, Young-Wook
    • Journal of the Korean Ceramic Society
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    • v.44 no.5 s.300
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    • pp.184-189
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    • 2007
  • In this study, a novel-processing route for producing microcellular cordierite ceramics has been developed. The proposed strategy for making the microcellular cordierite ceramics involves three steps: (i) fabricating ceramic-filled preceramic foams by heating a mixture of polysiloxane, expandable microspheres, talc, and alumina in a mold, (ii) cross-linking the foamed body, and (iii) transforming the body into microcellular cordierite ceramics by sintering. Cu jig was used for near net shaping in the foaming step. The experimental variables such as the shape of foaming jig and the content of expendable microsphere were investigated. By controlling the content of expendable microsphere, it was possible to make the porous cordierite ceramics with cell density of ${\sim}1.0{\times}10^9\;cells/cm^3$.

Surface Reaction Products of CP- Ti and Ti-25wt%Pd Castings Used for Dental Application (치과용 티타늄 및 Ti-25wt%Pd 주조체의 표면반응생성물)

  • 정준영;문수;이진형
    • Journal of Biomedical Engineering Research
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    • v.25 no.5
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    • pp.383-389
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    • 2004
  • A commercially pure Ti(CP-Ti) and Ti-25wt%Pd alloy for dental applications were cast into a phosphate-bonded Al$_2$ $O_3$/ $SiO_2$ investment mold and the surface of the casting specimens were investigated by means of SEM/EDS, XRD and XPS. The addition of 25wt%Pd in CP-Ti showed a moderate mold reaction owing to the considerable lowering of melting point. XRD analysis of the investment after burn-out treatment revealed that it consisted essentially of $SiO_2$, Al$_2$ $O_3$, P$_2$O$\_$5/, Mg$_3$(P $O_4$)$_2$, AlP $O_4$, Mg$_2$ $SiO_4$, MgAl$_2$ $O_4$ The mold reaction products were Ti$\_$5/Si$_3$ and Ti $O_2$ in case of CP-Ti casting and Ti $O_2$ and SiO$\_$x/ in case of Ti-25wt% Pd casting.

Characteristics of perovskite-structure Sr(Ti1-xFex)O3 thick film gas sensors (페롭스카이트 구조 Sr(Ti1-xFex)O3 후막 가스센서의 특성)

  • Jin, Guang-Hu;Lee, Woon-Young;Lee, Hyun-Gyu;Park, Jin-Seong
    • Journal of Sensor Science and Technology
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    • v.18 no.6
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    • pp.456-461
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    • 2009
  • Perovskite-structure $Sr(Ti_{1-x}Fe_x)O_3$ thick films, in which x is 0.4 or 0.6, were prepared by normal ceramic process on alumina substrate. Electrical resistance was measured as a function of thermal treatment condition including atmosphere, time, and temperature. The resistance of $Sr(Ti_{1-x}Fe_x)O_3$ films is lower than those of $SrTiO_3$ or $SrFeO_3$ films. The temperature coefficient of resistance over $550^{\circ}C$ was measured to be 0 for the $Sr(Ti_{1-x}Fe_x)O_3$ films after thermal treatment at $1100^{\circ}C$ in air. The sensing property of the films was also measured as a function of temperature and gas such as $O_2$, CO, $CO_2$, NO and $NO_2$. $Sr(Ti_{1-x}Fe_x)O_3$ films showed a good sensing property for $O_2$, but no sensing signal for CO, $CO_2$, NO and $NO_2$.

Effects of Y2O3 and Al2O3 Addition on the Properties of Hot Pressed AlN Ceramics (AlN 세라믹의 hot pressing에 사용되는 Y2O3 및 Al2O3 소결조제의 효과)

  • Kong, Man-Sik;Hong, Hyun-Seon;Lee, Sung-Kyu;Seo, Min-Hye;Jung, Hang-Chul
    • Korean Journal of Materials Research
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    • v.17 no.10
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    • pp.560-566
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    • 2007
  • AlN plates were fabricated by hot pressing at $1700-1900^{\circ}C$ using yttria and alumina (3 and $10\;{\mu}m$ particle size) powders as additives and characterized: density, thermal conductivity, transverse rupture strength, and grain size measurement by SEM and EDS. Density values of $3.31-3.34\;g/cm^3$ are largely attributed to hot pressing of powder mixtures in carbon mold under $N_2$ atmosphere which caused effective degree of oxygen removal from yttrium-aluminate phase expected to form at $1100^{\circ}C$. The grain size of hot pressed AlN was almost homogeneous, with size approximately from 3.2 to $4.0\;{\mu}m$ after hot pressing. $Al_2O_3$ powder of $3\;{\mu}m$ particle size resulted in better transverse rupture strength and finer grain size compared to $10\;{\mu}m$ $Al_2O_3$ powder. The thermal conductivity of AlN ranged between $83-92.7\;W/m{\cdot}K$ and decreased with $Al_2O_3$ addition. Fine grain size is preferred for better mechanical properties and thermal conductivity.

Analysis of the Phase Formation and the Sinterability of K+-β/β"-Al2O3 at High Temperatures (≥1600 ℃) (K+-β/β"-Al2O3의 고온 상관계와 소결성 분석)

  • Jang, Min-Ho;Kim, Seung-Gyun;Kim, Seok-Jun;Haw, Jung-Rim;Lim, Sung-Ki
    • Applied Chemistry for Engineering
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    • v.20 no.3
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    • pp.317-321
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    • 2009
  • In order to analyze the high temperature phase formation and the sinterability of super ionic conductor $K^+-{\beta}/{\beta}"-Al_2O_3$ which is commonly used as a solid oxide electrolyte, the pure $K^+-{\beta}/{\beta}"-Al_2O_3$ powder in the ternary system $K_2O-LiO_2-Al_2O_3$ was synthesized by solid state reaction and formed to tube and disk using slip casting method and cold isostatic pressing (CIP), respectively. The slip casting was conducted in an alumina mold with the slurry containing 40 wt% of solid contents and the CIP was carried out under 20 MPa. The samples were sintered at $1600^{\circ}C$, $1700^{\circ}C$ and $1750^{\circ}C$, respectively, and their phase formation and the sintering density were investigated according to the forming method. The samples produced by CIP showed far higher ${\beta}"-Al_2O_3$ fraction as compared with those by slip casting. On the other hand, the samples by slip casting showed slightly higher sintering density. The relative density reached to about 83% at $1750^{\circ}C$ and for 1 h, independent of the forming method. In the case of 90 min socking time, the density was decreased owing to the exaggerated grain growth and the pores by $K_2O$ evaporation.